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Chapter 17




Milk powder
The method of preserving various foodstuffs by drying them, and thereby
depriving micro-organisms of the water necessary for their growth, has
been known for centuries. According to Marco Polo’s accounts of his
travels in Asia, Mongolians produced milk powder by drying milk in the
sun.
    Today milk powder is produced on a large scale in modern plants.
Skimmilk powder has a maximum shelf life of about 3 years. Whole milk
powder has a maximum shelf life of about 6 months. This is because the
fat in the powder oxidises during storage, with a consequent gradual
deterioration in taste.




Dairy Processing Handbook/chapter 17                                              361
Drying
      Drying means that the water in a liquid product – in this case milk – is re-
      moved, so that the product acquires a solid form. The water content of milk
      powder ranges between 2.5 and 5%, and no bacteria growth occurs at
      such a low water content. Drying extends the shelf life of the milk, simulta-
      neously reducing its weight and volume. This reduces the cost of transport-
      ing and storing the product.
         Freeze-drying has been used to produce high-quality powder. In this
      process the water is evaporated from the milk under vacuum. This method
      offers advantages from the quality aspect, as the protein fraction is not
      affected. The powder will always be affected to a greater or lesser extent if
      drying is carried out at a higher temperature. Freeze-drying is not however
      widely used, partly because of the high energy demand.
         Commercial methods of drying are based on heat being supplied to the
      product. The water is evaporated and removed as vapour. The residue is
      the dried product – the milk powder. Two principal methods are used for
      drying in the dairy industry: roller drying and spray drying. In spray drying,
      the milk is first concentrated by evaporation and then dried in a spray tower.
         During the first stage of drying the excess water, in free form between
      the particles of the dry solids, is evaporated. In the final stage the water in
      pores and capillaries of the solid particles is also evaporated.
         The first stage is relatively fast, whereas the last stage demands more
      energy and time. The product will be significantly affected by the heat if this
      drying is carried out in such a way that milk particles are in contact with the
      hot heat transfer surfaces – as in the case of roller drying. The powder may
      then contain charred particles which impair its quality.

      Various uses of milk powder
      Dried milk is used for many applications, such as:
      • recombination of milk
      • mixing into dough in the bakery industry to increase the volume of the
         bread and improve its water-binding capacity. The bread will then remain
         fresh for a longer period of time.
      • mixing into pastry dough to make it crisper
      • as a substitute for eggs in bread and pastries
      • producing milk chocolate in the chocolate industry
      • producing sausages and various types of ready-cooked meals in the
         food industry and catering trade
      • as a substitute for mother’s milk in baby foods
      • production of ice-cream
      • animal feed


        Table 17.1
        Extra grade skimmilk powder
        (ADMI* specification for skimmed milk powder)

        Property                         Spray dried                Roller dried
                                        not exceeding              not exceeding
        Milk fat content                    1.25 %                     1.25 %
        Moisture content                    4.00 %                     4.00 %
        Titratable acidity, l.a.            0.15 %                     0.15 %
        Solubility index                    1.25 ml **                15.00 ml
        Bacterial estimate            50 000 per gram            50 000 per gram
        Scorched particles         Disc B (15.0 mg)           Disc C (22.5 mg)
        *  ADMI = American Dry Milk Institute Inc. (This institution has also published
           “Standards For Grades of Dry Milks including Methods of Analysis”).
        ** Except powders designated as “high-heat” (HH), for which the permitted
           maximum is 2.0 ml.




362                                                   Dairy Processing Handbook/chapter 17
Skimmilk powder
Skimmilk powder is by far the most common type of milk powder.
    Each field of application makes its own specific demands on milk pow-
der. If the powder is to be mixed with water in recombined milk for con-
sumption, it must be easily soluble and have the correct taste and nutritive
value. Some degree of caramellisation of the lactose is beneficial in choco-
late production. In the first case gentle drying of the product in a spray
tower is essential, whereas in the second case the powder must be sub-
jected to intense heat treatment in a roller dryer. Two types of powder are
therefore distinguishable:
1 roller dried powder
2 spray dried powder
    Table 17.1 shows an example of the standards applicable to skimmilk
powder. The solubility of spray powder is very good, whereas that of roller
dried powder is appreciably poorer, on account of the intense heat treat-
ment in roller drying.
    Depending on the intensity of the heat treatment, milk powder is classi-
fied into categories related to the temperature/time combinations the skim-
milk has been exposed to prior to evaporation and drying.
    Heat treatment denatures whey proteins, the percentage denaturated
increasing with the intensity of heat treatment. The degree of denaturation is
normally expressed by the Whey Protein Nitrogen Index (WPNI) as milli-
grams of undenatured whey protein (u.w-p) per gram of powder.
    Information about various categories of spray dried skimmilk powder is
summarised in Table 17.2.



   Table 17.2
   Categories of spray dried skimmilk powder.

   Category                                                     Temp/time     WPNI
                                                                            mg/g u.w-p
   Extra low-heat                                             <70°C              *
   Low-heat (LH) powder                                    70°C/15 s           > 6.0
   Medium-heat (MH) powder                                 85°C/20 s          5 – 6.0
   ”                                                       90°C/30 s          4 – 5.0
   ”                                                       95°C/30 s          3 – 4.0
   Medium high-heat (HH)                                  124°C/30 s         1.5 – 2.0
   High-heat (HH)                                       appr. 135°C/30 s       <1.4
   High-heat high stable (HHHS)                         appr. 135°C/30 s       <1.4
   (from selected milk)
   * Not measurable
   Table by Sanderson N.Z., J. Dairy Technology, 2, 35 (1967)




Whole milk powder
Spray dried whole milk powder is nomally produced from fat standardised
milk. After standardisation the milk need not be homogenised provided that
it is thoroughly agitated, without air inclusion, before evaporation and again
between evaporation and spray drying. The concentrate is however hom-
ogenised in certain cases for production of instant whole milk.
     Fat standardised milk for production of roller dried powder is normally
homogenised.
     Whole milk powder, unlike skimmilk powder, is not categorised. Milk
intended for whole milk powder is normally pasteurised at 80 – 85°C to
inactivate most of the lipolytic enzymes that would otherwise degrade the
milk fat during storage.



Dairy Processing Handbook/chapter 17                                                     363
Instant-milk powder
      Special methods for the production of both skimmilk and whole milk pow-
      der with extremely good solubility – known as instant powder – are also
      available. This powder has a larger grain size, influenced by agglomeration,
      than normal spray powder and dissolves instantly even in cold water.

      Bulk density
      When powders are shipped over long distances it is important that they
      have a high bulk density to reduce the volume, since in most cases trans-
      portation costs are calculated by volume. A high bulk density also saves
      packaging material. However, in some instances the producers may be
      interested in low bulk density to supply optically larger amounts of powder
      than that of their competitors. Low bulk density, as influenced by agglomer-
      ation, is also an important characteristic of instant powders.

      Definition
      Bulk density is the weight of a unit volume of powder; in practice it is ex-
      pressed as g/ml, g/100 ml or g/l.

      Factors influencing bulk density
      The bulk density of milk powders is a very complex property; it is the result
      of several other properties and is influenced by a number of factors. The
      primary factors determining bulk density are:
      1 The particle density, given by :
         – powder material density
         – the content of the occluded air inside the particles
      2 The content of interstitial air, i.e. the air between the particles.

      Powder material density
      The powder material density is given by the composition of the powder. It
      depends on the contents and densities of the individual components, and
      can be calculated according formula:


                                     100
                    %A %B %C
                        +    +    + etc. + % moisture
                     DA   DB   DC


            % A, % B, % C are equivalent to the percentages of the
            components having densities DA, DB, DC.



      Occluded air content
      Milk powder normally contains between 10 and 30 ml of entrapped air per
      100 g of powder. There are many factors influencing the occluded air in
      powder particles.
         Some of these factors will just be touched upon below:
      • Incorporation of air into the feed. The concentrate is effectively deaerated
      by evaporation, but when it is transferred to the spray dryer it may pick
      up air from leaking pipelines, etc.
      • The system chosen for spraying the concentrate into the dryer.
      • The properties of the feed. The amount of air incorporated into the prod-
      uct depends not only on the intensities of whipping action before or during
      atomisation, but also on the properties of feed, i.e. the ability of the feed to
      form stable foam. This property is mainly influenced by the content and
      state of proteins and the possible presence of whipping inhibitors. Thus
      concentrates which contain fat are much less prone to foaming than skim-
      milk. The following factors influence the foaming properties of skimmilk in
      the drying process:



364                                                Dairy Processing Handbook/chapter 17
• Undenaturated whey proteins have a great tendency to foam; this can
be reduced by heat treatment proportional to the degree of denaturation,
see Table 17.2.
• Concentrates with a low total solids content foam more than highly
concentrated feeds.
• Cold concentrates are more easily whipped than warm ones.

Interstitial air
The air content between the particles, the interstitial air, may amount to
about 127 ml/100 g of powder. This is a very complex property which de-
pends for example on the particle size distribution and the degree of ag-
glomeration.



Production of milk powder
In the production of roller dried powder, the pre-treated milk is admitted to
the roller dryer and the whole drying process takes place in one stage.
    In the production of spray dried powder, the milk is first evaporated un-
der vacuum to a DM content of about 45 – 55%. Spray dried skimmilk
powder is manufactured in two basic qualities:
• ordinary product and
• agglomerated product (instant milk powder) by various spray drying
    systems.
Following both roller and spray drying, the powder is packed in cans, paper
bags, laminated bags or plastic bags, depending on the quality and the
requirements of the consumers.



Raw material
Very strict demands are made on the quality of the raw material for produc-
tion of milk powder. Table 17.1 shows that the number of bacteria per gram
of powder must not exceed 50 000, or even 30 000 in some countries. This
corresponds to about 5 000 (or 3 000) bacteria per litre of reconstituted
product, provided that no reinfection occurs. Since spray powder produc-          Strict demands are made on
tion involves vacuum evaporation, it is just as important as in the production    the quality of the raw material
of condensed milk to keep heat-resistant bacteria under control so that they      for production of milk powder.
will not multiply during evaporation. Bactofuge treatment or microfiltration is
therefore also used in powder production to remove bacteria spores from
the milk, thereby improving the bacteriological quality of the end product.
    Milk for powder production must not be subjected to excessive, intense
heat treatment prior to delivery to the milk powder plant. Such heat treat-
ment would cause the whey protein to coagulate, and the solubility, aroma
and taste of the milk powder would be impaired. The milk is subjected to
the peroxidase test or the whey protein test to determine whether the pre-
ceding heat treatment was too intense. Both of these tests indicate whether
or not the milk was previously pasteurised at a high temperature.



General pre-treatment of the milk
In the production of skimmilk powder the milk is clarified in conjunction with
fat separation. This is also the case if the fat content is standardised in a
direct standardisation system. Standardised milk used for producing whole
milk powder is not normally homogenised unless it is to be roller dried.
    Skimmilk intended for powder production must be pasteurised at least to
a negative phosphatase test. In the production of dried whole milk the heat
treatment must be so intense that the lipases will also be inactivated. This
normally involves high-temperature pasteursation to a negative peroxidase
test.




Dairy Processing Handbook/chapter 17                                                                                365
Roller or drum drying
                                           In roller drying the milk is distributed on rotating, steam-heated drums. The
                                           water in the milk evaporates and is drawn off by a flow of air when it comes
                                           in contact with the hot drum surface. The high temperature of the heating
                                           surfaces converts the protein to a form which is not easily soluble and
                                           which discolours the product.
                                               Intense heat treatment increases the water-binding properties of the
                                           powder. This characteristic is useful in the prepared-food industry.
                                               The distinction between trough-fed and spray-fed roller dryers is based
                                           on the manner in which the milk is fed on to the drums.
                                               Figure 17.1 shows the principle of the trough-fed roller dryer. The pre-
                                           treated milk is admitted to a trough formed by the cast iron drums and their
                                           end walls. A thin layer of milk on the drums is heated quickly when it comes
                                           in contact with the hot surface. The water is evaporated and the layer of
                                           milk on the drum dries. This film is continuously scraped off by knives in
                                           contact with the periphery of each drum.
                                               The dried milk falls into a screw conveyor in which it is ground into flakes.
                                           The flakes are then transferred to a grinder, and hard and burned particles
Fig. 17.1 Principle of the trough-fed      are separated on a screen at the same time.
roller dryer.                                  Depending on capacity, the double roller dryer is 1 – 6 m long and has a
              Milk                         drum diameter of 0.6 – 3 m. The size depends on film thickness, tempera-
              Heating medium               ture, drum speed and the required DM content of the dried product.
              Air for pneumatic                The thickness of the dry layer can be varied by adjusting the gap be-
              transportation and cooling   tween the drums.
                                               Figure 17.2 shows the principle of the spray-fed roller dryer. Nozzles
                                           above the drums spray a thin film of pre-treated milk on the hot surfaces of
                                           the drums. In this arrangement almost 90% of the heat transfer area is
                                           utilized, as opposed to less than 75% in the trough-fed dryer.
                                               The film thickness is determined by the supply pressure to the spray
                                           nozzles. The drying time can also be controlled by adjusting the tempera-
                                           ture and the speed of the drums. This provides some scope for controlling
                                           the characteristics of the powder. If the parameters are correct, the milk film
                                           should be almost dry when it is scraped off the drums.
                                               The dry film scraped off the drums is subjected to the same treatment as
                                           for the trough-fed dryer.

                                           Spray drying
                                           Spray drying is carried out in two phases. In the first phase the pre-treated
                                           milk is evaporated to a DM content of 45 – 55%. In the second phase the
                                           concentrate is pumped to a drying tower for final drying. This process takes
                                           place in three stages:
                                           • Dispersion of the concentrate into very fine droplets.
                                           • Mixing of the finely dispersed concentrate into a stream of hot air which
Fig. 17.2 Principle of the spray-fed          quickly evaporates the water.
roller dryer.                              • Separation of the dry milk particles from the drying air.
              Milk                         Evaporation is a necessary production stage for high-quality powder. With-
              Heating medium               out prior concentration the powder particles will be very small and will have
              Air for pneumatic            a high air content, poor wettability and a short shelf life. The process will
              transportation and cooling   then also be uneconomical.
                                              Falling-film evaporators are generally used for concentration, which is
                                           carried out in two or more stages to a DS content of 45 – 55%. The equip-
                                           ment is the same as that used in the production of condensed milk.


                                           Basic drying installations
                                           Single-stage drying
                                           The most simple installation for making ordinary powder is the spray dryer
                                           with a pneumatic conveying system, figure 17.3.
                                              This system works on the single-stage drying principle, which means


366                                                                                     Dairy Processing Handbook/chapter 17
3


                                                      5
                               4
                                                                           8
                                                                                   Fig. 17.3 Conventional spray dryer
                                                                                   (one-stage drying) with conical base
                                                                                   chamber.
                                                                                   1 Drying chamber
                                   1
                                                                                   2 Air heater
                                                                                   3 Milk concentrate tank
                                                                                   4 High pressure pump
                                                                                   5 Atomiser
                                                                                   6 Main cyclone
                                                                                   7 Transport system cyclone
                                                                                   8 Air suction fans and filters
                                                                               7
                                                          6
                                                                                                  Milk
                           2                                                                      Air
                                                                                                  Powder




that all removal of moisture from the concentrate to the required final mois-
ture content takes place in the spray drying chamber (1). The subsequent
pneumatic conveying system serves only to collect the powder leaving the
chamber cone together with the powder fraction separated from the ex-
haust air in the main cyclone (6), to cool the powder and feed it via the final
cyclone (7) to the bagging-off hopper.

Two-stage drying
In a two-stage drying system producing the same type of powder as the
previously mentioned installation, the pneumatic conveying system is re-           Percentage of initial value
placed by a fluid bed dryer, the working principle of which is discussed           100
below under the heading “Operating principle of spray drying”.                       90
                                                                                                           D
                                                                                     80
Three-stage drying                                                                   70
Three-stage drying is an extension of the two-stage concept developed to
achieve even greater savings in plant operation costs.                               60                          W
                                                                                     50                              V
Operating principle of spray drying                                                  40
                                                                                     30
Single-stage drying                                                                                                  4% H20
                                                                                     20
Figure 17.3 shows the arrangement of a single-stage drying plant. The milk
concentrate is fed to the drying chamber (1) by a high-pressure pump (4),            10
and then continues to the atomiser (5). The very small milk droplets are              0
sprayed into the mixing chamber, where they are mixed with hot air.                       45 50   60    70     80      90 100
    Air is drawn in by a fan through a filter and supplied to a heater (2),                             Droplet solid content (%)
where it is heated to 150 – 250°C. The hot air flows through a distributor to
a mixing chamber. In the mixing chamber the atomised milk is mixed thor-           Fig. 17.4 Weight, volume and diameter
oughly with the hot air and the water in the milk is evaporated. Most of the       decrease of droplet under ideal drying
drying takes place as the droplets are decelerated by air friction following       conditions down to 4% H2O.
release from the atomiser at high velocity. The free water evaporates instan-      D = Diameter
taneously. The water in the capillaries and pores must first diffuse to the        W = Weight
surfaces of the particles before it can be evaporated. This takes place as         V = Volume
the powder slowly settles in the spray tower. The milk is only heated to 70 –
80°C because the heat content of the air is continuously consumed by
evaporation of water.


Dairy Processing Handbook/chapter 17                                                                                       367
Loss of water from the droplets leads to a considerable reduction in
                                           weight, volume and diameter. Under ideal drying conditions, weight will
                                           decrease to about 50%, volume to about 40%, and the diameter to about
                                           75% of the droplet size produced by release from the atomiser, figure 17.4.
                                              During the drying process the milk powder settles in the drying chamber
                                           and is discharged at the bottom. It is conveyed pneumatically to the pack-
                                           ing section by cooling air which is drawn into the conveyor duct by a fan.
                                           After cooling, the mixture of cooling air and powder flows to the discharge
                                           unit (7), where the powder is separated from the air before being packed.
                                              Some small, light particles may be mixed with the air that leaves the
                                           drying chamber. This powder is separated in one or more cyclones (6, 7).
                                           After separation the powder is returned to the main stream of milk powder
                                           on the way to packing. The cleaned drying air is extracted from the plant by
                                           a fan.

                                           Milk atomising
                                           The more finely dispersed the milk droplets, the larger their specific area will
                                           be and the more effective the drying. One litre of milk has a surface area of
                                           about 0.05 m2. If this quantity of milk is atomised in the spray tower, each of
                                           the small droplets will have a surface area of 0.05 – 0.15 mm2 . The total
                                           surface area of all the milk droplets from the original litre of milk will be about
      A                                    35 m2. Atomising thus increases the specific area about 700 times.
                                               The design of the atomising equipment depends on the particle size and
                                           the properties required of the dried product. These properties can be
                                           granularity, texture, solubility, density and wettability. Certain dryers have
                                           stationary nozzles, see figure 17.5. The arrangement in figure 17.5 A is used
                                           in low spray towers and is located so that the relatively large milk droplets
       B                                   will be discharged in counterflow in relation to the drying air. A stationary
                                           nozzle which discharges the milk in the same direction as the air flow is
                                           shown in figure 17.5 B. In this case the milk feed pressure determines the
                                           particle size. At high feed pressures (up to 30 MPa or 300 bar) the powder
                                           will be very fine and have a high density. At low pressures (20 – 5 MPa or
                                           200 – 50 bar) the particle sizes will be larger and there will be no dust-size
                                           particles.
                                               Figure 17.6 shows another very common type of atomiser, consisting of
                                           a rotating disc with passages from which the milk is ejected at high velocity.
                                           In this case the properties of the product are controlled by the speed of
                                           rotation of the disc. It can be varied between 5 000 and 25 000 r/min.

                                           Two-stage drying
                                           The last traces of moisture are the most difficult to remove, unless high
Fig. 17.5 Stationary nozzles for atomis-   outlet drying temperatures are used to provide a sufficient driving force. As
ing the milk in a spray drying chamber.    elevated outlet drying temperatures can have a detrimental effect on pow-
A Counterflow nozzle
                                           der quality, it is essential to operate at lower outlet temperatures with dairy
B Nozzle discharging in the direction of
    the air flow
                                           products. If the moisture content of the resulting powder is still too high, an
                                           after-drying stage is incorporated after the spray dryer in a two-stage proc-
                                           ess as illustrated in figure 17.7.
                                               Two-stage drying methods for producing powdered milk product com-
                                           bine spray drying as the first stage and fluid bed drying as the second
                                           stage.
                                               The moisture content of the powder leaving the chamber is 2 – 3 per
                                           cent higher than the final moisture content. The function of the fluid bed
                                           dryer is to remove excess moisture and finally to cool the powder down.
                                               Drying of milk in two stages was originally developed to obtain agglomer-
                                           ated powders in straight-through processing, but in the early seventies was
                                           adopted for non-agglomerated powders so that the advantage of product
                                           quality improvement could be combined with the better process economy
Fig. 17.6 Rotating disc for atomising
milk in the spray drying chamber.
                                           of two-stage processing.
                                               The powder from both single-stage and two-stage installations consists
                                           predominantly of single particles; it is dusty and difficult to reconstitute.
                                           There are however some slight differences. Two-stage dried powder is
                                           coarser due to bigger primary particles and the presence of some agglom-


368                                                                                      Dairy Processing Handbook/chapter 17
erates. Consequently it is not so dusty and can be reconstituted more easi-
ly. However, the biggest difference between these two powders is in the
properties that are influenced by heat exposure during drying.
    The properties in question are the solubility index and the content of
occluded air, both lower, and bulk density, which is higher. The droplet
temperature just after atomisation is low, just slightly above the wet bulb
temperature of the drying air. The particle temperature increases gradually
with progressive water removal, finally achieving a temperature which is
below the outlet air temperature – how much lower depends on the mois-
ture content of the particles.
    The one-stage and two-stage drying systems are compared in table
17.3.




                      2




                                                                                                 Milk
                                                                                                 Heating medium
                                                                                                 Powder
                                                3
      1                   4                                                        Fig. 17.7 Spray dryer with fluid bed
                                                                                   attachment (two-stage drying).
                                                                                   1 Indirect heater
                                  5                                                2 Drying chamber
                                                                                   3 Vibrating fluid bed
                                                          7
                                                                                   4 Heater for fluid bed air
                                 6                                                 5 Ambient cooling air for fluid bed
                                                                                   6 Dehumidified cooling air for fluid bed
                                                                                   7 Sieve



Three-stage drying
The three-stage dryer involves transfer of the second drying stage into the
base of the spray drying chamber and having the final drying and cooling
conducted in the third stage located outside the drying chamber.
    There are two main types of three-stage dryers:
1 Spray dryers with integrated fluid bed
2 Spray dryers with integrated belt
    The principle of the second type, spray dryers with integrated bed, will
be touched upon below.
    The Filtermat type of dryer is shown in figure 17.8. It consists of a main
drying chamber (3) and three smaller chambers for crystallisation (when
required, e.g. for production of whey powder), final drying and cooling (8,9,
10).
    The product is atomised by nozzles located in the top of the main cham-
ber of the dryer. The feed is conveyed to the nozzles by a high pressure
pump. Atomisation pressure is up to 200 bar. Most of the drying air is sup-
plied to the drying chamber around the individual nozzles at temperatures
up to 280°C.
    Primary drying of the droplets takes place as they fall from the nozzles (2)
to the moving belt (7) located at the base of the chamber. The powder is
deposited on the belt in an agglomerated porous layer.
    The second drying stage takes place as drying air is sucked through the



Dairy Processing Handbook/chapter 17                                                                                   369
Table 17.3
                                                 Comparison of one-stage and two-stage drying systems.

                                                 Drying system                                    One-stage Two-stage
                                                                                                  Inlet temp. Inlet temp.                 Inlet temp.
                                                                                                     200°C       200°C                       230°C
                                                 Spray dryer (First stage)
                                                 Evaporation in chamber, kg/h                          1 150               1 400              1 720
                                                 Powder from chamber:
                                                  6 % moisture, kg/h                                       –               1 460              1 790
                                                  3.5% moisture, kg/h                                  1 140                   –                  –
                                                 Energy consumption,
                                                  spray drying total, Mcal                             1 818               1 823              2 120
                                                 Energy/kg powder, kcal                                1 595               1 250              1 184
                                                 Fluid Bed (Second Stage)
                                                 Drying air, kg/h                                             –            3 430              4 290
                                                 Inlet air temperature, °C                                    –              100                100
Fig. 17.8 Spray dryer with integrated            Evaporation in fluid bed, kg/h                               –               40                 45
belt, Filtermat (three-stage drying).            Powder from fluid bed
1 High pressure feed pump                          3.5 % moisture, kg/h                                       –            1 420              1 745
2 Nozzle arrangement                             Energy consumption, kW                                       –               20                 22
3 Primary drying chamber                         Energy consumption,
4 Air filters                                      total in fluid bed, Mcal                                   –                  95              115
5 Heater/cooler
6 Air distributor                                Total plant
7 Belt assembly                                  Energy consump. total, Mcal                           1 818               1 918              2 235
8 Retention chamber                              Energy/kg powder total, kcal                          1 595               1 350              1 280
9 Final drying chamber                           Energy relation                                         100                  85                 80
10 Cooling chamber
11 Powder discharge                              Basis: Same drying chamber size with inlet air flow = 31,500 kg/h.
12 Cyclone arrangement                           Product: skimmilk, 48% solids in concentrate.
13 Fans                                          Source: Evaporation, Membrane Filtration, Spray Drying - North European Dairy Journal, 1985 Copenhagen, Denmark.
                                                 ISBN No. 87-7477-000-4.
14 Fines recovery system
15 Sifting system
16 Heat recovery system

                                                                                  2                                5
                                         5                                                                                                     13
                4
                                                                                 6

                     16

                                                                                                                             5                          13

                                         1                      3
                                                                                        8             9       10

                                             7


                                                                                                                               11
                    13

                                    12

                       14

                                                                                                                15
              Concentrated milk
              Milk powder
              Heating air


370                                                                                                               Dairy Processing Handbook/chapter 17
powder layer. The moisture content of the powder falling on the belt (7) is
12 – 20 % depending upon the type of product. This second drying stage
on the belt reduces the moisture content to 8-10 %. The moisture content
is very important to achieving the exact degree of agglomeration of the
product and porosity of the powder layer. The third and last drying stage for
skimmilk and whole milk concentrates takes place in two chambers (8, 9),
where hot air at an inlet temperature of up to 130°C is sucked through the
powder layer and the belt in the same way as in the main chamber. The
powder is cooled in a final chamber (10). Chamber (8) is used in cases
where crystallisation of lactose is required (whey powder). In this case air is
not conveyed to the chamber, so the moisture content remains at a higher
level, up to 10 %. The third drying stage takes place in chamber (9), and
cooling air is supplied to chamber (10).
    Only a small amount of powder leaves the plant together with the drying
and cooling air as fines. This powder is separated from the air in a cyclone
battery (12). The powder is recirculated, either to the main chamber or to a
point in the process appropriate to the type of product and the agglomera-
tion required.
    After leaving the dryer the powder agglomerates are broken down to the
required size in a sifter (15) or milled, depending on the type of product.

Production of instant powder
Milk powder which will dissolve quickly in water must be instantised, i.e. the
milk particles must be treated so that they form larger, porous agglomer-
ates. To obtain the correct porosity the milk particles must first be dried so
that most of the water in the capillaries and pores is replaced by air. The
particles must then be humidified, so that the surfaces of the particles swell
quickly, closing the capillaries. The surfaces of the particles will then be-
come sticky and the particles will adhere to form agglomerates.
    One method of producing instantised powder is to recirculate the dry          Fig. 17.9 Rotating disc designed for
milk particles back to the mixing chamber containing drying air and atom-         production of instantised powder.
ised milk particles, figure 17.9. As soon as the dry particles are admitted to
the chamber, their surfaces are humidified by the evaporated water and the
particles swell. The capillaries and pores close and the particles become
sticky. Other milk particles adhere to the surface and agglomerates are
formed.

Fluid-bed drying
More efficient instantisation can be obtained with a fluid bed of the type
shown in figure 17.10. The fluid bed is connected to the bottom of the
drying chamber and consists of a casing with a perforated bottom. The
casing is spring mounted and can be vibrated by a motor. When a layer of
powder is distributed on the perforated bottom, the vibrations convey the
powder at uniform speed along the length of the casing.
   The powder from the drying chamber is admitted to the first section,




                                                                                                    Fig. 17.10 Fluid bed
                                                                                                    for instantising milk
                                                                                                    powder.



                                                                                                             Milk powder
                                                                                                             Steam
                                                                                                             Hot air
                                                                                                             Cold air




Dairy Processing Handbook/chapter 17                                                                                 371
where it is humidified by steam. The vibrations convey the powder through
                                         the drying sections, where air at a gradually decreasing temperature is ad-
                                         mitted through the powder bed. Agglomeration takes place in the first stage
                                         of drying when the particles adhere to each other. Water is evaporated from
                                         the agglomerates during their passage through the drying sections. They
                                         will have attained the required dryness when they have passed through the
                                         fluid-bed casing.
                                             Any larger particles at the outlet of the dry bed are screened and recircu-
                                         lated to the inlet. The screened and instantised particles are conveyed by
                                         the cooling air to a battery of cyclones, where they are separated from the
                                         air and packaged.
                                             The drying air from the fluid bed, together with the air from the spray
                                         tower, is then blown to the cyclone for recovery of milk particles.

                                         Heat recovery
                                         A large amount of heat is lost in the drying process. Some can be recov-
                                         ered in heat exchangers, but the drying air contains dust and vapour and
                                         therefore requires specially designed exchangers.
                                            In several cases a special type of heat exchanger with glass pipes is
                                         used, see figure 17.11. The smooth glass surface prevents fouling to a
                                         great extent. A CIP system is included in the plant.
                                            The warm air is introduced from the bottom and forced through the glass
                                         pipes. The fresh air to be heated flows on the outside of the pipes. With this
                                         method of heat recovery the efficiency of the spray drying plant can be
                                         increased by 25 – 30%.
                                            A further possibility is to recover the heat in the condensate from the
                                         evaporation plant. The plant operates in parallel with the spray drying plant,
                                         and such a solution is therefore feasible with savings of 5—8% of the drying
                                         costs.


                                                                            2
                                                                                                                 4
Fig. 17.11 Heat recovery from effluent
air in a spray drying plant.
1 Fan for fresh air
2 Glass pipe heat exchanger
3 Heater
                                                                                               3
4 Spray tower
5 Cyclones
6 Fan for effluent air                   1                    6



                                                                                5




                                         Packing milk powder
                                         The types and sizes of packages vary widely from one country to another.
                                         The powder is often packed in laminated powder bags with an inner bag of
                                         polyethylene. The polyethylene bag is often welded, and this package is
                                         practically as airtight as sheet-metal drums. The most common bag sizes
                                         are 25 and 15 kg, although other sizes are also used as it is very easy to
                                         vary the weight of the powder in the bags to meet specific customer re-
                                         quirements. Milk powder for households and similar small-scale consumers
                                         is packed in tin cans, laminated bags or plastic bags which, in turn, are
                                         packed in cartons.



372                                                                                  Dairy Processing Handbook/chapter 17
Changes in milk powder during storage
The fat in whole milk powder oxidises during storage. On an industrial scale
the shelf life can be extended by special pretreatment of the milk, by the
addition of anti-oxidants and, in the case of sheet-metal drums, by filling
under inert gas.
   Milk powder should be stored under cool conditions and protected
against contact with water during storage. All chemical reactions in milk
powder, at room temperature and with a low water content, take place so
slowly that the nutritive value is not affected even after years of storage.

Dissolving milk powder
One part of ordinary spray-dried powder is mixed with about ten parts of
water at a temperature of 30 – 50°C. The dissolving time is about 20 – 30
minutes. Longer times are needed at lower temperatures. 8 – 12 hours are
required if the powder is to be dissolved in cold water.
    If instantised powder is used, the required quantity of water is poured
into a tank and the powder is then added. The powder dissolves after very
brief stirring, even if the water is cold. The milk is then immediately ready for
drinking.
    The water quality is very important at dissolving. It must be borne in mind
that at drying including the first concentration phase (evaporation), the milk
has been rid of pure (distilled) water. More about the water quality in chapter
18, Recombined milk products.




Dairy Processing Handbook/chapter 17                                                373
374   Dairy Processing Handbook/chapter 17

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Milk powder

  • 1. Chapter 17 Milk powder The method of preserving various foodstuffs by drying them, and thereby depriving micro-organisms of the water necessary for their growth, has been known for centuries. According to Marco Polo’s accounts of his travels in Asia, Mongolians produced milk powder by drying milk in the sun. Today milk powder is produced on a large scale in modern plants. Skimmilk powder has a maximum shelf life of about 3 years. Whole milk powder has a maximum shelf life of about 6 months. This is because the fat in the powder oxidises during storage, with a consequent gradual deterioration in taste. Dairy Processing Handbook/chapter 17 361
  • 2. Drying Drying means that the water in a liquid product – in this case milk – is re- moved, so that the product acquires a solid form. The water content of milk powder ranges between 2.5 and 5%, and no bacteria growth occurs at such a low water content. Drying extends the shelf life of the milk, simulta- neously reducing its weight and volume. This reduces the cost of transport- ing and storing the product. Freeze-drying has been used to produce high-quality powder. In this process the water is evaporated from the milk under vacuum. This method offers advantages from the quality aspect, as the protein fraction is not affected. The powder will always be affected to a greater or lesser extent if drying is carried out at a higher temperature. Freeze-drying is not however widely used, partly because of the high energy demand. Commercial methods of drying are based on heat being supplied to the product. The water is evaporated and removed as vapour. The residue is the dried product – the milk powder. Two principal methods are used for drying in the dairy industry: roller drying and spray drying. In spray drying, the milk is first concentrated by evaporation and then dried in a spray tower. During the first stage of drying the excess water, in free form between the particles of the dry solids, is evaporated. In the final stage the water in pores and capillaries of the solid particles is also evaporated. The first stage is relatively fast, whereas the last stage demands more energy and time. The product will be significantly affected by the heat if this drying is carried out in such a way that milk particles are in contact with the hot heat transfer surfaces – as in the case of roller drying. The powder may then contain charred particles which impair its quality. Various uses of milk powder Dried milk is used for many applications, such as: • recombination of milk • mixing into dough in the bakery industry to increase the volume of the bread and improve its water-binding capacity. The bread will then remain fresh for a longer period of time. • mixing into pastry dough to make it crisper • as a substitute for eggs in bread and pastries • producing milk chocolate in the chocolate industry • producing sausages and various types of ready-cooked meals in the food industry and catering trade • as a substitute for mother’s milk in baby foods • production of ice-cream • animal feed Table 17.1 Extra grade skimmilk powder (ADMI* specification for skimmed milk powder) Property Spray dried Roller dried not exceeding not exceeding Milk fat content 1.25 % 1.25 % Moisture content 4.00 % 4.00 % Titratable acidity, l.a. 0.15 % 0.15 % Solubility index 1.25 ml ** 15.00 ml Bacterial estimate 50 000 per gram 50 000 per gram Scorched particles Disc B (15.0 mg) Disc C (22.5 mg) * ADMI = American Dry Milk Institute Inc. (This institution has also published “Standards For Grades of Dry Milks including Methods of Analysis”). ** Except powders designated as “high-heat” (HH), for which the permitted maximum is 2.0 ml. 362 Dairy Processing Handbook/chapter 17
  • 3. Skimmilk powder Skimmilk powder is by far the most common type of milk powder. Each field of application makes its own specific demands on milk pow- der. If the powder is to be mixed with water in recombined milk for con- sumption, it must be easily soluble and have the correct taste and nutritive value. Some degree of caramellisation of the lactose is beneficial in choco- late production. In the first case gentle drying of the product in a spray tower is essential, whereas in the second case the powder must be sub- jected to intense heat treatment in a roller dryer. Two types of powder are therefore distinguishable: 1 roller dried powder 2 spray dried powder Table 17.1 shows an example of the standards applicable to skimmilk powder. The solubility of spray powder is very good, whereas that of roller dried powder is appreciably poorer, on account of the intense heat treat- ment in roller drying. Depending on the intensity of the heat treatment, milk powder is classi- fied into categories related to the temperature/time combinations the skim- milk has been exposed to prior to evaporation and drying. Heat treatment denatures whey proteins, the percentage denaturated increasing with the intensity of heat treatment. The degree of denaturation is normally expressed by the Whey Protein Nitrogen Index (WPNI) as milli- grams of undenatured whey protein (u.w-p) per gram of powder. Information about various categories of spray dried skimmilk powder is summarised in Table 17.2. Table 17.2 Categories of spray dried skimmilk powder. Category Temp/time WPNI mg/g u.w-p Extra low-heat <70°C * Low-heat (LH) powder 70°C/15 s > 6.0 Medium-heat (MH) powder 85°C/20 s 5 – 6.0 ” 90°C/30 s 4 – 5.0 ” 95°C/30 s 3 – 4.0 Medium high-heat (HH) 124°C/30 s 1.5 – 2.0 High-heat (HH) appr. 135°C/30 s <1.4 High-heat high stable (HHHS) appr. 135°C/30 s <1.4 (from selected milk) * Not measurable Table by Sanderson N.Z., J. Dairy Technology, 2, 35 (1967) Whole milk powder Spray dried whole milk powder is nomally produced from fat standardised milk. After standardisation the milk need not be homogenised provided that it is thoroughly agitated, without air inclusion, before evaporation and again between evaporation and spray drying. The concentrate is however hom- ogenised in certain cases for production of instant whole milk. Fat standardised milk for production of roller dried powder is normally homogenised. Whole milk powder, unlike skimmilk powder, is not categorised. Milk intended for whole milk powder is normally pasteurised at 80 – 85°C to inactivate most of the lipolytic enzymes that would otherwise degrade the milk fat during storage. Dairy Processing Handbook/chapter 17 363
  • 4. Instant-milk powder Special methods for the production of both skimmilk and whole milk pow- der with extremely good solubility – known as instant powder – are also available. This powder has a larger grain size, influenced by agglomeration, than normal spray powder and dissolves instantly even in cold water. Bulk density When powders are shipped over long distances it is important that they have a high bulk density to reduce the volume, since in most cases trans- portation costs are calculated by volume. A high bulk density also saves packaging material. However, in some instances the producers may be interested in low bulk density to supply optically larger amounts of powder than that of their competitors. Low bulk density, as influenced by agglomer- ation, is also an important characteristic of instant powders. Definition Bulk density is the weight of a unit volume of powder; in practice it is ex- pressed as g/ml, g/100 ml or g/l. Factors influencing bulk density The bulk density of milk powders is a very complex property; it is the result of several other properties and is influenced by a number of factors. The primary factors determining bulk density are: 1 The particle density, given by : – powder material density – the content of the occluded air inside the particles 2 The content of interstitial air, i.e. the air between the particles. Powder material density The powder material density is given by the composition of the powder. It depends on the contents and densities of the individual components, and can be calculated according formula: 100 %A %B %C + + + etc. + % moisture DA DB DC % A, % B, % C are equivalent to the percentages of the components having densities DA, DB, DC. Occluded air content Milk powder normally contains between 10 and 30 ml of entrapped air per 100 g of powder. There are many factors influencing the occluded air in powder particles. Some of these factors will just be touched upon below: • Incorporation of air into the feed. The concentrate is effectively deaerated by evaporation, but when it is transferred to the spray dryer it may pick up air from leaking pipelines, etc. • The system chosen for spraying the concentrate into the dryer. • The properties of the feed. The amount of air incorporated into the prod- uct depends not only on the intensities of whipping action before or during atomisation, but also on the properties of feed, i.e. the ability of the feed to form stable foam. This property is mainly influenced by the content and state of proteins and the possible presence of whipping inhibitors. Thus concentrates which contain fat are much less prone to foaming than skim- milk. The following factors influence the foaming properties of skimmilk in the drying process: 364 Dairy Processing Handbook/chapter 17
  • 5. • Undenaturated whey proteins have a great tendency to foam; this can be reduced by heat treatment proportional to the degree of denaturation, see Table 17.2. • Concentrates with a low total solids content foam more than highly concentrated feeds. • Cold concentrates are more easily whipped than warm ones. Interstitial air The air content between the particles, the interstitial air, may amount to about 127 ml/100 g of powder. This is a very complex property which de- pends for example on the particle size distribution and the degree of ag- glomeration. Production of milk powder In the production of roller dried powder, the pre-treated milk is admitted to the roller dryer and the whole drying process takes place in one stage. In the production of spray dried powder, the milk is first evaporated un- der vacuum to a DM content of about 45 – 55%. Spray dried skimmilk powder is manufactured in two basic qualities: • ordinary product and • agglomerated product (instant milk powder) by various spray drying systems. Following both roller and spray drying, the powder is packed in cans, paper bags, laminated bags or plastic bags, depending on the quality and the requirements of the consumers. Raw material Very strict demands are made on the quality of the raw material for produc- tion of milk powder. Table 17.1 shows that the number of bacteria per gram of powder must not exceed 50 000, or even 30 000 in some countries. This corresponds to about 5 000 (or 3 000) bacteria per litre of reconstituted product, provided that no reinfection occurs. Since spray powder produc- Strict demands are made on tion involves vacuum evaporation, it is just as important as in the production the quality of the raw material of condensed milk to keep heat-resistant bacteria under control so that they for production of milk powder. will not multiply during evaporation. Bactofuge treatment or microfiltration is therefore also used in powder production to remove bacteria spores from the milk, thereby improving the bacteriological quality of the end product. Milk for powder production must not be subjected to excessive, intense heat treatment prior to delivery to the milk powder plant. Such heat treat- ment would cause the whey protein to coagulate, and the solubility, aroma and taste of the milk powder would be impaired. The milk is subjected to the peroxidase test or the whey protein test to determine whether the pre- ceding heat treatment was too intense. Both of these tests indicate whether or not the milk was previously pasteurised at a high temperature. General pre-treatment of the milk In the production of skimmilk powder the milk is clarified in conjunction with fat separation. This is also the case if the fat content is standardised in a direct standardisation system. Standardised milk used for producing whole milk powder is not normally homogenised unless it is to be roller dried. Skimmilk intended for powder production must be pasteurised at least to a negative phosphatase test. In the production of dried whole milk the heat treatment must be so intense that the lipases will also be inactivated. This normally involves high-temperature pasteursation to a negative peroxidase test. Dairy Processing Handbook/chapter 17 365
  • 6. Roller or drum drying In roller drying the milk is distributed on rotating, steam-heated drums. The water in the milk evaporates and is drawn off by a flow of air when it comes in contact with the hot drum surface. The high temperature of the heating surfaces converts the protein to a form which is not easily soluble and which discolours the product. Intense heat treatment increases the water-binding properties of the powder. This characteristic is useful in the prepared-food industry. The distinction between trough-fed and spray-fed roller dryers is based on the manner in which the milk is fed on to the drums. Figure 17.1 shows the principle of the trough-fed roller dryer. The pre- treated milk is admitted to a trough formed by the cast iron drums and their end walls. A thin layer of milk on the drums is heated quickly when it comes in contact with the hot surface. The water is evaporated and the layer of milk on the drum dries. This film is continuously scraped off by knives in contact with the periphery of each drum. The dried milk falls into a screw conveyor in which it is ground into flakes. The flakes are then transferred to a grinder, and hard and burned particles Fig. 17.1 Principle of the trough-fed are separated on a screen at the same time. roller dryer. Depending on capacity, the double roller dryer is 1 – 6 m long and has a Milk drum diameter of 0.6 – 3 m. The size depends on film thickness, tempera- Heating medium ture, drum speed and the required DM content of the dried product. Air for pneumatic The thickness of the dry layer can be varied by adjusting the gap be- transportation and cooling tween the drums. Figure 17.2 shows the principle of the spray-fed roller dryer. Nozzles above the drums spray a thin film of pre-treated milk on the hot surfaces of the drums. In this arrangement almost 90% of the heat transfer area is utilized, as opposed to less than 75% in the trough-fed dryer. The film thickness is determined by the supply pressure to the spray nozzles. The drying time can also be controlled by adjusting the tempera- ture and the speed of the drums. This provides some scope for controlling the characteristics of the powder. If the parameters are correct, the milk film should be almost dry when it is scraped off the drums. The dry film scraped off the drums is subjected to the same treatment as for the trough-fed dryer. Spray drying Spray drying is carried out in two phases. In the first phase the pre-treated milk is evaporated to a DM content of 45 – 55%. In the second phase the concentrate is pumped to a drying tower for final drying. This process takes place in three stages: • Dispersion of the concentrate into very fine droplets. • Mixing of the finely dispersed concentrate into a stream of hot air which Fig. 17.2 Principle of the spray-fed quickly evaporates the water. roller dryer. • Separation of the dry milk particles from the drying air. Milk Evaporation is a necessary production stage for high-quality powder. With- Heating medium out prior concentration the powder particles will be very small and will have Air for pneumatic a high air content, poor wettability and a short shelf life. The process will transportation and cooling then also be uneconomical. Falling-film evaporators are generally used for concentration, which is carried out in two or more stages to a DS content of 45 – 55%. The equip- ment is the same as that used in the production of condensed milk. Basic drying installations Single-stage drying The most simple installation for making ordinary powder is the spray dryer with a pneumatic conveying system, figure 17.3. This system works on the single-stage drying principle, which means 366 Dairy Processing Handbook/chapter 17
  • 7. 3 5 4 8 Fig. 17.3 Conventional spray dryer (one-stage drying) with conical base chamber. 1 Drying chamber 1 2 Air heater 3 Milk concentrate tank 4 High pressure pump 5 Atomiser 6 Main cyclone 7 Transport system cyclone 8 Air suction fans and filters 7 6 Milk 2 Air Powder that all removal of moisture from the concentrate to the required final mois- ture content takes place in the spray drying chamber (1). The subsequent pneumatic conveying system serves only to collect the powder leaving the chamber cone together with the powder fraction separated from the ex- haust air in the main cyclone (6), to cool the powder and feed it via the final cyclone (7) to the bagging-off hopper. Two-stage drying In a two-stage drying system producing the same type of powder as the previously mentioned installation, the pneumatic conveying system is re- Percentage of initial value placed by a fluid bed dryer, the working principle of which is discussed 100 below under the heading “Operating principle of spray drying”. 90 D 80 Three-stage drying 70 Three-stage drying is an extension of the two-stage concept developed to achieve even greater savings in plant operation costs. 60 W 50 V Operating principle of spray drying 40 30 Single-stage drying 4% H20 20 Figure 17.3 shows the arrangement of a single-stage drying plant. The milk concentrate is fed to the drying chamber (1) by a high-pressure pump (4), 10 and then continues to the atomiser (5). The very small milk droplets are 0 sprayed into the mixing chamber, where they are mixed with hot air. 45 50 60 70 80 90 100 Air is drawn in by a fan through a filter and supplied to a heater (2), Droplet solid content (%) where it is heated to 150 – 250°C. The hot air flows through a distributor to a mixing chamber. In the mixing chamber the atomised milk is mixed thor- Fig. 17.4 Weight, volume and diameter oughly with the hot air and the water in the milk is evaporated. Most of the decrease of droplet under ideal drying drying takes place as the droplets are decelerated by air friction following conditions down to 4% H2O. release from the atomiser at high velocity. The free water evaporates instan- D = Diameter taneously. The water in the capillaries and pores must first diffuse to the W = Weight surfaces of the particles before it can be evaporated. This takes place as V = Volume the powder slowly settles in the spray tower. The milk is only heated to 70 – 80°C because the heat content of the air is continuously consumed by evaporation of water. Dairy Processing Handbook/chapter 17 367
  • 8. Loss of water from the droplets leads to a considerable reduction in weight, volume and diameter. Under ideal drying conditions, weight will decrease to about 50%, volume to about 40%, and the diameter to about 75% of the droplet size produced by release from the atomiser, figure 17.4. During the drying process the milk powder settles in the drying chamber and is discharged at the bottom. It is conveyed pneumatically to the pack- ing section by cooling air which is drawn into the conveyor duct by a fan. After cooling, the mixture of cooling air and powder flows to the discharge unit (7), where the powder is separated from the air before being packed. Some small, light particles may be mixed with the air that leaves the drying chamber. This powder is separated in one or more cyclones (6, 7). After separation the powder is returned to the main stream of milk powder on the way to packing. The cleaned drying air is extracted from the plant by a fan. Milk atomising The more finely dispersed the milk droplets, the larger their specific area will be and the more effective the drying. One litre of milk has a surface area of about 0.05 m2. If this quantity of milk is atomised in the spray tower, each of the small droplets will have a surface area of 0.05 – 0.15 mm2 . The total surface area of all the milk droplets from the original litre of milk will be about A 35 m2. Atomising thus increases the specific area about 700 times. The design of the atomising equipment depends on the particle size and the properties required of the dried product. These properties can be granularity, texture, solubility, density and wettability. Certain dryers have stationary nozzles, see figure 17.5. The arrangement in figure 17.5 A is used in low spray towers and is located so that the relatively large milk droplets B will be discharged in counterflow in relation to the drying air. A stationary nozzle which discharges the milk in the same direction as the air flow is shown in figure 17.5 B. In this case the milk feed pressure determines the particle size. At high feed pressures (up to 30 MPa or 300 bar) the powder will be very fine and have a high density. At low pressures (20 – 5 MPa or 200 – 50 bar) the particle sizes will be larger and there will be no dust-size particles. Figure 17.6 shows another very common type of atomiser, consisting of a rotating disc with passages from which the milk is ejected at high velocity. In this case the properties of the product are controlled by the speed of rotation of the disc. It can be varied between 5 000 and 25 000 r/min. Two-stage drying The last traces of moisture are the most difficult to remove, unless high Fig. 17.5 Stationary nozzles for atomis- outlet drying temperatures are used to provide a sufficient driving force. As ing the milk in a spray drying chamber. elevated outlet drying temperatures can have a detrimental effect on pow- A Counterflow nozzle der quality, it is essential to operate at lower outlet temperatures with dairy B Nozzle discharging in the direction of the air flow products. If the moisture content of the resulting powder is still too high, an after-drying stage is incorporated after the spray dryer in a two-stage proc- ess as illustrated in figure 17.7. Two-stage drying methods for producing powdered milk product com- bine spray drying as the first stage and fluid bed drying as the second stage. The moisture content of the powder leaving the chamber is 2 – 3 per cent higher than the final moisture content. The function of the fluid bed dryer is to remove excess moisture and finally to cool the powder down. Drying of milk in two stages was originally developed to obtain agglomer- ated powders in straight-through processing, but in the early seventies was adopted for non-agglomerated powders so that the advantage of product quality improvement could be combined with the better process economy Fig. 17.6 Rotating disc for atomising milk in the spray drying chamber. of two-stage processing. The powder from both single-stage and two-stage installations consists predominantly of single particles; it is dusty and difficult to reconstitute. There are however some slight differences. Two-stage dried powder is coarser due to bigger primary particles and the presence of some agglom- 368 Dairy Processing Handbook/chapter 17
  • 9. erates. Consequently it is not so dusty and can be reconstituted more easi- ly. However, the biggest difference between these two powders is in the properties that are influenced by heat exposure during drying. The properties in question are the solubility index and the content of occluded air, both lower, and bulk density, which is higher. The droplet temperature just after atomisation is low, just slightly above the wet bulb temperature of the drying air. The particle temperature increases gradually with progressive water removal, finally achieving a temperature which is below the outlet air temperature – how much lower depends on the mois- ture content of the particles. The one-stage and two-stage drying systems are compared in table 17.3. 2 Milk Heating medium Powder 3 1 4 Fig. 17.7 Spray dryer with fluid bed attachment (two-stage drying). 1 Indirect heater 5 2 Drying chamber 3 Vibrating fluid bed 7 4 Heater for fluid bed air 6 5 Ambient cooling air for fluid bed 6 Dehumidified cooling air for fluid bed 7 Sieve Three-stage drying The three-stage dryer involves transfer of the second drying stage into the base of the spray drying chamber and having the final drying and cooling conducted in the third stage located outside the drying chamber. There are two main types of three-stage dryers: 1 Spray dryers with integrated fluid bed 2 Spray dryers with integrated belt The principle of the second type, spray dryers with integrated bed, will be touched upon below. The Filtermat type of dryer is shown in figure 17.8. It consists of a main drying chamber (3) and three smaller chambers for crystallisation (when required, e.g. for production of whey powder), final drying and cooling (8,9, 10). The product is atomised by nozzles located in the top of the main cham- ber of the dryer. The feed is conveyed to the nozzles by a high pressure pump. Atomisation pressure is up to 200 bar. Most of the drying air is sup- plied to the drying chamber around the individual nozzles at temperatures up to 280°C. Primary drying of the droplets takes place as they fall from the nozzles (2) to the moving belt (7) located at the base of the chamber. The powder is deposited on the belt in an agglomerated porous layer. The second drying stage takes place as drying air is sucked through the Dairy Processing Handbook/chapter 17 369
  • 10. Table 17.3 Comparison of one-stage and two-stage drying systems. Drying system One-stage Two-stage Inlet temp. Inlet temp. Inlet temp. 200°C 200°C 230°C Spray dryer (First stage) Evaporation in chamber, kg/h 1 150 1 400 1 720 Powder from chamber: 6 % moisture, kg/h – 1 460 1 790 3.5% moisture, kg/h 1 140 – – Energy consumption, spray drying total, Mcal 1 818 1 823 2 120 Energy/kg powder, kcal 1 595 1 250 1 184 Fluid Bed (Second Stage) Drying air, kg/h – 3 430 4 290 Inlet air temperature, °C – 100 100 Fig. 17.8 Spray dryer with integrated Evaporation in fluid bed, kg/h – 40 45 belt, Filtermat (three-stage drying). Powder from fluid bed 1 High pressure feed pump 3.5 % moisture, kg/h – 1 420 1 745 2 Nozzle arrangement Energy consumption, kW – 20 22 3 Primary drying chamber Energy consumption, 4 Air filters total in fluid bed, Mcal – 95 115 5 Heater/cooler 6 Air distributor Total plant 7 Belt assembly Energy consump. total, Mcal 1 818 1 918 2 235 8 Retention chamber Energy/kg powder total, kcal 1 595 1 350 1 280 9 Final drying chamber Energy relation 100 85 80 10 Cooling chamber 11 Powder discharge Basis: Same drying chamber size with inlet air flow = 31,500 kg/h. 12 Cyclone arrangement Product: skimmilk, 48% solids in concentrate. 13 Fans Source: Evaporation, Membrane Filtration, Spray Drying - North European Dairy Journal, 1985 Copenhagen, Denmark. ISBN No. 87-7477-000-4. 14 Fines recovery system 15 Sifting system 16 Heat recovery system 2 5 5 13 4 6 16 5 13 1 3 8 9 10 7 11 13 12 14 15 Concentrated milk Milk powder Heating air 370 Dairy Processing Handbook/chapter 17
  • 11. powder layer. The moisture content of the powder falling on the belt (7) is 12 – 20 % depending upon the type of product. This second drying stage on the belt reduces the moisture content to 8-10 %. The moisture content is very important to achieving the exact degree of agglomeration of the product and porosity of the powder layer. The third and last drying stage for skimmilk and whole milk concentrates takes place in two chambers (8, 9), where hot air at an inlet temperature of up to 130°C is sucked through the powder layer and the belt in the same way as in the main chamber. The powder is cooled in a final chamber (10). Chamber (8) is used in cases where crystallisation of lactose is required (whey powder). In this case air is not conveyed to the chamber, so the moisture content remains at a higher level, up to 10 %. The third drying stage takes place in chamber (9), and cooling air is supplied to chamber (10). Only a small amount of powder leaves the plant together with the drying and cooling air as fines. This powder is separated from the air in a cyclone battery (12). The powder is recirculated, either to the main chamber or to a point in the process appropriate to the type of product and the agglomera- tion required. After leaving the dryer the powder agglomerates are broken down to the required size in a sifter (15) or milled, depending on the type of product. Production of instant powder Milk powder which will dissolve quickly in water must be instantised, i.e. the milk particles must be treated so that they form larger, porous agglomer- ates. To obtain the correct porosity the milk particles must first be dried so that most of the water in the capillaries and pores is replaced by air. The particles must then be humidified, so that the surfaces of the particles swell quickly, closing the capillaries. The surfaces of the particles will then be- come sticky and the particles will adhere to form agglomerates. One method of producing instantised powder is to recirculate the dry Fig. 17.9 Rotating disc designed for milk particles back to the mixing chamber containing drying air and atom- production of instantised powder. ised milk particles, figure 17.9. As soon as the dry particles are admitted to the chamber, their surfaces are humidified by the evaporated water and the particles swell. The capillaries and pores close and the particles become sticky. Other milk particles adhere to the surface and agglomerates are formed. Fluid-bed drying More efficient instantisation can be obtained with a fluid bed of the type shown in figure 17.10. The fluid bed is connected to the bottom of the drying chamber and consists of a casing with a perforated bottom. The casing is spring mounted and can be vibrated by a motor. When a layer of powder is distributed on the perforated bottom, the vibrations convey the powder at uniform speed along the length of the casing. The powder from the drying chamber is admitted to the first section, Fig. 17.10 Fluid bed for instantising milk powder. Milk powder Steam Hot air Cold air Dairy Processing Handbook/chapter 17 371
  • 12. where it is humidified by steam. The vibrations convey the powder through the drying sections, where air at a gradually decreasing temperature is ad- mitted through the powder bed. Agglomeration takes place in the first stage of drying when the particles adhere to each other. Water is evaporated from the agglomerates during their passage through the drying sections. They will have attained the required dryness when they have passed through the fluid-bed casing. Any larger particles at the outlet of the dry bed are screened and recircu- lated to the inlet. The screened and instantised particles are conveyed by the cooling air to a battery of cyclones, where they are separated from the air and packaged. The drying air from the fluid bed, together with the air from the spray tower, is then blown to the cyclone for recovery of milk particles. Heat recovery A large amount of heat is lost in the drying process. Some can be recov- ered in heat exchangers, but the drying air contains dust and vapour and therefore requires specially designed exchangers. In several cases a special type of heat exchanger with glass pipes is used, see figure 17.11. The smooth glass surface prevents fouling to a great extent. A CIP system is included in the plant. The warm air is introduced from the bottom and forced through the glass pipes. The fresh air to be heated flows on the outside of the pipes. With this method of heat recovery the efficiency of the spray drying plant can be increased by 25 – 30%. A further possibility is to recover the heat in the condensate from the evaporation plant. The plant operates in parallel with the spray drying plant, and such a solution is therefore feasible with savings of 5—8% of the drying costs. 2 4 Fig. 17.11 Heat recovery from effluent air in a spray drying plant. 1 Fan for fresh air 2 Glass pipe heat exchanger 3 Heater 3 4 Spray tower 5 Cyclones 6 Fan for effluent air 1 6 5 Packing milk powder The types and sizes of packages vary widely from one country to another. The powder is often packed in laminated powder bags with an inner bag of polyethylene. The polyethylene bag is often welded, and this package is practically as airtight as sheet-metal drums. The most common bag sizes are 25 and 15 kg, although other sizes are also used as it is very easy to vary the weight of the powder in the bags to meet specific customer re- quirements. Milk powder for households and similar small-scale consumers is packed in tin cans, laminated bags or plastic bags which, in turn, are packed in cartons. 372 Dairy Processing Handbook/chapter 17
  • 13. Changes in milk powder during storage The fat in whole milk powder oxidises during storage. On an industrial scale the shelf life can be extended by special pretreatment of the milk, by the addition of anti-oxidants and, in the case of sheet-metal drums, by filling under inert gas. Milk powder should be stored under cool conditions and protected against contact with water during storage. All chemical reactions in milk powder, at room temperature and with a low water content, take place so slowly that the nutritive value is not affected even after years of storage. Dissolving milk powder One part of ordinary spray-dried powder is mixed with about ten parts of water at a temperature of 30 – 50°C. The dissolving time is about 20 – 30 minutes. Longer times are needed at lower temperatures. 8 – 12 hours are required if the powder is to be dissolved in cold water. If instantised powder is used, the required quantity of water is poured into a tank and the powder is then added. The powder dissolves after very brief stirring, even if the water is cold. The milk is then immediately ready for drinking. The water quality is very important at dissolving. It must be borne in mind that at drying including the first concentration phase (evaporation), the milk has been rid of pure (distilled) water. More about the water quality in chapter 18, Recombined milk products. Dairy Processing Handbook/chapter 17 373
  • 14. 374 Dairy Processing Handbook/chapter 17