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Shrinkage Behavior of Ultra High Performance
     Concrete at the Manufacturing Stage


               Sungwook KIM
CONTENT


      Introduction

      Mix Proportion & Material Properties

      Test Results

      On Going Study

      Conclusion

                        2
1. Introduction (Problems)


                          Drying shrinkage

                                                                 Edge



                    Autogenous shrinkage
                                                 Steel reinforcement




         Typical Shrinkage Strains of UHPC



                               Shrinkage
                                cracking




 “Highly vulnerable to premature shrinkage cracking”
                                             3
※ What are the influencing factors for shrinkage cracking?


             “Influencing factors”
                                       Elastic stress generated
                                       by shrinkage only
                                             ε
                                       (σ=EC· sh)
                                                                         • Strength test
          Material
          strength
 Stress




                           Creep relaxation
                                              Residual stress
                                              regarding stress
                                              relaxation
                                                                         • Setting test
                                       Age of cracking

             Delay in cracking

                                              Time                         • Ring-test
 “by J. Weiss, 1999”


 Shrinkage            Tensile       Shrinkage         Tensile
                                                                      • Free shrinkage test
 potential             creep          rate           strength




                                                                  4
2. Mix Proportions and Material Properties

                                                                                                                         *   : Shrinkage reducing agent
  Mix Proportions (ratio in weight)                                                                                      **   : Expansive admixture
                                          Silica Fume                                        Superplasticizer                                   Steel
 Nomenclature       W/B     Cement                            Filler         Sand                                 SRA*             EA**
                                              (SF)                                                (SP)                                          fiber
     Mix. A                                                                                                         -                -
                    0.2          1.0            0.25           0.3               1.1               0.012                                        Vf=2%
     Mix. B                                                                                                        0.01            0.075



  Properties of Steel Fiber                                                                                     Relative Humidity & Temp.

                     Density       Tensile strength        Length of fiber             Aspect ratio               Relative                 Temperature
  Type of fiber
                    (kg/cm3)           (MPa)                   (mm)                     (mm/mm)                 Humidity (RH)                 (℃)
  Straight type       7.8               2,500                      13                         65                   60±5%                        23±1℃



  Chemical Compositions of Materials

 Composition %                                                                                             Specific surface         Density
                    CaO     Al2O3      SiO2      Fe2O3       MgO            SO3        K2O         F-CaO
    (mass)                                                                                                     (cm2/g)              (g/cm3)
     Cement         61.33      6.40    21.01      3.12        3.02          2.30         -           -           3,413                   3.15
 Silica fume (SF)   0.38       0.25    96.00      0.12        0.10           -           -           -          200,000                  2.10
       EA           13.55      18.66    3.80           -       -        51.35          0.56        16.02         3,117                   2.98



                                                                        5
3. Test Results (Mechanical Properties)

    Compressive strength                                Flexural tensile strength                                    Secant elastic modulus
                                    fc        a                                      f ft         a                                           Ec          a 
                                         exp                                                exp                                                    exp     
                                   f 28      bt                                     f 28        bt                                          Ec 28       bt 




    Mixture         a          b           R2           Mixture     a           b               R2                   Mixture      a           b           R2
    Mix. A      0.971     -0.271       0.9842            Mix. A   0.303       -0.058          0.9916                 Mix. A     0.389        0.001       0.9948
    Mix. B      1.162     -0.326       0.9862            Mix. B   0.456       -0.101          0.9732                 Mix. B     0.381        0.001       0.9986


                               Compressive strength                      Flexural tensile strength                             Secant elastic modulus
             Flow                    (MPa)                                        (MPa)                                                (GPa)
Mixture
             (mm)
                        1day       3days        7days   28days    1day        3days            7days        28days      1day      3days           7days      28days
Mix. A        235       78.8       105.6        126.2   152.4     26.3         28.7             33.8         34.1       28.2          40.3        41.2         43.3
Mix. B        240       70.7       98.7         127.3   152.2     24.1         25.1             32.5         33.4       30.9          41.1        44.6         46.0

                                                                          6
3. Test Results (Setting properties)

  Setting properties of UHPC (ASTM C 403)


               Final setting



               Initial setting




               ● Mix.A                                   Log ( PR)  b  a  Log (t )       (1)
               ◆ Mix.B
                                                         where, PR=penetration resistance (psi)
                                                                t=elapsed time (min)


                                                                    ※I.S.: PR=3.5MPa, F.S.: PR=28MPa

    Mixture       a                b             R2          Initial Setting (hr)   Final Setting (hr)

    Mix. A     5.1483            11.0284       0.99507               11.0                 13.5
    Mix. B     8.3353            20.6517       0.99519               7.5                  11.5

                                           7
3. Test Results (Autogenous Shrinkage)

     Relationship between Autogenous shrinkage and Setting time

     Thermocouple



            Embedded
              Strain
              gage




                                                                                           Plastic
                                                                                           Shrinkage
                                                                                           Reduction




                                                  where, εauto(t) = autogenous shrinkage (με)
 auto(t )   total (t )   plastic(t )   (2)         εtotal(t) = total shrinkage except drying shrinkage (με)
                                                        εtotal(t) = plastic shrinkage (με)
                                                        8
3. Test Results (Free Shrinkage)

  Free shrinkage with different exposed surface-to-volume ratios (S/Vs)

       Thermocouple



              Embedded
                Strain
                gage




                                                                                  550mm
                                                                   152mm          246mm
                                                                                  550mm             152mm
                                                                   152mm          246mm             152mm
                 Volume                                 35mm
                                                                   Sealing   Exposed concrete       Sealing
                                                      35mm
                 expansion
                                                                   Sealing   Exposed concrete       Sealing
                                                                               S/V=0.0286
                                                                                  550mm
                                                                   165mm          550mm
                                                                                  220mm            165mm
                                                                   165mm          220mm            165mm
                      Combined effect of SRA and EA
                                                        76mm




                                           ≈ 40~44%
                                                                   Sealing   Exposed concrete       Sealing
                                                      76mm




                                                                   Sealing   Exposed concrete       Sealing


                                                                               S/V=0.0132

                                                                                          “by H. T. See, 2003”

                                                               9
3. Test Results (Test procedure: Ring-test (AASHTO PP34-98))
                                                                                                  Teflon sheet

                   Wooden base                      Outer ring         Wooden base                   Outer ring




                                 Inner steel ring                                     Inner steel ring




                                             Teflon sheet                                          Teflon sheet

                  Wooden base                   Outer ring             Wooden base                    Outer ring

                                                        Thermocouple                                        Thermocouple



                                 Inner steel ring                                     Inner steel ring




“Data Logger system”
                  Strain gages                                         Strain gages


                                                                 10
3. Test Results (Ring-test)
                                                                                  Strain gage

  Temperature compensation of inner steel ring


                                                                                 Thermocouple



                                                                            “Coefficient
                                                                            of Thermal
                                                                             Expansion
                                                                             =16με/℃”




         st (t )   m (t )  C  t   (3)

        where, εst(t) = actual steel strain by shrinkage of concrete (με)
              εm(t) = measured steel strain (με)
              C = coefficient of thermal expansion of steel ring (16με/℃)
              Δt = time (hours)

                                                    11
3. Test Results (Ring-test)
                                                                              Drying direction
  Average strains of inner steel ring
                                                                   Silicon                          Steel ring
                                                                   sealing
                      A - R1                                                     Steel gage
                                                                 Concrete                            152mm

  • Type of Mixture               • Thickness of concrete ring                      267mm
   A: Mix. A                       R1: 35mm                                         305mm
   B: Mix. B                       R2: 76mm                                  R1=375mm or R2=457mm




                       “Mix. A”                                     “Mix. B”



                                                                                                    34%

                                                                                              48%




                                         12
3. Test Results (Restrained Shrinkage Behaviors)

  Calculated maximum pressures and tensile stresses


    Maximum interface pressures                 Maximum residual tensile stresses
    by Eq. (4)                                  by Eq. (5)

             (ros  ris )
                2     2
                                                                     (ros  ris ) (ric  roc )
                                                                        2     2      2     2

        Pi               Est  st   (4)         t max                                       Est  st        (5)
                   2
                2ros                                                    2ros (roc  ric )
                                                                           2         2     2



                                                              40
                                                                         Mix.A            Mix.B
                                                                            Mix. A         Mix. B
                                                              35         계열7              계열8

                                                              30                                     Stresses generated
                                                                                                     by shrinkage only




                                                Stess (MPa)
                                                              25                                     (σ=EC·εsh)

                                                              20                          Relaxed stresses

                                                              15

                                                              10

                                                               5
                                                                                                         Residual stresses
                                                                                                         considering stress
                                                               0
                                                                                                         relaxation
                                                                   0    4        8   12     16      20    24     28
                                                                                     Age (day)
                                           13
3. Test Results (Restrained Shrinkage Behaviors)

  Tensile creep strains of UHPC with time dependent restrained forces


    Tensile creep strains of UHPC            Tensile creep strains-to-free shrinkage ratio
    under restrained condition               of UHPC under restrained condition




                                ≈ 39%
                                                                                      ≈ 0.46




                                        14
4. On Going Study (Tensile Test at very early Age)

   Carrying out tensile test within 1 days after mixing


      Strain of steel ring occurs           Tensile tests are carrying in order to
      before initial setting time           estimate crack at very early age




                                                                         “by Dao, 2009”




                                       15
4. Concluding Remarks

         This study investigated experimentally the shrinkage behavior
         and the corresponding stresses in UHPC for the control of cracks
    1    due to the restraint of forms at early age

         Free shrinkage and restrained steel strains were reduced in terms of
    2    the shrinkage reducing effect of EA and SRA

         Ring tests also verified the possibility to compute the confining
         tensile stress and strain according to the shrinkage of UHPC at
    3    very early age

         Further studies will investigate solutions enabling to get tensile
         strength at very early age and simulate the cross-sectional
         stiffness and restraint of the form, and verify these solutions
    4    experimentally

                                      16
Thank you for
your attention




             17

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Shrinkage Behavior and Properties of Ultra High Performance Concrete at Early Ages

  • 1. Shrinkage Behavior of Ultra High Performance Concrete at the Manufacturing Stage Sungwook KIM
  • 2. CONTENT Introduction Mix Proportion & Material Properties Test Results On Going Study Conclusion 2
  • 3. 1. Introduction (Problems) Drying shrinkage Edge Autogenous shrinkage Steel reinforcement Typical Shrinkage Strains of UHPC Shrinkage cracking “Highly vulnerable to premature shrinkage cracking” 3
  • 4. ※ What are the influencing factors for shrinkage cracking? “Influencing factors” Elastic stress generated by shrinkage only ε (σ=EC· sh) • Strength test Material strength Stress Creep relaxation Residual stress regarding stress relaxation • Setting test Age of cracking Delay in cracking Time • Ring-test “by J. Weiss, 1999” Shrinkage Tensile Shrinkage Tensile • Free shrinkage test potential creep rate strength 4
  • 5. 2. Mix Proportions and Material Properties * : Shrinkage reducing agent Mix Proportions (ratio in weight) ** : Expansive admixture Silica Fume Superplasticizer Steel Nomenclature W/B Cement Filler Sand SRA* EA** (SF) (SP) fiber Mix. A - - 0.2 1.0 0.25 0.3 1.1 0.012 Vf=2% Mix. B 0.01 0.075 Properties of Steel Fiber Relative Humidity & Temp. Density Tensile strength Length of fiber Aspect ratio Relative Temperature Type of fiber (kg/cm3) (MPa) (mm) (mm/mm) Humidity (RH) (℃) Straight type 7.8 2,500 13 65 60±5% 23±1℃ Chemical Compositions of Materials Composition % Specific surface Density CaO Al2O3 SiO2 Fe2O3 MgO SO3 K2O F-CaO (mass) (cm2/g) (g/cm3) Cement 61.33 6.40 21.01 3.12 3.02 2.30 - - 3,413 3.15 Silica fume (SF) 0.38 0.25 96.00 0.12 0.10 - - - 200,000 2.10 EA 13.55 18.66 3.80 - - 51.35 0.56 16.02 3,117 2.98 5
  • 6. 3. Test Results (Mechanical Properties) Compressive strength Flexural tensile strength Secant elastic modulus fc  a  f ft  a  Ec  a   exp   exp   exp  f 28 bt  f 28 bt  Ec 28  bt  Mixture a b R2 Mixture a b R2 Mixture a b R2 Mix. A 0.971 -0.271 0.9842 Mix. A 0.303 -0.058 0.9916 Mix. A 0.389 0.001 0.9948 Mix. B 1.162 -0.326 0.9862 Mix. B 0.456 -0.101 0.9732 Mix. B 0.381 0.001 0.9986 Compressive strength Flexural tensile strength Secant elastic modulus Flow (MPa) (MPa) (GPa) Mixture (mm) 1day 3days 7days 28days 1day 3days 7days 28days 1day 3days 7days 28days Mix. A 235 78.8 105.6 126.2 152.4 26.3 28.7 33.8 34.1 28.2 40.3 41.2 43.3 Mix. B 240 70.7 98.7 127.3 152.2 24.1 25.1 32.5 33.4 30.9 41.1 44.6 46.0 6
  • 7. 3. Test Results (Setting properties) Setting properties of UHPC (ASTM C 403) Final setting Initial setting ● Mix.A Log ( PR)  b  a  Log (t ) (1) ◆ Mix.B where, PR=penetration resistance (psi) t=elapsed time (min) ※I.S.: PR=3.5MPa, F.S.: PR=28MPa Mixture a b R2 Initial Setting (hr) Final Setting (hr) Mix. A 5.1483 11.0284 0.99507 11.0 13.5 Mix. B 8.3353 20.6517 0.99519 7.5 11.5 7
  • 8. 3. Test Results (Autogenous Shrinkage) Relationship between Autogenous shrinkage and Setting time Thermocouple Embedded Strain gage Plastic Shrinkage Reduction where, εauto(t) = autogenous shrinkage (με)  auto(t )   total (t )   plastic(t ) (2) εtotal(t) = total shrinkage except drying shrinkage (με) εtotal(t) = plastic shrinkage (με) 8
  • 9. 3. Test Results (Free Shrinkage) Free shrinkage with different exposed surface-to-volume ratios (S/Vs) Thermocouple Embedded Strain gage 550mm 152mm 246mm 550mm 152mm 152mm 246mm 152mm Volume 35mm Sealing Exposed concrete Sealing 35mm expansion Sealing Exposed concrete Sealing S/V=0.0286 550mm 165mm 550mm 220mm 165mm 165mm 220mm 165mm Combined effect of SRA and EA 76mm ≈ 40~44% Sealing Exposed concrete Sealing 76mm Sealing Exposed concrete Sealing S/V=0.0132 “by H. T. See, 2003” 9
  • 10. 3. Test Results (Test procedure: Ring-test (AASHTO PP34-98)) Teflon sheet Wooden base Outer ring Wooden base Outer ring Inner steel ring Inner steel ring Teflon sheet Teflon sheet Wooden base Outer ring Wooden base Outer ring Thermocouple Thermocouple Inner steel ring Inner steel ring “Data Logger system” Strain gages Strain gages 10
  • 11. 3. Test Results (Ring-test) Strain gage Temperature compensation of inner steel ring Thermocouple “Coefficient of Thermal Expansion =16με/℃”  st (t )   m (t )  C  t (3) where, εst(t) = actual steel strain by shrinkage of concrete (με) εm(t) = measured steel strain (με) C = coefficient of thermal expansion of steel ring (16με/℃) Δt = time (hours) 11
  • 12. 3. Test Results (Ring-test) Drying direction Average strains of inner steel ring Silicon Steel ring sealing A - R1 Steel gage Concrete 152mm • Type of Mixture • Thickness of concrete ring 267mm A: Mix. A R1: 35mm 305mm B: Mix. B R2: 76mm R1=375mm or R2=457mm “Mix. A” “Mix. B” 34% 48% 12
  • 13. 3. Test Results (Restrained Shrinkage Behaviors) Calculated maximum pressures and tensile stresses Maximum interface pressures Maximum residual tensile stresses by Eq. (4) by Eq. (5) (ros  ris ) 2 2 (ros  ris ) (ric  roc ) 2 2 2 2 Pi  Est  st (4)  t max  Est  st (5) 2 2ros 2ros (roc  ric ) 2 2 2 40 Mix.A Mix.B Mix. A Mix. B 35 계열7 계열8 30 Stresses generated by shrinkage only Stess (MPa) 25 (σ=EC·εsh) 20 Relaxed stresses 15 10 5 Residual stresses considering stress 0 relaxation 0 4 8 12 16 20 24 28 Age (day) 13
  • 14. 3. Test Results (Restrained Shrinkage Behaviors) Tensile creep strains of UHPC with time dependent restrained forces Tensile creep strains of UHPC Tensile creep strains-to-free shrinkage ratio under restrained condition of UHPC under restrained condition ≈ 39% ≈ 0.46 14
  • 15. 4. On Going Study (Tensile Test at very early Age) Carrying out tensile test within 1 days after mixing Strain of steel ring occurs Tensile tests are carrying in order to before initial setting time estimate crack at very early age “by Dao, 2009” 15
  • 16. 4. Concluding Remarks This study investigated experimentally the shrinkage behavior and the corresponding stresses in UHPC for the control of cracks 1 due to the restraint of forms at early age Free shrinkage and restrained steel strains were reduced in terms of 2 the shrinkage reducing effect of EA and SRA Ring tests also verified the possibility to compute the confining tensile stress and strain according to the shrinkage of UHPC at 3 very early age Further studies will investigate solutions enabling to get tensile strength at very early age and simulate the cross-sectional stiffness and restraint of the form, and verify these solutions 4 experimentally 16
  • 17. Thank you for your attention 17