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T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104
www.ijera.com 93 | P a g e
Investigation of Mechanical Properties in Polyester and Phenyl-
ester Composites Reinforced With Chicken Feather Fiber
T. Subramani1
, S.Krishnan2
, S.K.Ganesan3
, G.Nagarajan4
1
Professor & Dean, Department Of Civil Engineering, VMKV Engineering College, Vinayaka Missions
University, Salem, India.
2
Associate Professor and Head, Department of Mechanical Engineering, Mahendra College of Engineering,
Salem, India..
3
Assistant Professor, Department Of Mechanical Engineering, VMKV Engineering College, Vinayaka
Missions University, Salem, India.
4
Associate Professor, Department Of Mechanical Engineering, Annapoorna Engineering College, Salem,
Tamilnadu, India
ABSTRACT
The purpose of the study is to utilize the chicken feather and finding the mechanical properties of the chicken
feather reinforcing with polyester and phenyl ester. The bi-directional CFF reinforced composites were
produced with phenyl ester and polyester resins with fiber reinforced composites, the chicken feather fibers
(CFF) were cleaned, tested to know the mechanical properties and tensile behavior. It is found that the
compressive properties of the CFF reinforced composites are significantly better than the control composites,
however, the tensile and the flexural properties are determine by tensile, compressive, and flexural test. The
CFF reinforced composite have potential applications due to its improved behavior and structural applications.
The poultry waste can be utilized and used in any engineering applications, and it will be preferred due to low-
cost and superior characteristics and the most importantly it will not cause ecological and health problems.
KEYWORDS: Investigation, Mechanical Properties, Polyester Phenyl-ester Composites, Chicken Feather
Fiber.
I INTRODUCTION
1.1 CFF COMPOSITE
Throughout history, technological innovations
have helped humankind improve their standards of
living, with the rapidness of development and
research is so impressive. However, keratin
technology also creates a negative environmental
impact. Therefore efforts are invested in making use
of natural based biodegradable and sustainable
material that exist in nature rather than create a new
material. Textile structures reinforced composites,
specifically with fibres, have gained importance in
engineering and technical applications due to their
light weight, higher tenacity, superior elasticity and
strength, good thermal resistance, low density, and
better rigidity. The CFF are commonly described as a
waste by-product and they are contributing to
environmental pollution due to the disposal problems.
There are two main chicken feather disposal methods
that exist, a burning and burying. Both of them have
negative impact on the environment. Recent studies
on the chicken feather waste demonstrated that the
waste can be a potential composite reinforcement.
The composite reinforcement application of the CFF
offers much more effective way to solve
environmental concerns compared to the traditional
disposal methods. Some of the advantages of the CFF
are inexpensive, renewable available. The CFF as a
composite reinforcement having certain desirable
properties including lightweight, high thermal
insulation, excellent acoustic properties, non-
abrasive behavior and excellent hydrophobic
properties. The CFF has the lowest density value
compared to the all natural and synthetic fibers. The
found that the CFF keratin biofibers allows an even
distribution within and adherence to polymers due to
their hydro-phobic nature and they reported that CFF
reinforced composites have good thermal stability
and low energy dissipation. The main purpose of this
study is to manufacture and determine the mechanical
properties of the CFF reinforced phenyl ester and
polyester thermo set composites. The chicken feather
fibres were tested and analyzed to identify the
properties. The CFF reinforced composites were
fabricated by hand layup techniques. phenylester and
polyester resin were used as matrixes and the
composites were manufactured by using three
different fibre mixing proportions. The mechanical
properties of these composites were determined and
compared including tensile, flexural and compressive
test properties.
This industry has changed very little throughout ages
and still generates money by either
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(i) exporting raw materials (jute, flax, sisal
or coir, animal) or
(ii) manufacturing
Traditional products such as bags, carpet backing,
ropes, baskets, brushes and paper. Both have Suffered
a decrease in revenue in the past years due to stiff
competition with synthetic Materials and Related
products. The strategy discussed in this report aims to
add value to the crops by processing the fibres into so
called natural fibre composites. Composites are
hybrid materials made of a polymer resin reinforced
by fibres, combining the high mechanical and
physical performance of the fibres and the
appearance, bonding and physical properties of
polymers. Due to the wide variety of available
manufacturing processes, each resulting in their own
characteristic products, the design possibilities are
numerous. Consequently, a composite product and its
manufacturing process can be chosen to best fit the
environment in which the products will be made and
used. Besides the technical feasibility, manufacturing
of composites becomes also financially feasible when
using domestically grown natural fibres in
combination with simple manufacturing processes.
Potential products are roofing panels, fluid
containers, bridges and Small boats. Due to the
interest of western society in environmental friendly
high performance materials, Research institutes such
as Delft University of Technology already possesses
detailed knowledge on natural fibre composites.
Using the natural fibre link, which connects the
western composite industry to the traditional rural
fibre industry, will facilitate the transfer of this
knowledge. This link results in four benefits:
 Matching modern and traditional technology
 Compatibility of different cultures
 Increasing use of sustainable, cheap natural
resources
When starting up a natural fibre composite
industry, the benefits can be summarized into
Economical, Environmental and Technical, as
follows:
 The entire production chain can be developed,
maximizing the benefits for the targeted
 in terms of money and employment.
 Due to the interest on natural fibre composites
in western world, targeted countries can
participate in co-operative research,
participating in globalization. This is increased
when Also the export market for natural fibre
composites is aimed at.
 Environmental benefits can be found in the
sustainable character of the materials used and
the fact that NF composites can replace tropical
hardwood.
 Working conditions are improved due to the
friendly character of the fibres (no skin
irritation) and lightweight property of the
products, reducing the physical strain of the
work. The latter benefits women largely, since
they are well represented in the rural industry.
1.2 GENERAL CHARACTERISTICS OF CFF
In this way, lignin dissolved in styrene could be
incorporated into thermosetting matrix and perform
The following enhancements:
(a) Acting as a toughening agent
(b) Improving the connectivity in the network
(c) Adding additional stiffening groups to the matrix
(d) Acting as a sizing agent between natural fibers
and the resin matrix
(e) Behaving as a co monomer for the resin
(f) Inducing plasticity in the deformation zone at
crack tips to improve toughness,
(g) Acting as a free radical trap to reduce radical
scission effects during fracture in highly cross linked
polymers
(h) Improving flame resistance
(i) Modifying biodegradability
(j) Providing enhanced photo resistance and thermal
stability
(k) Expanding fatigue lifetime
(l) Contributing to the green engineering of materials
Chicken feathers are a waste product from the
processing of chickens for food. Chicken feather fiber
(CFF) offers a large, cheap fiber market as an
additive for medium density fiberboard (MDF).
Chicken feathers consist of approximately half fiber
and half quill (by weight). Both the fiber and quill
consist of hydrophobic keratin, a protein with
strength similar to that of nylon and with a diameter
smaller than that of wood fiber. The quills have
commercial applications in shampoo, hair
conditioner, hair coloring, and dietary supplements.
The fiber is more durable than the quill and has a
higher aspect ratio. Finding a high-volume, high-
value use for CFF, which is most commonly land
filled or used for feed protein, would greatly benefit
the poultry industry and would represent another
source of fiber for the wood industry.
1.3 USES OF CHICKEN FEATHER
While feathers are often considered a by-product
of poultry production (and often a waste by-product),
some produces raise poultry specifically for their
feathers. Feathers are used in a number of decorative
products such as boas, feather fans, masks, costume
accessories, bird ornaments, and even earrings and
flowers. Feathers are also routinely used in the
production of fishing flies. While chicken feathers
don't weigh much, with the amount of chicken
produced in the annually, the volume of feathers
produced is considerable. For the 8+ billion broilers
produced each year, 2-3 billion pounds of feathers are
produced. Research has shown that the keratin in the
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feathers (a protein also found in hair, hoofs, horns,
and wool) can be used in the production of a wide
variety of products. Feather protein has properties in
common with cellulose, the starch that forms wood
and paper. Feathers are keratin just like wool but the
surface area is much large because the diameter of the
fibers is smaller. So the fiber can absorb more than
wool or cellulose fibers. The crystal structure of
feather fibers also makes them naturally stable and
durable. More than 16 million diapers, made from
wood pulp, are discarded each year. A year's worth of
feathers could replace approximately 25% of the
wood pulp used annually for diapers. Three
companies – Feather fiber Corporation, Maxim
Systems and Tyson Foods - are now working to scale
up production of absorbent feather-based products
including diapers, filters, insulation, upholstery
padding, paper and even clothing. The orderly
structure of keratin helps stabilize the structure of
plastics, making them stronger. Feather meal is
produced by a high-pressure steam processing
method similar to autoclaving, followed by drying.
Heat and steam hydrolyze the feathers into a cysteine-
rich, high protein product that is 60% digestible.
1.4 GENERAL CHARACTERISTICS
1.4.1 Poly ester& Phenyl ester
Polyester fibres are produced by the melt
spinning process. Raw materials are heated to a
spinning mass, which is then pressed through
spinnerets. Manufacturing techniques are now
developed to the point where they can produce fibres
adapted to suit the widest possible. Applications: they
can have round, oval or angular profiles, making
them firm to the touch. They can be dull, bright or
glittery On care labels polyester fibres are often given
the abbreviation: "PES".
1.4.2.Properties
Amongst the most important properties:
 Polyester fibres are particularly resistant to light
and weather and can withstand climatic effects.
 They can be used where lightness and fineness
are primary requirements.
 Polyester fibres are very well suited to blends
with natural fibres.
 Fabrics in 100% polyester, or blends with an
appropriately high proportion, are very crease-
resistant and retain shape even when affected by
moisture. fibres have good moisture transport
and dry quickly.
 Polyester is the number one manmade fiber used
in fabrics, worldwide. It tends to be an
inexpensive fiber to produce and its general
characteristics and non crop-based availability
have allowed for the creation of inexpensive
clothing and fabrics, which transformed the
textile industry in 1941. The largest innovation in
polyester was the recent discovery of
microfibers. This discovery allowed polyester
manufacturers to transform the texture and feel
of polyester into a super-soft, durable,
lightweight fabric.
 Polyester was introduced to the American public
in 1951 as the fabric that doesn't need to be
ironed. It quickly became known as wash-and-
wear fabric. However, it also earned other, less
flattering attributions, such as causing skin
irritations with some people or being texturally
unpleasant to the touch.
 Wearing polyester became associated with being
cheap and this connection has continued to affect
how consumers perceive the product. This drove
more innovation in the industry as manufacturers
began to hide or reliable polyester in new
blended fabrics.
 The properties of polyester fabrics include:
inexpensive cost; superior strength and
resilience; lightweight; hydrophobic (it feels dry
or moves moisture effects away from touch); it
has an unusually high melting point; is resistant
to dyes, solvents and most chemicals; stain
resistant; resists stretching and shrinking; quick
drying; wrinkle, mildew and abrasion resistant;
retains heat-set pleats and creases and is easy to
launder
III MATERIALS
3.1 CHICKEN FEATHER FIBER STRUCTURE
OF CHICKEN FEATHER
Figure 3.1 Structure of a contour feather
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Figure 3.2
Down feathers are smaller than contour
feathers and lack barbules and the accompanying
hooklets. They are soft and fluffy, located beneath the
contour feathers. They provide most of a chicken's
insulation. There are several subcategories of down,
including natal down, present only at hatching, and
powder down, which is a specialized feather type that
sheds a fine, white keratin powder. The waxy powder
is composed of granules so small that it is unwettable
and thus forms a waterproof barrier for contour
feathers(Figure 3.1 & Figure 3.2).
The semi plume is a feather type that mediates
between the categories of contour and down. Semi
plumes share characteristics with both; they have a
large rachis and predominantly downy vanes.
Filoplumes are smaller than semi plumes, with only a
few barbs at the tip of a fine shaft. These likely serve
a sensory function in chickens, registering vibrations
and changes in pressure. The smallest type of feather
is the bristle, which is stiff and has few, if any, short
barbs near the tip. Bristles are protective in function
and are found on a chicken's head, at the base of the
beak, around the eyes, and covering the nostrils.
While older and larger chickens would be expected to
have relatively more contour feathers. (Figure.3.3 &
Figure 3.4)
3.2 PICTURE OF CHICKEN FEATHER
Figure 3.3 Picture Of Chicken Feather
In order to maximize the yield of a desirable type of
feathers, feather collection could be Planned for days
on which chickens of a particular feather type
distribution are processed. Each contour feather has a
feather shaft and a flat vane extending from it .The
naked portion of the shaft that is implanted in a bird's
skin is the calm‟s. The portion bearing branches is the
rachis, which is filled with a porous substance termed
the medulla. Branches are termed barbs and provide
an axis from which barbules can branch. Barbules are
very closely spaced and interlock via hook lets, or
barbicels, in order to provide strength and repel
water. Flightless birds, including the emu and the
ostrich, have few, if any, hook lets .Thus, it can be
assumed that hook lets are not abundant in chickens.
3.3 PRIMARY TYPES OF CHICKEN FEATHER
Figure 3.4The five primary types of chicken feathers
(a) contour (b) bristle, (c) semiplume, (d) down, (e)
filoplume
3.4 PROCESSED CHICKEN FEATHER
FRACTIONS
Large contour feathers are approximately
half feather fiber and half quill by mass These are
useful categories because several companies‟
proprietary processing technologies yield these two
fractions, fiber and quill, shown in. Also, that fiber
keratin and quill keratin are characteristic of the two
forms of microcrystalline keratin in feathers. In
simple terms, the quill is the hard. Central axis off
which soft, interlocking fibers. The fibers are hollow
Smaller feathers have a greater proportion of fiber,
which has a higher aspect ratio than the quill as is
apparent in single keratin fiber has a maximum
diameter of 50 μm . Quill fractions are composed of
both inner and outer quill; outer quill is more densely
structured than inner quill, which is porous, as is
apparent in have reported that the presence of quill
among fibers results in a more granular, lightweight
and bulky material. A typical quill has dimensions on
the order of centimeters (length) by millimeters
(diameter).
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3.5 CROSS SECTION VIEW OF CHICKEN
FEATHER
Figure 3.5 Cross Section View Of Chicken Feather
3.6 CONSTITUTION OF CHICKEN FEATHER
 Serine -16%
 Proline -12%
 Glycine -11%
 Valine -9%
 Cysteine-7%
And the rest are numerous amino acids in
small percentages
Chicken feather is treated as a waste product from
the poultry sector, approximately „2*1013
kg of
chicken feather generated in India every year.The
cross section and the longitudinal features of the
different region of the rachis and the Barbs. Hence,
the ESEM micrographs of the barbs showed a
tertiary structure, i.e. the barbules that are attached
to the barbs in a manner similar to the barbs being
attached to the rachis. Thus, according to the ESEM
micrographs, a feather is composed of four units, i.e.
the calm‟s, the rachis the barbs and the barbules.
Show the morphological features of the main units
of the poultry feather shows the two principal units,
namely the rachis and the barbs shows the secondary
and the tertiary units, namely the barbs and the
barbules. The barbules are attached to the barbs in a
manner similar to the barbs being attached to the
rachis shows the primary, the secondary and the
tertiary units.
3.7 PREPARATION OF CHICKEN FEATHER
Figure 3.6 Raw Poultry Feather
Figure 3.7 Water Treatment
The concentration of the chemical solutions
is function of nature and the desired product. Hence,
according to the application, the poultry feathers
may be converted to useful products in the form of
powder, fiber or wool. In combination with a
suitable resin, the aforementioned natural fibres can
be turned in to NF Composites. The resin is applied
as a liquid and turns solid upon drying. Whereas the
fibres add strength to the composite, the resin must
at least have the following characteristics:
Figure 3.8 Wool Product
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 Good impregnation To allow all the different
fibres to act as a single material, even the
smallest fibres have to be „glued‟ together by
the resin. The better the impregnation the
higher the load a Composite can carry.
 Control moisture content of the natural fibres
After processing, the natural fibres still
contain a significant amount of water. The
strength of the fibre is highest at a certain
percentage of moist. Therefore the fibre must
neither be too dry or too moist. The resin
must allow evaporation of superfluous moist
before it forms an impermeable solid film.
 Non-toxic Since in most of the rural societies
health regulations at the work-floor are
absent,Application of toxic materials will be
an act of violence.
 High availability usually a higher availability
results in a reduction of material costs.
3.8 SAMPLE PREPARATION IN POLYESTER
Table-3.1 Sample Preparation In Polyester
POLY ESTER
(in gms)
FIBER
(Chicken
Feather)
(in gms)
TOTAL
(in gms)
STRIP
PREPARATIO
N
FINDING
PROPERTIES
80 20 100 BIE-
DIRECTION
Tensile
Compressive
Flexural Rigidity
70 30 100
UNI-
DIRECTION
Tensile
Compressive60 40 100
Flexural Rigidity
3.9 SAMPLE PREPARATION IN PHENYL
ESTER
Table-3.2 Sample Preparation In Phenyl Ester
POLY ESTER
(in gms)
FIBER
(Chicken
Feather)
(in gms)
TOTAL
(in gms)
STRIP
PREPARATIO
N
FINDING
PROPERTIES
80 20 100 BIE-
DIRECTION
Tensile
Compressive
Flexural Rigidity
70 30 100
UNI-
DIRECTION
Tensile
Compressive60 40 100
Flexural Rigidity
3.10 RESIN PREPARATION
Figure 3.9 Wool Product
The matrix material is a general purpose unsaturated
polyester resin available from “FIBER CHEM
PRODUCTS” In Salem. Due to the fact that the
keratin feather fibers are characterized by a very
short and classified as a fibers, and they were washed
by using a lab dyeing machine with a polar solvent
(ethanol). After the washing process the chicken
features were rinsed and left to dry for 24 hours under
normal room temperatures. The highly filled
composites are prepared by a new technique
developed. The concentration range was varied from
10%to 30% mixing of feathers because of practical
reasons
3.11METHODS
3.11.1 Hand lay-up
Prior to the composite manufacturing, the
CFF samples were conditioned for 48 hours at the
fibre linear density values were determined in
accordance with ASTM and the tensile properties of
the fibres were determined in accordance with
ASTM. The composites were fabricated with
different fibre loadings (10%, 20% and 30%).
Initially, polyester resin was mixed in hardener using
a mixer in a bowl after the phenyl ester, polyester,
resin was also prepared separately. The matrix
materials were prepared in a portion of 70% of resin
matrix and 30% of hardener by volume. Then, the
fibres were spread into mould and covered with the
matrix. The composites were manufactured by using
a hand lay-up technique with size mould of 210 mm
length x 210 mm width x 10 mm thickness. The
composites were kept for 24 hours at room
temperature and subsequently put in an oven for 8
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hours at 80°C for curing. The control and the CFF
reinforced composites were evaluated in accordance
with ASTM size.
3.12 MOULD PREPATATION
Dimension of the cavity :l x b x t =
200mm x 150mm x10mm.
Figure :3-10 Source Of Feathers
Fig:3-11 Source Of Feathers
Feathers collected at the Gold Kist chicken
processing facility had been removed from chickens
by hot water and mechanically driven rubber fingers
and then diverted from the plant in a trough of water.
The feathers were collected by hand from a conveyor
belt carrying waste – chicken heads, feet, and feathers
– to an offal truck. The feathers were transported on
ice and then frozen, because feather masses which are
commingled with chicken parts, water, and fats
decompose in a biological process that is accelerated
at high temperatures. The feathers were later cleaned
in a washing machine with approximately 7 L of anti-
microbial soap per m
3
of feathers and then dried in a
rotary drier.
Figure 3.10 & Figure 3.11 shows the source
of feathers and processing information. Processing
involves grinding the feathers and separating them
into fiber and quill fractions. All examined quill
fractions were composed of both inner and outer
quill. Details on how the feathers are processed are
generally difficult to ascertain, as many of the
processing techniques are proprietary. Sample B was
cut by hand at Georgia Tech into fiber and quill
fractions. The fiber fraction was then chopped with a
household coffee grinder until each fiber was
separated.
3.13 STRIP PREPARATION
Figure 3.12 Strip Preparation
Figure 3.12 Strip Preparation
Dimensions:
Tensile Test : l x b x t = 150mm x 25mm x 10mm.
Flexural Test : l x b x t = 150mm x 25mm x 10mm
Impact Test : l x b x t =150mm x 10mm x 10mm
As materials suppliers, very little training is required
since this segment is already well Developed. The
only required training might be to produce spun yarns
with a variety in thicknesses and fabrics with
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different weave patterns. It is also important that as
sale of composites increases, local farmers are
persuaded to increase fibre production to meet the
demand. A point of attention is the fact that today the
natural fibres and the related processes are optimized
to produce an optimum fibre for textile applications.
For natural fibres for composite applications, a
different variety of fibres and different way of
processing might be more suitable.
3.14 WORK PIECE WITH TESTING FIGURE
Figure 3.13 Strip Preparation and Testing
The development of successful applications
for CFM will be aided by an understanding of their
mechanical properties. Selecting compatible matrix
materials for CFM will specifically require an
understanding of the Young‟s module chicken feather
fractions.
IV RESULT AND DISCUSSION
It can be seen that CFF reinforced
composite will have potential applications due to its
improved the behaviour, the tensile and flexural
properties can be enhanced with the increasing
percentage of CFF and also different resin. Another
way to enhance the composite properties is to
determine an effective treatment to eliminate lack of
adhesion between matrix and CFF fiber.
4.1 TENSILE TEST PERFORMENCE
The details of Tensile Test of composite for
varies percentage of CFF with Phenyl Ester and
Polyester mixtures as follows:
4.1.1 COMPARISION OF TENSILE TEST :
Composites
Cross
Sectional
Area
[mm2
]
Peak
Load
(in N)
%
Elongation
UTS
[N/mm
2
]
10 CFF- 90%
Phenyl Ester
275 401.778 1.440 1.462
20 CFF -80%
Phenyl ester
250 461.482 3.380 1.844
30 CFF -70%
Phenyl ester
300 268.353 1.560 0.893
10 CFF - 90%
Polyester
200 538.020 1.480 2.688
20 CFF -
80%
Polyester
200 943.732 2.780 4.719
30 CFF -70%
Polyester
250 228.867 0.980 0.912
x-axis : composites in %
y-axis : Tensile Stress [N/mm2
]
4.1.2 Graph for Tensile Test
Composite Material : 10%CFF & 90%Phenylester.
0
1
2
3
4
5
UTS
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Composite Material : 20%CFF & 80%Phenylester.
Composite Material: 30%CFF & 70%Phenylester.
Composite Material : 10%CFF & 90%Polyester.
Composite Material: 20%CFF & 80%Polyester.
Composite Material : 30%CFF & 70%Polyester.
4.2.BENDING TEST PERFORMANCE
The details of flexural Test of composite
for varies percentage of CFF with Phenyl Ester and
Polyester mixtures as follows:
4.2.1 COMPARISION OF BENDING TEST:
Composites
Cross
Sectional
Area
[mm2
]
Peak Load
[N]
Flexural
Strength
(Mpa)
Flex
ural
Mod
ulas
Gpa
)
10 CFF-
90% Phenyl
Ester
156 214.849 10.846
5.84
9
20 CFF -
80% Phenyl
ester
104 114.228 12.974
17.7
65
30 CFF -
70% Phenyl
ester
156 265.380 13.391
5.90
8
10 CFF -
90%
Polyester
104 96.825 10.997
13.8
25
20 CFF -
80%
Polyester
104 139.292 15.821
14.5
20
30 CFF -
70%
Polyester
130 175.736 12.775
8.74
9
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x-axis : Composites in %
y-axis : Flexural Strength(Mpa)
4.2.2 Graph for Flexural Test
Composite Material : 10%CFF & 90%Phenylester
Composite Material : 20%CFF & 80% Phenylester.
Composite Material : 30%CFF & 70%Phenylester.
Composite Material : 10%CFF & 90% Polyester.
Composite Material : 20%CFF & 80%Polyester.
Composite Material : 30%CFF & 70%Polyester..
4.3 IMPACT TEST
WhWhen the Impact resistance decreases with an increase
n in the modulus of elasticity, which means that stiffer
mamaterials will have less impact resistance. Resilient
mamaterials will have better impact resistance. The details
of of Impact Test of composite for varies percentage of
CF CFF with Phenyl Ester and Polyester mixtures as
follfollows:
0
5
10
15
20
Flexural
Strength(Mp
a)
T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104
www.ijera.com 103 | P a g e
Figure 4.3 Broken Workpiece After The Test
4.3.1 COMPARISION OF IMPACT TEST:
Sl.No Sample Composites
Impact value for
given sample in J
1.
10 CFF -
90%Phenylester
0.35
2.
20 CFF -
80%Phenylester
0.35
3.
30 CFF -
70%Phenylester
0.30
4. 10 CFF -90%Polyester 0.25
5. 20 CFF -80%Polyester 0.40
6. 30 CFF -70%Polyester 0.25
x-axis : Composites in % y-axis : Impact Value
in Joule.
V CONCLUSIONS
Usually the poultry waste are still destroyed by
using either burning or burying methods This studies
helps that the poultry waste can be utilised and used
any engineering applications and it will be preferred
due to low cost and superior characteristics and the
most importantly it is ecological and health
problems. The investigation shows that 20 % CFF
and 80% Polyester having highly superior properties
such as tensile, flexural and impact value The
tensile and flexural property values decrease when
the fibre loading percentages increases. Thus, the
reinforced composite better than at 5% level and the
Tensile and flexural properties of composite are
control with the resins Polyester having
significantly superior properties to the 25% CFF
reinforced composite. The CFF reinforced composite
have potential applications based on the mixer of
varies different resin and CFF fiber due to
improving its behaviour. The tensile and flexural
properties can be enhanced with the increasing the
percentage of CFF and also with different resin are
considered to eliminate lack of adhesion between
matrix and CFF fibre.
REFERENCES
[1]. A.L. Martı´nez-Herna´ndez, C. Velasco-
Santos, M. de-Icaza, Victor M. Castan.O,
Dynamical–mechanical and thermal analysis
of polymeric composites reinforced with
keratin biofibers from chicken feathers,
Composites: Part B 38 (2007) 405–410
[2]. Saira Taj, Munawar Ali Munawar, and Shafi
ullah Khan “Natural Fiber-Reinforced
Polymer Composites , Proc. Pakistan Acad.
Sci. 44(2):129-144.2007
[3]. D.Verma1, P.C.Gope, A.Shandilya,
A.Gupta, M.K.Maheshwari, “ Coir Fibre
Reinforcement and Application in Polymer
Composites: A Review” J. Mater. Environ.
Sci. 4 (2) (2013) 263-276, ISSN: 2028-2508,
CODEN: JMESCN
[4]. Wrześniewska-tosik K., Marcinkowska M.,
Niekraszewicz A., Potocka D. A., Mik
Pałczyńska M. “Fibrous Composites Based
on Keratin from Chicken Feathers” Fibres &
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[5]. Jyoti Prakash Dhal and S. C. Mishra
“Processing and Properties of Natural Fiber-
Reinforced Polymer Composite” Hindawi
Publishing Corporation, Journal of
Materials, Volume 2013, Article ID 297213,
6 pages 24 November 2012
[6]. Oladele I. O, Omotoyimbo J. A,
Ayemidejor S. H. “ Mechanical Properties of
Chicken Feather and Cow Hair Fibre
Reinforced High Density Polyethylene
Composites” International Journal of
Science and Technology Volume 3 No. 1,
January, 2014, PP 66-72
[7]. Jerrold E. Winandy James H. Muehl Jessie
A. Glaeser Walter Schmidt, “ Chicken
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Composites” Journal of Natural Fibers, Vol.
4(1) 2007, PP 35 -48
0
0.2
0.4
0.6
Impact
Value in J
T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com
ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104
www.ijera.com 104 | P a g e
[8]. Dr. Shajan Kuriakose, Dr. Deviprasad
Varma, Vaisakh V.G “ Mechanical
Behaviour of Coir reinforced Polyster
Composites–An Experimental Investigation”
IJETAE, ISSN 2250-2459, ISO 9001:2008,
(Volume 2, Issue 12, December 2012) , PP
751-747
[9]. C.Mahesh, B.Kondapanaidu,
K.Govindarajulu, and V.Balakrishna murthy,
“Experimental Investigation of Thermal and
Mechanical Properties ofPalmyra Fiber
Reinforced Polyster Composites With and
Without Chemical Treatment and Also
Addition of Chalk Powder” IJETT – Volume
5 Number 5 - Nov 2013, ISSN: 2231-5381,
PP 259 -271
[10]. K B jagadeeshgouda, P Ravinder Reddy, K
ishwaraprasad “Experimental Study Of
Behaviour Of Poultry Feather Fiber - A
Reinforcing Material For Composites”
IJRET: (EISSN: 2319-1163 | PISSN: 2321-
7308) VOLUME: 03 ISSUE: 02 | Feb-
2014,PP 362-371
[11]. D. Chandramohan & .K. Marimuthu, “ A
Review On Natural Fibers” Volumes/ Vol 8,
Issue2 / IJRRAS 8 (2) August 2011, PP
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[12]. V. Ananda Rao, Alok Satapathy, S.C.
Mishra, “ Polymer composites reinforced
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December 12-14, 2007, Indian Institute of
Technology Kanpur
[13]. Anthony N. Anyakora, “Investigation of
Mechanical Properties of Polyester Matrix
Reinforced with Coconut Palm Frond Fiber
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2012, [ISSN: 2045-7057] PP 1-6
[14]. Ahmed Salhi, Salah Kaci1, A.Boudene and
Y. Candau, “Development of Biocomposites
Based of Polymer Metrix and Keratin
Fibers:Contribution to Poultry FEATHER
biomass Recycling. Part-i” Conference and
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[15]. S. C. Mishra and Nadiya Bihary Nayak,
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pp 1794-1804, 2012.

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Investigation of Mechanical Properties in Polyester and Phenyl-ester Composites Reinforced With Chicken Feather Fiber

  • 1. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 93 | P a g e Investigation of Mechanical Properties in Polyester and Phenyl- ester Composites Reinforced With Chicken Feather Fiber T. Subramani1 , S.Krishnan2 , S.K.Ganesan3 , G.Nagarajan4 1 Professor & Dean, Department Of Civil Engineering, VMKV Engineering College, Vinayaka Missions University, Salem, India. 2 Associate Professor and Head, Department of Mechanical Engineering, Mahendra College of Engineering, Salem, India.. 3 Assistant Professor, Department Of Mechanical Engineering, VMKV Engineering College, Vinayaka Missions University, Salem, India. 4 Associate Professor, Department Of Mechanical Engineering, Annapoorna Engineering College, Salem, Tamilnadu, India ABSTRACT The purpose of the study is to utilize the chicken feather and finding the mechanical properties of the chicken feather reinforcing with polyester and phenyl ester. The bi-directional CFF reinforced composites were produced with phenyl ester and polyester resins with fiber reinforced composites, the chicken feather fibers (CFF) were cleaned, tested to know the mechanical properties and tensile behavior. It is found that the compressive properties of the CFF reinforced composites are significantly better than the control composites, however, the tensile and the flexural properties are determine by tensile, compressive, and flexural test. The CFF reinforced composite have potential applications due to its improved behavior and structural applications. The poultry waste can be utilized and used in any engineering applications, and it will be preferred due to low- cost and superior characteristics and the most importantly it will not cause ecological and health problems. KEYWORDS: Investigation, Mechanical Properties, Polyester Phenyl-ester Composites, Chicken Feather Fiber. I INTRODUCTION 1.1 CFF COMPOSITE Throughout history, technological innovations have helped humankind improve their standards of living, with the rapidness of development and research is so impressive. However, keratin technology also creates a negative environmental impact. Therefore efforts are invested in making use of natural based biodegradable and sustainable material that exist in nature rather than create a new material. Textile structures reinforced composites, specifically with fibres, have gained importance in engineering and technical applications due to their light weight, higher tenacity, superior elasticity and strength, good thermal resistance, low density, and better rigidity. The CFF are commonly described as a waste by-product and they are contributing to environmental pollution due to the disposal problems. There are two main chicken feather disposal methods that exist, a burning and burying. Both of them have negative impact on the environment. Recent studies on the chicken feather waste demonstrated that the waste can be a potential composite reinforcement. The composite reinforcement application of the CFF offers much more effective way to solve environmental concerns compared to the traditional disposal methods. Some of the advantages of the CFF are inexpensive, renewable available. The CFF as a composite reinforcement having certain desirable properties including lightweight, high thermal insulation, excellent acoustic properties, non- abrasive behavior and excellent hydrophobic properties. The CFF has the lowest density value compared to the all natural and synthetic fibers. The found that the CFF keratin biofibers allows an even distribution within and adherence to polymers due to their hydro-phobic nature and they reported that CFF reinforced composites have good thermal stability and low energy dissipation. The main purpose of this study is to manufacture and determine the mechanical properties of the CFF reinforced phenyl ester and polyester thermo set composites. The chicken feather fibres were tested and analyzed to identify the properties. The CFF reinforced composites were fabricated by hand layup techniques. phenylester and polyester resin were used as matrixes and the composites were manufactured by using three different fibre mixing proportions. The mechanical properties of these composites were determined and compared including tensile, flexural and compressive test properties. This industry has changed very little throughout ages and still generates money by either REVIEW ARTICLE OPEN ACCESS
  • 2. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 94 | P a g e (i) exporting raw materials (jute, flax, sisal or coir, animal) or (ii) manufacturing Traditional products such as bags, carpet backing, ropes, baskets, brushes and paper. Both have Suffered a decrease in revenue in the past years due to stiff competition with synthetic Materials and Related products. The strategy discussed in this report aims to add value to the crops by processing the fibres into so called natural fibre composites. Composites are hybrid materials made of a polymer resin reinforced by fibres, combining the high mechanical and physical performance of the fibres and the appearance, bonding and physical properties of polymers. Due to the wide variety of available manufacturing processes, each resulting in their own characteristic products, the design possibilities are numerous. Consequently, a composite product and its manufacturing process can be chosen to best fit the environment in which the products will be made and used. Besides the technical feasibility, manufacturing of composites becomes also financially feasible when using domestically grown natural fibres in combination with simple manufacturing processes. Potential products are roofing panels, fluid containers, bridges and Small boats. Due to the interest of western society in environmental friendly high performance materials, Research institutes such as Delft University of Technology already possesses detailed knowledge on natural fibre composites. Using the natural fibre link, which connects the western composite industry to the traditional rural fibre industry, will facilitate the transfer of this knowledge. This link results in four benefits:  Matching modern and traditional technology  Compatibility of different cultures  Increasing use of sustainable, cheap natural resources When starting up a natural fibre composite industry, the benefits can be summarized into Economical, Environmental and Technical, as follows:  The entire production chain can be developed, maximizing the benefits for the targeted  in terms of money and employment.  Due to the interest on natural fibre composites in western world, targeted countries can participate in co-operative research, participating in globalization. This is increased when Also the export market for natural fibre composites is aimed at.  Environmental benefits can be found in the sustainable character of the materials used and the fact that NF composites can replace tropical hardwood.  Working conditions are improved due to the friendly character of the fibres (no skin irritation) and lightweight property of the products, reducing the physical strain of the work. The latter benefits women largely, since they are well represented in the rural industry. 1.2 GENERAL CHARACTERISTICS OF CFF In this way, lignin dissolved in styrene could be incorporated into thermosetting matrix and perform The following enhancements: (a) Acting as a toughening agent (b) Improving the connectivity in the network (c) Adding additional stiffening groups to the matrix (d) Acting as a sizing agent between natural fibers and the resin matrix (e) Behaving as a co monomer for the resin (f) Inducing plasticity in the deformation zone at crack tips to improve toughness, (g) Acting as a free radical trap to reduce radical scission effects during fracture in highly cross linked polymers (h) Improving flame resistance (i) Modifying biodegradability (j) Providing enhanced photo resistance and thermal stability (k) Expanding fatigue lifetime (l) Contributing to the green engineering of materials Chicken feathers are a waste product from the processing of chickens for food. Chicken feather fiber (CFF) offers a large, cheap fiber market as an additive for medium density fiberboard (MDF). Chicken feathers consist of approximately half fiber and half quill (by weight). Both the fiber and quill consist of hydrophobic keratin, a protein with strength similar to that of nylon and with a diameter smaller than that of wood fiber. The quills have commercial applications in shampoo, hair conditioner, hair coloring, and dietary supplements. The fiber is more durable than the quill and has a higher aspect ratio. Finding a high-volume, high- value use for CFF, which is most commonly land filled or used for feed protein, would greatly benefit the poultry industry and would represent another source of fiber for the wood industry. 1.3 USES OF CHICKEN FEATHER While feathers are often considered a by-product of poultry production (and often a waste by-product), some produces raise poultry specifically for their feathers. Feathers are used in a number of decorative products such as boas, feather fans, masks, costume accessories, bird ornaments, and even earrings and flowers. Feathers are also routinely used in the production of fishing flies. While chicken feathers don't weigh much, with the amount of chicken produced in the annually, the volume of feathers produced is considerable. For the 8+ billion broilers produced each year, 2-3 billion pounds of feathers are produced. Research has shown that the keratin in the
  • 3. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 95 | P a g e feathers (a protein also found in hair, hoofs, horns, and wool) can be used in the production of a wide variety of products. Feather protein has properties in common with cellulose, the starch that forms wood and paper. Feathers are keratin just like wool but the surface area is much large because the diameter of the fibers is smaller. So the fiber can absorb more than wool or cellulose fibers. The crystal structure of feather fibers also makes them naturally stable and durable. More than 16 million diapers, made from wood pulp, are discarded each year. A year's worth of feathers could replace approximately 25% of the wood pulp used annually for diapers. Three companies – Feather fiber Corporation, Maxim Systems and Tyson Foods - are now working to scale up production of absorbent feather-based products including diapers, filters, insulation, upholstery padding, paper and even clothing. The orderly structure of keratin helps stabilize the structure of plastics, making them stronger. Feather meal is produced by a high-pressure steam processing method similar to autoclaving, followed by drying. Heat and steam hydrolyze the feathers into a cysteine- rich, high protein product that is 60% digestible. 1.4 GENERAL CHARACTERISTICS 1.4.1 Poly ester& Phenyl ester Polyester fibres are produced by the melt spinning process. Raw materials are heated to a spinning mass, which is then pressed through spinnerets. Manufacturing techniques are now developed to the point where they can produce fibres adapted to suit the widest possible. Applications: they can have round, oval or angular profiles, making them firm to the touch. They can be dull, bright or glittery On care labels polyester fibres are often given the abbreviation: "PES". 1.4.2.Properties Amongst the most important properties:  Polyester fibres are particularly resistant to light and weather and can withstand climatic effects.  They can be used where lightness and fineness are primary requirements.  Polyester fibres are very well suited to blends with natural fibres.  Fabrics in 100% polyester, or blends with an appropriately high proportion, are very crease- resistant and retain shape even when affected by moisture. fibres have good moisture transport and dry quickly.  Polyester is the number one manmade fiber used in fabrics, worldwide. It tends to be an inexpensive fiber to produce and its general characteristics and non crop-based availability have allowed for the creation of inexpensive clothing and fabrics, which transformed the textile industry in 1941. The largest innovation in polyester was the recent discovery of microfibers. This discovery allowed polyester manufacturers to transform the texture and feel of polyester into a super-soft, durable, lightweight fabric.  Polyester was introduced to the American public in 1951 as the fabric that doesn't need to be ironed. It quickly became known as wash-and- wear fabric. However, it also earned other, less flattering attributions, such as causing skin irritations with some people or being texturally unpleasant to the touch.  Wearing polyester became associated with being cheap and this connection has continued to affect how consumers perceive the product. This drove more innovation in the industry as manufacturers began to hide or reliable polyester in new blended fabrics.  The properties of polyester fabrics include: inexpensive cost; superior strength and resilience; lightweight; hydrophobic (it feels dry or moves moisture effects away from touch); it has an unusually high melting point; is resistant to dyes, solvents and most chemicals; stain resistant; resists stretching and shrinking; quick drying; wrinkle, mildew and abrasion resistant; retains heat-set pleats and creases and is easy to launder III MATERIALS 3.1 CHICKEN FEATHER FIBER STRUCTURE OF CHICKEN FEATHER Figure 3.1 Structure of a contour feather
  • 4. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 96 | P a g e Figure 3.2 Down feathers are smaller than contour feathers and lack barbules and the accompanying hooklets. They are soft and fluffy, located beneath the contour feathers. They provide most of a chicken's insulation. There are several subcategories of down, including natal down, present only at hatching, and powder down, which is a specialized feather type that sheds a fine, white keratin powder. The waxy powder is composed of granules so small that it is unwettable and thus forms a waterproof barrier for contour feathers(Figure 3.1 & Figure 3.2). The semi plume is a feather type that mediates between the categories of contour and down. Semi plumes share characteristics with both; they have a large rachis and predominantly downy vanes. Filoplumes are smaller than semi plumes, with only a few barbs at the tip of a fine shaft. These likely serve a sensory function in chickens, registering vibrations and changes in pressure. The smallest type of feather is the bristle, which is stiff and has few, if any, short barbs near the tip. Bristles are protective in function and are found on a chicken's head, at the base of the beak, around the eyes, and covering the nostrils. While older and larger chickens would be expected to have relatively more contour feathers. (Figure.3.3 & Figure 3.4) 3.2 PICTURE OF CHICKEN FEATHER Figure 3.3 Picture Of Chicken Feather In order to maximize the yield of a desirable type of feathers, feather collection could be Planned for days on which chickens of a particular feather type distribution are processed. Each contour feather has a feather shaft and a flat vane extending from it .The naked portion of the shaft that is implanted in a bird's skin is the calm‟s. The portion bearing branches is the rachis, which is filled with a porous substance termed the medulla. Branches are termed barbs and provide an axis from which barbules can branch. Barbules are very closely spaced and interlock via hook lets, or barbicels, in order to provide strength and repel water. Flightless birds, including the emu and the ostrich, have few, if any, hook lets .Thus, it can be assumed that hook lets are not abundant in chickens. 3.3 PRIMARY TYPES OF CHICKEN FEATHER Figure 3.4The five primary types of chicken feathers (a) contour (b) bristle, (c) semiplume, (d) down, (e) filoplume 3.4 PROCESSED CHICKEN FEATHER FRACTIONS Large contour feathers are approximately half feather fiber and half quill by mass These are useful categories because several companies‟ proprietary processing technologies yield these two fractions, fiber and quill, shown in. Also, that fiber keratin and quill keratin are characteristic of the two forms of microcrystalline keratin in feathers. In simple terms, the quill is the hard. Central axis off which soft, interlocking fibers. The fibers are hollow Smaller feathers have a greater proportion of fiber, which has a higher aspect ratio than the quill as is apparent in single keratin fiber has a maximum diameter of 50 μm . Quill fractions are composed of both inner and outer quill; outer quill is more densely structured than inner quill, which is porous, as is apparent in have reported that the presence of quill among fibers results in a more granular, lightweight and bulky material. A typical quill has dimensions on the order of centimeters (length) by millimeters (diameter).
  • 5. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 97 | P a g e 3.5 CROSS SECTION VIEW OF CHICKEN FEATHER Figure 3.5 Cross Section View Of Chicken Feather 3.6 CONSTITUTION OF CHICKEN FEATHER  Serine -16%  Proline -12%  Glycine -11%  Valine -9%  Cysteine-7% And the rest are numerous amino acids in small percentages Chicken feather is treated as a waste product from the poultry sector, approximately „2*1013 kg of chicken feather generated in India every year.The cross section and the longitudinal features of the different region of the rachis and the Barbs. Hence, the ESEM micrographs of the barbs showed a tertiary structure, i.e. the barbules that are attached to the barbs in a manner similar to the barbs being attached to the rachis. Thus, according to the ESEM micrographs, a feather is composed of four units, i.e. the calm‟s, the rachis the barbs and the barbules. Show the morphological features of the main units of the poultry feather shows the two principal units, namely the rachis and the barbs shows the secondary and the tertiary units, namely the barbs and the barbules. The barbules are attached to the barbs in a manner similar to the barbs being attached to the rachis shows the primary, the secondary and the tertiary units. 3.7 PREPARATION OF CHICKEN FEATHER Figure 3.6 Raw Poultry Feather Figure 3.7 Water Treatment The concentration of the chemical solutions is function of nature and the desired product. Hence, according to the application, the poultry feathers may be converted to useful products in the form of powder, fiber or wool. In combination with a suitable resin, the aforementioned natural fibres can be turned in to NF Composites. The resin is applied as a liquid and turns solid upon drying. Whereas the fibres add strength to the composite, the resin must at least have the following characteristics: Figure 3.8 Wool Product
  • 6. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 98 | P a g e  Good impregnation To allow all the different fibres to act as a single material, even the smallest fibres have to be „glued‟ together by the resin. The better the impregnation the higher the load a Composite can carry.  Control moisture content of the natural fibres After processing, the natural fibres still contain a significant amount of water. The strength of the fibre is highest at a certain percentage of moist. Therefore the fibre must neither be too dry or too moist. The resin must allow evaporation of superfluous moist before it forms an impermeable solid film.  Non-toxic Since in most of the rural societies health regulations at the work-floor are absent,Application of toxic materials will be an act of violence.  High availability usually a higher availability results in a reduction of material costs. 3.8 SAMPLE PREPARATION IN POLYESTER Table-3.1 Sample Preparation In Polyester POLY ESTER (in gms) FIBER (Chicken Feather) (in gms) TOTAL (in gms) STRIP PREPARATIO N FINDING PROPERTIES 80 20 100 BIE- DIRECTION Tensile Compressive Flexural Rigidity 70 30 100 UNI- DIRECTION Tensile Compressive60 40 100 Flexural Rigidity 3.9 SAMPLE PREPARATION IN PHENYL ESTER Table-3.2 Sample Preparation In Phenyl Ester POLY ESTER (in gms) FIBER (Chicken Feather) (in gms) TOTAL (in gms) STRIP PREPARATIO N FINDING PROPERTIES 80 20 100 BIE- DIRECTION Tensile Compressive Flexural Rigidity 70 30 100 UNI- DIRECTION Tensile Compressive60 40 100 Flexural Rigidity 3.10 RESIN PREPARATION Figure 3.9 Wool Product The matrix material is a general purpose unsaturated polyester resin available from “FIBER CHEM PRODUCTS” In Salem. Due to the fact that the keratin feather fibers are characterized by a very short and classified as a fibers, and they were washed by using a lab dyeing machine with a polar solvent (ethanol). After the washing process the chicken features were rinsed and left to dry for 24 hours under normal room temperatures. The highly filled composites are prepared by a new technique developed. The concentration range was varied from 10%to 30% mixing of feathers because of practical reasons 3.11METHODS 3.11.1 Hand lay-up Prior to the composite manufacturing, the CFF samples were conditioned for 48 hours at the fibre linear density values were determined in accordance with ASTM and the tensile properties of the fibres were determined in accordance with ASTM. The composites were fabricated with different fibre loadings (10%, 20% and 30%). Initially, polyester resin was mixed in hardener using a mixer in a bowl after the phenyl ester, polyester, resin was also prepared separately. The matrix materials were prepared in a portion of 70% of resin matrix and 30% of hardener by volume. Then, the fibres were spread into mould and covered with the matrix. The composites were manufactured by using a hand lay-up technique with size mould of 210 mm length x 210 mm width x 10 mm thickness. The composites were kept for 24 hours at room temperature and subsequently put in an oven for 8
  • 7. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 99 | P a g e hours at 80°C for curing. The control and the CFF reinforced composites were evaluated in accordance with ASTM size. 3.12 MOULD PREPATATION Dimension of the cavity :l x b x t = 200mm x 150mm x10mm. Figure :3-10 Source Of Feathers Fig:3-11 Source Of Feathers Feathers collected at the Gold Kist chicken processing facility had been removed from chickens by hot water and mechanically driven rubber fingers and then diverted from the plant in a trough of water. The feathers were collected by hand from a conveyor belt carrying waste – chicken heads, feet, and feathers – to an offal truck. The feathers were transported on ice and then frozen, because feather masses which are commingled with chicken parts, water, and fats decompose in a biological process that is accelerated at high temperatures. The feathers were later cleaned in a washing machine with approximately 7 L of anti- microbial soap per m 3 of feathers and then dried in a rotary drier. Figure 3.10 & Figure 3.11 shows the source of feathers and processing information. Processing involves grinding the feathers and separating them into fiber and quill fractions. All examined quill fractions were composed of both inner and outer quill. Details on how the feathers are processed are generally difficult to ascertain, as many of the processing techniques are proprietary. Sample B was cut by hand at Georgia Tech into fiber and quill fractions. The fiber fraction was then chopped with a household coffee grinder until each fiber was separated. 3.13 STRIP PREPARATION Figure 3.12 Strip Preparation Figure 3.12 Strip Preparation Dimensions: Tensile Test : l x b x t = 150mm x 25mm x 10mm. Flexural Test : l x b x t = 150mm x 25mm x 10mm Impact Test : l x b x t =150mm x 10mm x 10mm As materials suppliers, very little training is required since this segment is already well Developed. The only required training might be to produce spun yarns with a variety in thicknesses and fabrics with
  • 8. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 100 | P a g e different weave patterns. It is also important that as sale of composites increases, local farmers are persuaded to increase fibre production to meet the demand. A point of attention is the fact that today the natural fibres and the related processes are optimized to produce an optimum fibre for textile applications. For natural fibres for composite applications, a different variety of fibres and different way of processing might be more suitable. 3.14 WORK PIECE WITH TESTING FIGURE Figure 3.13 Strip Preparation and Testing The development of successful applications for CFM will be aided by an understanding of their mechanical properties. Selecting compatible matrix materials for CFM will specifically require an understanding of the Young‟s module chicken feather fractions. IV RESULT AND DISCUSSION It can be seen that CFF reinforced composite will have potential applications due to its improved the behaviour, the tensile and flexural properties can be enhanced with the increasing percentage of CFF and also different resin. Another way to enhance the composite properties is to determine an effective treatment to eliminate lack of adhesion between matrix and CFF fiber. 4.1 TENSILE TEST PERFORMENCE The details of Tensile Test of composite for varies percentage of CFF with Phenyl Ester and Polyester mixtures as follows: 4.1.1 COMPARISION OF TENSILE TEST : Composites Cross Sectional Area [mm2 ] Peak Load (in N) % Elongation UTS [N/mm 2 ] 10 CFF- 90% Phenyl Ester 275 401.778 1.440 1.462 20 CFF -80% Phenyl ester 250 461.482 3.380 1.844 30 CFF -70% Phenyl ester 300 268.353 1.560 0.893 10 CFF - 90% Polyester 200 538.020 1.480 2.688 20 CFF - 80% Polyester 200 943.732 2.780 4.719 30 CFF -70% Polyester 250 228.867 0.980 0.912 x-axis : composites in % y-axis : Tensile Stress [N/mm2 ] 4.1.2 Graph for Tensile Test Composite Material : 10%CFF & 90%Phenylester. 0 1 2 3 4 5 UTS
  • 9. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 101 | P a g e Composite Material : 20%CFF & 80%Phenylester. Composite Material: 30%CFF & 70%Phenylester. Composite Material : 10%CFF & 90%Polyester. Composite Material: 20%CFF & 80%Polyester. Composite Material : 30%CFF & 70%Polyester. 4.2.BENDING TEST PERFORMANCE The details of flexural Test of composite for varies percentage of CFF with Phenyl Ester and Polyester mixtures as follows: 4.2.1 COMPARISION OF BENDING TEST: Composites Cross Sectional Area [mm2 ] Peak Load [N] Flexural Strength (Mpa) Flex ural Mod ulas Gpa ) 10 CFF- 90% Phenyl Ester 156 214.849 10.846 5.84 9 20 CFF - 80% Phenyl ester 104 114.228 12.974 17.7 65 30 CFF - 70% Phenyl ester 156 265.380 13.391 5.90 8 10 CFF - 90% Polyester 104 96.825 10.997 13.8 25 20 CFF - 80% Polyester 104 139.292 15.821 14.5 20 30 CFF - 70% Polyester 130 175.736 12.775 8.74 9
  • 10. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 102 | P a g e x-axis : Composites in % y-axis : Flexural Strength(Mpa) 4.2.2 Graph for Flexural Test Composite Material : 10%CFF & 90%Phenylester Composite Material : 20%CFF & 80% Phenylester. Composite Material : 30%CFF & 70%Phenylester. Composite Material : 10%CFF & 90% Polyester. Composite Material : 20%CFF & 80%Polyester. Composite Material : 30%CFF & 70%Polyester.. 4.3 IMPACT TEST WhWhen the Impact resistance decreases with an increase n in the modulus of elasticity, which means that stiffer mamaterials will have less impact resistance. Resilient mamaterials will have better impact resistance. The details of of Impact Test of composite for varies percentage of CF CFF with Phenyl Ester and Polyester mixtures as follfollows: 0 5 10 15 20 Flexural Strength(Mp a)
  • 11. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 103 | P a g e Figure 4.3 Broken Workpiece After The Test 4.3.1 COMPARISION OF IMPACT TEST: Sl.No Sample Composites Impact value for given sample in J 1. 10 CFF - 90%Phenylester 0.35 2. 20 CFF - 80%Phenylester 0.35 3. 30 CFF - 70%Phenylester 0.30 4. 10 CFF -90%Polyester 0.25 5. 20 CFF -80%Polyester 0.40 6. 30 CFF -70%Polyester 0.25 x-axis : Composites in % y-axis : Impact Value in Joule. V CONCLUSIONS Usually the poultry waste are still destroyed by using either burning or burying methods This studies helps that the poultry waste can be utilised and used any engineering applications and it will be preferred due to low cost and superior characteristics and the most importantly it is ecological and health problems. The investigation shows that 20 % CFF and 80% Polyester having highly superior properties such as tensile, flexural and impact value The tensile and flexural property values decrease when the fibre loading percentages increases. Thus, the reinforced composite better than at 5% level and the Tensile and flexural properties of composite are control with the resins Polyester having significantly superior properties to the 25% CFF reinforced composite. The CFF reinforced composite have potential applications based on the mixer of varies different resin and CFF fiber due to improving its behaviour. The tensile and flexural properties can be enhanced with the increasing the percentage of CFF and also with different resin are considered to eliminate lack of adhesion between matrix and CFF fibre. REFERENCES [1]. A.L. Martı´nez-Herna´ndez, C. Velasco- Santos, M. de-Icaza, Victor M. Castan.O, Dynamical–mechanical and thermal analysis of polymeric composites reinforced with keratin biofibers from chicken feathers, Composites: Part B 38 (2007) 405–410 [2]. Saira Taj, Munawar Ali Munawar, and Shafi ullah Khan “Natural Fiber-Reinforced Polymer Composites , Proc. Pakistan Acad. Sci. 44(2):129-144.2007 [3]. D.Verma1, P.C.Gope, A.Shandilya, A.Gupta, M.K.Maheshwari, “ Coir Fibre Reinforcement and Application in Polymer Composites: A Review” J. Mater. Environ. Sci. 4 (2) (2013) 263-276, ISSN: 2028-2508, CODEN: JMESCN [4]. Wrześniewska-tosik K., Marcinkowska M., Niekraszewicz A., Potocka D. A., Mik Pałczyńska M. “Fibrous Composites Based on Keratin from Chicken Feathers” Fibres & Textiles in Eastern Europe 2011, vol. 19, no. 6 (89) pp. 118-123. [5]. Jyoti Prakash Dhal and S. C. Mishra “Processing and Properties of Natural Fiber- Reinforced Polymer Composite” Hindawi Publishing Corporation, Journal of Materials, Volume 2013, Article ID 297213, 6 pages 24 November 2012 [6]. Oladele I. O, Omotoyimbo J. A, Ayemidejor S. H. “ Mechanical Properties of Chicken Feather and Cow Hair Fibre Reinforced High Density Polyethylene Composites” International Journal of Science and Technology Volume 3 No. 1, January, 2014, PP 66-72 [7]. Jerrold E. Winandy James H. Muehl Jessie A. Glaeser Walter Schmidt, “ Chicken Feather Fiber as an Additive in MDF Composites” Journal of Natural Fibers, Vol. 4(1) 2007, PP 35 -48 0 0.2 0.4 0.6 Impact Value in J
  • 12. T. Subramani et al. Int. Journal of Engineering Research and Applications www.ijera.com ISSN : 2248-9622, Vol. 4, Issue 12( Part 4), December 2014, pp.93-104 www.ijera.com 104 | P a g e [8]. Dr. Shajan Kuriakose, Dr. Deviprasad Varma, Vaisakh V.G “ Mechanical Behaviour of Coir reinforced Polyster Composites–An Experimental Investigation” IJETAE, ISSN 2250-2459, ISO 9001:2008, (Volume 2, Issue 12, December 2012) , PP 751-747 [9]. C.Mahesh, B.Kondapanaidu, K.Govindarajulu, and V.Balakrishna murthy, “Experimental Investigation of Thermal and Mechanical Properties ofPalmyra Fiber Reinforced Polyster Composites With and Without Chemical Treatment and Also Addition of Chalk Powder” IJETT – Volume 5 Number 5 - Nov 2013, ISSN: 2231-5381, PP 259 -271 [10]. K B jagadeeshgouda, P Ravinder Reddy, K ishwaraprasad “Experimental Study Of Behaviour Of Poultry Feather Fiber - A Reinforcing Material For Composites” IJRET: (EISSN: 2319-1163 | PISSN: 2321- 7308) VOLUME: 03 ISSUE: 02 | Feb- 2014,PP 362-371 [11]. D. Chandramohan & .K. Marimuthu, “ A Review On Natural Fibers” Volumes/ Vol 8, Issue2 / IJRRAS 8 (2) August 2011, PP 194-206. [12]. V. Ananda Rao, Alok Satapathy, S.C. Mishra, “ Polymer composites reinforced with short fibers obtained from poultry feathers” Proceedings of International and INCCOM-6 Conference, Future Trends in Composite Materials and Processing, December 12-14, 2007, Indian Institute of Technology Kanpur [13]. Anthony N. Anyakora, “Investigation of Mechanical Properties of Polyester Matrix Reinforced with Coconut Palm Frond Fiber for the Production of Low Strength Building Products” IJMSE, Vol. 3, NO. 10, October 2012, [ISSN: 2045-7057] PP 1-6 [14]. Ahmed Salhi, Salah Kaci1, A.Boudene and Y. Candau, “Development of Biocomposites Based of Polymer Metrix and Keratin Fibers:Contribution to Poultry FEATHER biomass Recycling. Part-i” Conference and Training School Multiphase Polymer and Composite Systems: From nanoscale to Macro Composites: June 7-10, 2011 Paris – Est, France, PP 1-4. [15]. S. C. Mishra and Nadiya Bihary Nayak, “An Investigation of Dielectric Properties of Chicken Feather Reinforced Epoxy Matrix Composite” JRPC, Vol. 0, No. 00/2010, Jan 28, 2010, PP 1-7. [16]. Menandro N. Acda, “Waste Chicken Feather as Reinforcement in Cement-Bonded Composites” Philippine Journal of Science, 139 (2): 161-166, December 2010, ISSN 0031 – 7683, PP 161-166 [17]. Yun-Xian Wang, Xue-Jun Cao “Extracting keratin from chicken feathers by using a hydrophobic ionic liquid” Process Biochemistry 47 (2012) PP 896-899. [18]. A S Singha* And Vijay Kumar Thakur, “Mechanical properties of natural fibre reinforced polymer composites” Bull. Mater. Sci., Vol. 31, No. 5, October 2008, pp. 791–799. © Indian Academy of Science [19]. M.Omakupt. Soil erosion mapping using Remote Sensing data and Geographic Information System, URL: http://www.gisdevelopment.netAsian GIS journal. (1989) [20]. Subramani, T. “Experimental Investigations on Coir Fibre Reinforced Bituminous Mixes” International Journal of Engineering Research and Applications, Vol.2, Issue.3, pp 1794-1804, 2012.