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Ac conductivity study of polyaniline ni cufe2o3 composites
1.
International Journal of
Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 10-12 © IAEME INTERNATIONAL JOURNAL OF MECHANICAL ENGINEERING AND TECHNOLOGY (IJMET) ISSN 0976 – 6340 (Print) ISSN 0976 – 6359 (Online) Volume 5, Issue 11, November (2014), pp. 10-12 © IAEME: www.iaeme.com/IJMET.asp Journal Impact Factor (2014): 7.5377 (Calculated by GISI) www.jifactor.com 10 IJMET © I A E M E AC CONDUCTIVITY STUDY OF POLYANILINE / NiCuFe2O3 COMPOSITES Divakar S.J1, Sangshetty Kalyane2 1Department of Physics, Singhania University, Pacheri Bari Jhunjhunu, Rajastan, India 2Department of Physics, BKIT, Bhalki, Karnataka, India ABSTRACT The PANI/ NiCuFe2O3 composites have been synthesized by Insitu polymerization of aniline in the presence of NiCuFe2O3 by chemical oxidation method with various compositions viz., 10, 30, and 50 Wt. % of NiCuFe2O3 in PANI. The AC conductivity was studied in the frequency range 102– 107 Hz. The dimensions of NiCuFe2O3 particles in the matrix have a greater influence on the conductivity values. Keywords: AC conductivity, Polyaniline, NiCuFe2O3, Composites. 1. INTRODUCTION Polymers have become increasingly attractive because of its large number of applications inapplied and basic science. Conductive polymer composite (CPC) materials result from the mixture of conductive particles dispersed in an insulating phase. The filler is usually a metal powder, carbonblack, fiber of carbon black, metal fibers, etc and the insulating phase can be a thermosetting resin, thermoplastic, elastomer, etc. The composite material combines both the intrinsic properties of the fillers (mechanical, electrical, magnetic, and thermal) and of the matrix (elasticity, easy to manipulate, low cost). The various conductive properties of CPC have allowed them to find a variety of industrial applications. They are used, for example, as protection devices against electromagnetic radiation and for the dissipation of electrostatic discharge, and in microelectronics as electrical conductive adhesive for electrical connections. The control of the conductivity of CPC is also interesting for applications including sensor, electrochemical actuators, electromagnetic shielding, polymeric batteries etc. The conductivity of these composites depends strongly on the nature and interaction of the filler with the polymeric matrix [1-6]. Therefore mixed ferrites (NiCuFe2O3) was selected as filler due to its interesting electrical properties, this paper emphasize on the effect of NiCuFe2O3 addition on transport properties of polyaniline.
2.
International Journal of
Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 10-12 © IAEME 11 2. EXPERIMENTAL All Chemicals used are analytical grade (AR) and were procured, used as received. The monomer aniline was doubly distilled prior to use. Synthesis of Polyaniline / NiCuFe2O3 composites has been carried out by single step in situ polymerization technique. 0.1 mol of aniline was dissolved in 1 M of Hydrochloric acid to form aniline hydrochloride. Fine grinded powder of NiCuFe2O3 is added in the weight percent of 10, 30 and 50 to the above solution with vigorous stirring to keepNiCuFe2O3 suspended in the solution. To this reaction mixture, 0.1 M of oxidizing agent ammonium persulphate [(NH4)2S2O8] in 1 M of Hydrochloric acid was added slowly with continuous stirring for 4-8 hr at 0-50 C to polymerize. The precipitated powder was recovered, vacuum filtered and washed with deionised water. Finally, the resultant precipitate was dried in an oven for 24 hr to achieve constant weight. In this way, three different PANI /NiCuFe2O3 composites with different weight of NiCuFe2O3(10, 30 and 50) in PANI have been synthesized [7-11]. 2.1 Preparation of pallets The pellets of 10 mm diameter are formed with thickness varying upto 2 mm by applying pressure of 10 Tons in a UTM – 40 (40 Ton Universal testing machine). For conductivity measurement, In this experiment, three different samples of each composite varying in their weight percentage are investigated for their frequency dependent Dielectric constant. 3. RESULTS AND DISCUSSIONS Figure 1 shows the variation of ac conductivity as a function of frequency for polyaniline – NiCuFe2O3 composites (different wt %). In all the cases, it is observed that, the ac conductivity is quite low for lower frequency and increases with increase in applied frequency but 30wt% of composite shows maximum value. The observed behavior may be due to Debye like relaxation mechanism taking place in all these materials. 0 .0 5 .0 x 1 0 6 1 .0 x 1 0 7 1 .5 x 1 0 7 2 0 1 8 1 6 1 4 1 2 1 0 8 6 4 2 0 -2 F r e q u e n c y (H z ) ( S/cm) s ac 1 0 % P C U F 3 0 % P C U F 5 0 % P C U F Figure 1: Variation of ac conductivity as a function of frequency for Polyaniline- NiCuFe2O3
3.
International Journal of
Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 10-12 © IAEME 12 4. CONCLUSION Polyaniline composites with different weight percentages of NiCuFe2O3 in PANI were synthesized by chemical oxidative polymerization of monomer aniline. The results of ac conductivity show a strong dependence on the weight percent of NiCoFe2O3 in polyaniline. REFERENCES [1]. Kumar, G. N. H.; Rao, J. L.; Gopal, N. O.; Narasimhulu, K. V.;Chakradhar, R. P. S.; Rajulu, A. V. Polymer 2004, 45, 5407. [2]. Michaeli, W.; Pfefferkorn, T. G., PolymEngSci 2009, 49, 1511. [3]. Bard, W. S.; Pakade, S. V.; Yawale, S. P. J Non-Cryst Solids 2007, 353, 1460. [4]. Bhargav, P. B.; Mohan, V.; Sharma, A. K.; Rao, V. V. R. CurrentApplPhys 2009, 9, 165. [5]. Abdelaziz, M.; Abdelrazek, E. M. Phys B 2004, 349, 84. [6]. Mott, N. F.; Davis, E. A. Electronic processes in nanocrystalline materials; Clarendon Press: Oxford, UK, 1979. [7]. Tkaczyk, S. W.; Kityk, I. V.; Schiffer, R. J Phy D Appl Phys 2002, 35, 563. [8]. Prakash, R. S.; Marimuthu, R.; Mandale, A. B. Polymer 2001, 42, 261. AQ5 [9]. Anilkumar, K. R.; Parveen, A.; Badiger, G. R.; AmbikaPrasad,M. V. N. Physica B 2009, 404, 1664. [10]. Sangshetty Kalyane, Magnetic properties study of polyaniline-CeO2 composites at X-Band frequency. Deccan Journal of Chemistry.Vol.1, Issue-2, July 2014.p. 29-31. [11]. SangshettyKalyane, Permeability study of Pani-Dy2O3 Composites in X-Band Frequency. Deccan Journal of Chemistry. Vol.1, Issue-2, July 2014, p. 33-35. [12]. K C Sajjan, Muhammad Faisal, Khened B.S and Syed Khasim, “Humidity Sensing Properties of Polyaniline/Potassium Molybdate Composites”, International Journal of Electrical Engineering Technology (IJEET), Volume 4, Issue 2, 2013, pp. 179 - 186, ISSN Print: 0976-6545, ISSN Online: 0976-6553. [13]. A.M.Bhavikatti, Dr.Subhash Kulkarni and Dr. Arunkumar, “Electromagnetic Studies on Nano-Sized Magnesium Ferrite”, International Journal of Electronics and Communication Engineering Technology (IJECET), Volume 2, Issue 2, 2011, pp. 8 - 15, ISSN Print: 0976- 6464, ISSN Online: 0976 –6472. [14]. T. K. Vishnuvardhan, V. R. Kulkarni, C. Basavaraja, S C Raghavendra, M Revanasiddappa, Ambika Prasad Mvn and Do Sung Hu, “Synthesis Characterization and Study of Dielectric Properties of Conducting Co-Polymer of Panippy-Y2o3 Nanocomposites”, International Journal of Advanced Research in Engineering Technology (IJARET), Volume 4, Issue 6, 2013, pp. 278 - 287, ISSN Print: 0976-6480, ISSN Online: 0976-6499.
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