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International Journal of Engineering Research and Development
e-ISSN: 2278-067X, p-ISSN: 2278-800X, www.ijerd.com
Volume 6, Issue 5 (March 2013), PP. 80-83

    Cause and Effect Analysis for Reheating the Titanium
        alloys while forging operation- A case study
                          Nice Menachery1, Binoy Boban2, Jino Joy3
     Department of Mechanical Engineering, SCMS School of Engineering and Technology, Kerala, India


    Abstract:- Titanium alloys usually reheated in the electrical furnace during the forging operations, the
    factors for reheating were noted and analyzed with the help of cause and effect diagram. During the
    forging operations, the temperature range usually preferred for the titanium alloy lies between 850°c
    and 930°c. If the temperature of the alloy is decreased, during the preheating stage it should be
    reheated in the electrical furnace, to obtain the forging temperature. The reheating of the titanium alloy
    in the furnace results in more power consumption and time loss which may results in lower profit. In
    this paper the different factors that results the reheating of the titanium alloy, Ti6Al4V while the
    forging operations is identified. The temperature while forging the titanium is recorded using the
    optical pyrometer and the factors for the temperature variation is analyzed using the managerial tool.

    Indexterms:- Titanium alloys, Ti6Al4V, Cause and effect diagram, forging, control charts, 10 Tonne
    hammer

                                       I.         INTRODUCTION
          Titanium and its alloys have attractive engineering properties. They are about 40 percentages lighter
than steel and 60 percentage heavier than aluminium. Titanium alloys have highest strength to weight ratio of
any other metals, roughly 30 percentage greater than aluminium and steel. Other properties of titanium include
high corrosion resistance, low thermal conductivity, high melting point than iron, low coefficient of expansion
and high electrical resistivity. The presence of a thin, tough oxide surface film provide excellent resistance to
atmospheric and organics containing chlorides. Titanium alloys can be classified in to different allotropic phases
such as alpha, beta and alpha-beta alloys. Titanium’s mechanical properties are closely related to these allotropic
phases[1]. At room temperature, it has a closed packed structure, designated as alpha phase. At around 885ºc,
the alpha phase transforms to a body centered cubic structure, known as beta phase, which is stable up to
titanium’s melting point of about 1680ºc.
          Alpha alloys contains elements as aluminium, tin ,chromium, zirconium, vanadium and molybdenum
in amounts varying from about 1 to 10 percent. They are nonheat- treatable, having good stability between 540ºc
and 220ºc. Beta alloys have exceptionally high strengths-over 14085 kg/cm2 having low toughness and low
fatigue strength limits their use. Alpha- Beta Alloys are most widely used group of titanium alloys, having their
behavior falls in a range between the two single- phase alloys. These alloys are heat treatable and formable than
other type of alloys.
          All the titanium forging alloys are double or triple melted, they rarely contain segregations of other
materials that might cause wide variations in forgeability. Initial breakdown forging of titanium alloys can be
done at temperatures above the β transus because the body-centered cubic structure is more ductile and forging
pressure requirements are generally lower. The main contribution of isothermal forging is to eliminate the
influence of die chilling and material strain hardening, as a result number of forging operations and machining
cost can be minimised.[2]
          The present research highlights the main factor that lead to the reheating of the titanium alloy in the
electrical furnace with the help of cause and effect diagram under controlled environment.

                              II.           METHODS AND MATERIALS
        The characterization of the alloy billet was carried out in German made, foundry master spectrometer
connected with Wasag Lab Software is shown in figure 1. It was identified the major constituents of alloy as
6.75% Al and 4.5% V by weight.




                                                 Figure 1: Spectrometer
                                                        80
Cause and Effect Analysis for Reheating the Titanium alloys while forging…

          The billets having a bar stock unit size of 150 mm diameter and 215 mm length, each carrying net
weight of 17.5 kg were heated in electrical furnace for 700°c and soaked for an hour. After the initial soaking at
700°c, the billets were heated to a temperature of 930°c at a rate of 50°c per hour and soak it for 120 minutes.
Heating temperature for the operations should be controlled within narrow limits. Titanium and titanium alloys
must be protected from contamination by oxygen, nitrogen, hydrogen and carbon during heating for the forging
operations Although heating in vacuum or in a suitably inert atmosphere is feasible, this is most effectively done
by coating the forging slugs in a liquid glaze which is allowed to dry before heating for forging. Prolonged
heating should be avoided for all titanium alloys.
          For forging operations the preferred temperature lies between 850°c and 950°c. After proper heating
the billets were transferred in to the hammer for the further processing. The hammer having a capacity of 10
tonne is applied along the alloy surface for creating different shapes.
          While the forging operations the temperature of the alloy may be reduced to below the working
temperature range. Due to the reduction of the temperature the alloys should be reheated in the electrical
furnace, under precisely setting the temperature gradient under controlled environment.
          The forging temperature of titanium alloys is absolutely critical to the process and die heating is
essential, as excessive heat losses through the tooling will produce defective forgings. Despite the protection
offered by the glass coating, a small amount of contamination does occur and must be removed by grinding or
chemical etching. When forging titanium, care should be taken to prevent contact with steel scale. A thermal
type reaction can occur and seriously damage a forging die. Apparently the titanium reduces iron oxide in an
exothermic reaction set off by pressure and high temperature.
          If an unscheduled delay such as a press breakdown occurs, the stocks should be removed from the
furnace, and then it should be reheated when forging is resumed. Particular attention need to be paid throughout
the processing cycle to avoid contamination by oxygen, nitrogen, carbon, and/or hydrogen, which can severely
impair ductility and toughness properties and overall quality of a forged part.

                                     TEMPERATURE                   TEMPERATURE
                             JOB       AFTER 10              JOB     AFTER 10
                             NO         BLOWS                NO       BLOWS
                               1             927             12            863
                               2             920             13            845
                               3             915             14            918
                               4             920             15            915
                               5             908             16            912
                               6             903             17            909
                               7             898             18            904
                               8             901             19            897
                               9             890             20            894
                              10             880             21            887
                              11           885
                                     Table 1: Temperature of the jobs after 10 blows

         The temperature of each of stocks during the forging operations were noted (Table 1). Optical
pyrometer which intercepts the thermal radiation from the alloy were used to measure the temperature of the
billets while the operation.
         The temperature of the alloys may be increased due to the plastic deformation of the stock or the
temperature decreases during the transferring of the stock from furnace to the hammer. [1] The various reasons
for the variation of the temperature and the reheating of the titanium alloys at the electrical furnace during the
operations were identified and their effects were explored in this work. Statistical process control charts are used
to determine temperature variation and fishbone diagram is used to identify the causes and effects of the
increases or decrease in temperature.

                             III.         RESULTS AND DISCUSSIONS
        The forging operations of the Ti6Al4V, titanium alloy having a batch size of 21 was taken in to the
study. During the operations one of the alloy temperature decreases below the minimum range. The average
temperature of each alloy in the batch is calculated after 10 blows and it is represented in a control charts,

                                                        81
Cause and Effect Analysis for Reheating the Titanium alloys while forging…

having an upper control limit of 930°c, lower control limit of 850°C. and mean temperature of 899.57°C and it
is represented in figure 2.




                                   Figure 2: Control chart for the forging temperature

From the figure 2 it is evident that, the temperature of one job ( job no 13) is decreased, which results in the
reheating of that particular job in the electrical furnace. The reheating of the titanium alloy in the electrical
furnace results in increase power consumption, fuels, working hour etc. and if the forging temperature of the
alloy becomes below 850⁰c,changes will happens in the microstructure of alloy, and also in the formation and
filling of the material.
          The different causes for the reheating of the titanium alloy in the electrical furnace includes unskilled
workers, short circuiting of electrical systems, improper die packing, conventional material handling systems,
environmental factors such as presence of salvage, surrounding temperature. These main causes are supported
by some other causes also, which is represented in figure 3.




                                       Figure 3: Cause and effect diagram

                                       IV.          CONCLUSION
          The different causes for the reheating of the titanium alloy during the forging operations were
determined with the help of fishbone diagram.

        Proper training should be given to the workers in order to reduce the no. of blows            during the
         operations and handling of the job.
         The efficiency of the compressor should be calibrated periodically.

                                                        82
Cause and Effect Analysis for Reheating the Titanium alloys while forging…

        Periodically the maintenance operations should be carried out in the hammer. The forging operations
         should be done below the maximum capacity of the hammer.
        Conventional material handling systems should be replaced by conveyors and AGV’s to reduce the
         travelling time between the hammer and the furnace.
        The efficiency of the Plant layout should be tested using Arena software. Inventory and scraps should
         be removed after each operations.
         Application of Kaizen in industry wills results im good performance.
         Operation of the electrical furnace should be done at controlled environment

ACKNOWLEDGMENT
The authors would like to thank all of his colleagues for their support in completing this case study.

                                                REFERENCES
  [1]    Y G Zhou, W.D Zeng, H Q Yu,(2005) “An investigation of a new near-beta forging process for
         titanium alloys and its application in aviation components”, Materials Science and Engineering, vol.
         393, no. 1, pp. 204-212.
  [2]    C.C Chen, J E Coyne (1976), “ Deformation Characteristics of Ti-6Al-4V alloy under Isothermal
         Forging conditions”, metallurgical transactions A, vol 7( A): pg 1931-1940.
  [3]    James D Destefani, ”Properties & selection: Non ferrous alloys and special purpose materials”, ASM
         international,ASM handbook, pages 586-605.
  [4]    Dale H Besterfeild, Glen H Besterfeild, “Total Quality Management”, 2003, pages 205-213.

                                               AUTHORS
First author
 Nice Menachery, graduated in Mechanical Engineering from Calicut University, doing Post Graduate Student
in Production & Industrial Engineering at SCMS School of Engineering and Technology, affiliated to Mahatma
Gandhi University, Kerala, India.

Second author
Binoy Boban, graduated in Mechanical Engineering from Anna University, doing Post Graduate Student in
Production & Industrial Engineering at SCMS School of Engineering and Technology, affiliated to Mahatma
Gandhi University, Kerala, India.

Third author
Jino Joy, graduated in Mechanical Engineering from Anna University, doing Post Graduate Student in
Production & Industrial Engineering at SCMS School of Engineering and Technology, affiliated to Mahatma
Gandhi University, Kerala, India.




                                                        83

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Welcome to International Journal of Engineering Research and Development (IJERD)

  • 1. International Journal of Engineering Research and Development e-ISSN: 2278-067X, p-ISSN: 2278-800X, www.ijerd.com Volume 6, Issue 5 (March 2013), PP. 80-83 Cause and Effect Analysis for Reheating the Titanium alloys while forging operation- A case study Nice Menachery1, Binoy Boban2, Jino Joy3 Department of Mechanical Engineering, SCMS School of Engineering and Technology, Kerala, India Abstract:- Titanium alloys usually reheated in the electrical furnace during the forging operations, the factors for reheating were noted and analyzed with the help of cause and effect diagram. During the forging operations, the temperature range usually preferred for the titanium alloy lies between 850°c and 930°c. If the temperature of the alloy is decreased, during the preheating stage it should be reheated in the electrical furnace, to obtain the forging temperature. The reheating of the titanium alloy in the furnace results in more power consumption and time loss which may results in lower profit. In this paper the different factors that results the reheating of the titanium alloy, Ti6Al4V while the forging operations is identified. The temperature while forging the titanium is recorded using the optical pyrometer and the factors for the temperature variation is analyzed using the managerial tool. Indexterms:- Titanium alloys, Ti6Al4V, Cause and effect diagram, forging, control charts, 10 Tonne hammer I. INTRODUCTION Titanium and its alloys have attractive engineering properties. They are about 40 percentages lighter than steel and 60 percentage heavier than aluminium. Titanium alloys have highest strength to weight ratio of any other metals, roughly 30 percentage greater than aluminium and steel. Other properties of titanium include high corrosion resistance, low thermal conductivity, high melting point than iron, low coefficient of expansion and high electrical resistivity. The presence of a thin, tough oxide surface film provide excellent resistance to atmospheric and organics containing chlorides. Titanium alloys can be classified in to different allotropic phases such as alpha, beta and alpha-beta alloys. Titanium’s mechanical properties are closely related to these allotropic phases[1]. At room temperature, it has a closed packed structure, designated as alpha phase. At around 885ºc, the alpha phase transforms to a body centered cubic structure, known as beta phase, which is stable up to titanium’s melting point of about 1680ºc. Alpha alloys contains elements as aluminium, tin ,chromium, zirconium, vanadium and molybdenum in amounts varying from about 1 to 10 percent. They are nonheat- treatable, having good stability between 540ºc and 220ºc. Beta alloys have exceptionally high strengths-over 14085 kg/cm2 having low toughness and low fatigue strength limits their use. Alpha- Beta Alloys are most widely used group of titanium alloys, having their behavior falls in a range between the two single- phase alloys. These alloys are heat treatable and formable than other type of alloys. All the titanium forging alloys are double or triple melted, they rarely contain segregations of other materials that might cause wide variations in forgeability. Initial breakdown forging of titanium alloys can be done at temperatures above the β transus because the body-centered cubic structure is more ductile and forging pressure requirements are generally lower. The main contribution of isothermal forging is to eliminate the influence of die chilling and material strain hardening, as a result number of forging operations and machining cost can be minimised.[2] The present research highlights the main factor that lead to the reheating of the titanium alloy in the electrical furnace with the help of cause and effect diagram under controlled environment. II. METHODS AND MATERIALS The characterization of the alloy billet was carried out in German made, foundry master spectrometer connected with Wasag Lab Software is shown in figure 1. It was identified the major constituents of alloy as 6.75% Al and 4.5% V by weight. Figure 1: Spectrometer 80
  • 2. Cause and Effect Analysis for Reheating the Titanium alloys while forging… The billets having a bar stock unit size of 150 mm diameter and 215 mm length, each carrying net weight of 17.5 kg were heated in electrical furnace for 700°c and soaked for an hour. After the initial soaking at 700°c, the billets were heated to a temperature of 930°c at a rate of 50°c per hour and soak it for 120 minutes. Heating temperature for the operations should be controlled within narrow limits. Titanium and titanium alloys must be protected from contamination by oxygen, nitrogen, hydrogen and carbon during heating for the forging operations Although heating in vacuum or in a suitably inert atmosphere is feasible, this is most effectively done by coating the forging slugs in a liquid glaze which is allowed to dry before heating for forging. Prolonged heating should be avoided for all titanium alloys. For forging operations the preferred temperature lies between 850°c and 950°c. After proper heating the billets were transferred in to the hammer for the further processing. The hammer having a capacity of 10 tonne is applied along the alloy surface for creating different shapes. While the forging operations the temperature of the alloy may be reduced to below the working temperature range. Due to the reduction of the temperature the alloys should be reheated in the electrical furnace, under precisely setting the temperature gradient under controlled environment. The forging temperature of titanium alloys is absolutely critical to the process and die heating is essential, as excessive heat losses through the tooling will produce defective forgings. Despite the protection offered by the glass coating, a small amount of contamination does occur and must be removed by grinding or chemical etching. When forging titanium, care should be taken to prevent contact with steel scale. A thermal type reaction can occur and seriously damage a forging die. Apparently the titanium reduces iron oxide in an exothermic reaction set off by pressure and high temperature. If an unscheduled delay such as a press breakdown occurs, the stocks should be removed from the furnace, and then it should be reheated when forging is resumed. Particular attention need to be paid throughout the processing cycle to avoid contamination by oxygen, nitrogen, carbon, and/or hydrogen, which can severely impair ductility and toughness properties and overall quality of a forged part. TEMPERATURE TEMPERATURE JOB AFTER 10 JOB AFTER 10 NO BLOWS NO BLOWS 1 927 12 863 2 920 13 845 3 915 14 918 4 920 15 915 5 908 16 912 6 903 17 909 7 898 18 904 8 901 19 897 9 890 20 894 10 880 21 887 11 885 Table 1: Temperature of the jobs after 10 blows The temperature of each of stocks during the forging operations were noted (Table 1). Optical pyrometer which intercepts the thermal radiation from the alloy were used to measure the temperature of the billets while the operation. The temperature of the alloys may be increased due to the plastic deformation of the stock or the temperature decreases during the transferring of the stock from furnace to the hammer. [1] The various reasons for the variation of the temperature and the reheating of the titanium alloys at the electrical furnace during the operations were identified and their effects were explored in this work. Statistical process control charts are used to determine temperature variation and fishbone diagram is used to identify the causes and effects of the increases or decrease in temperature. III. RESULTS AND DISCUSSIONS The forging operations of the Ti6Al4V, titanium alloy having a batch size of 21 was taken in to the study. During the operations one of the alloy temperature decreases below the minimum range. The average temperature of each alloy in the batch is calculated after 10 blows and it is represented in a control charts, 81
  • 3. Cause and Effect Analysis for Reheating the Titanium alloys while forging… having an upper control limit of 930°c, lower control limit of 850°C. and mean temperature of 899.57°C and it is represented in figure 2. Figure 2: Control chart for the forging temperature From the figure 2 it is evident that, the temperature of one job ( job no 13) is decreased, which results in the reheating of that particular job in the electrical furnace. The reheating of the titanium alloy in the electrical furnace results in increase power consumption, fuels, working hour etc. and if the forging temperature of the alloy becomes below 850⁰c,changes will happens in the microstructure of alloy, and also in the formation and filling of the material. The different causes for the reheating of the titanium alloy in the electrical furnace includes unskilled workers, short circuiting of electrical systems, improper die packing, conventional material handling systems, environmental factors such as presence of salvage, surrounding temperature. These main causes are supported by some other causes also, which is represented in figure 3. Figure 3: Cause and effect diagram IV. CONCLUSION The different causes for the reheating of the titanium alloy during the forging operations were determined with the help of fishbone diagram.  Proper training should be given to the workers in order to reduce the no. of blows during the operations and handling of the job.  The efficiency of the compressor should be calibrated periodically. 82
  • 4. Cause and Effect Analysis for Reheating the Titanium alloys while forging…  Periodically the maintenance operations should be carried out in the hammer. The forging operations should be done below the maximum capacity of the hammer.  Conventional material handling systems should be replaced by conveyors and AGV’s to reduce the travelling time between the hammer and the furnace.  The efficiency of the Plant layout should be tested using Arena software. Inventory and scraps should be removed after each operations.  Application of Kaizen in industry wills results im good performance.  Operation of the electrical furnace should be done at controlled environment ACKNOWLEDGMENT The authors would like to thank all of his colleagues for their support in completing this case study. REFERENCES [1] Y G Zhou, W.D Zeng, H Q Yu,(2005) “An investigation of a new near-beta forging process for titanium alloys and its application in aviation components”, Materials Science and Engineering, vol. 393, no. 1, pp. 204-212. [2] C.C Chen, J E Coyne (1976), “ Deformation Characteristics of Ti-6Al-4V alloy under Isothermal Forging conditions”, metallurgical transactions A, vol 7( A): pg 1931-1940. [3] James D Destefani, ”Properties & selection: Non ferrous alloys and special purpose materials”, ASM international,ASM handbook, pages 586-605. [4] Dale H Besterfeild, Glen H Besterfeild, “Total Quality Management”, 2003, pages 205-213. AUTHORS First author Nice Menachery, graduated in Mechanical Engineering from Calicut University, doing Post Graduate Student in Production & Industrial Engineering at SCMS School of Engineering and Technology, affiliated to Mahatma Gandhi University, Kerala, India. Second author Binoy Boban, graduated in Mechanical Engineering from Anna University, doing Post Graduate Student in Production & Industrial Engineering at SCMS School of Engineering and Technology, affiliated to Mahatma Gandhi University, Kerala, India. Third author Jino Joy, graduated in Mechanical Engineering from Anna University, doing Post Graduate Student in Production & Industrial Engineering at SCMS School of Engineering and Technology, affiliated to Mahatma Gandhi University, Kerala, India. 83