Al6061 Nanoindentation results

1. Al6061 NI results
NIST Project
Ali Khosravani
Jordan Weaver

3. 4
5
6
7
8
-3
x 10
50
55
60
65
0.6
0.5
0.4
0.3
0.2
0.1
0
-0.1
70
Fit4 Average Abs Residual
E
eff
h-change
Fit4 Max Abs Residual
0.023
0.022
0.021
0.02
0.019
0.018
0.017
0.016
0.015
0.014
Aged at 400F for 2hrs_ 100micron tip_001

4. AR_ 100micron tip_ test 001
40
20
0
65 70 75 80
Modulus [GPa]
40
20
0
0.96 0.98 1 1.02
R2
40
20
0
40 60 80 100
Modulus Length [#points]
40
20
0
-0.7 -0.6 -0.5 -0.4 -0.3
H
r
[nm]
50
0
0.009 0.01 0.011 0.012 0.013
Fit1 Avg.Abs.Res.
40
20
0
0.02 0.03 0.04 0.05 0.06
Fit1 Max.Abs.Res.
40
20
0
0.1 0.11 0.12 0.13
Fit2 Avg.Abs.Res.
40
20
0
0.25 0.3 0.35 0.4 0.45
Fit2 Max.Abs.Res.
50
0
0.5 0.6 0.7 0.8 0.9
h change [nm/nm]
0.4 0.5 0.6 0.7
40
20
0
P change [mN/mN]
6 6.5 7 7.5
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
40
20
0
0.018 0.02 0.022 0.024
Fit4 Max.Abs.Res.
40
20
0
0.2 0.21 0.22 0.23
P* [mN]
40
20
0
18.5 19 19.5
h* [nm]
0 1 2 3
-3
x 10
20
10
0
dP [mN]
40
20
0
-0.2 -0.1 0 0.1 0.2
dH [nm]
effective
sample
Fit1
Fit2
Fit3

5. AR_ 100micron tip_ test 001
Estat =
mean: 74.0953
median: 74.5196
stdev: 1.4504
min: 70.4381
max: 75.9712
Ystat =
mean: 0.5090
median: 0.5134
stdev: 0.0169
min: 0.4678
max: 0.5321
Hstat =
mean: 26.4590
median: 26.6196
stdev: 0.5423
min: 25.0907
max: 27.1902
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=70.4792; Bunge=0, 0, 0; Strength=0.50739; Hardening=26.4099
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
300
250
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 5 10 15
4
x 10
0
-0.5
-1
-1.5
-2
-2.5
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8
8
6
4
2
0
-2
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

6. AR_ 100micron tip_ test 003
40
20
0
66 68 70 72 74 76
Modulus [GPa]
200
100
0
0.95 0.96 0.97 0.98 0.99 1
R2
0 50 100 150
100
50
0
Modulus Length [#points]
100
50
0
-2 -1.5 -1 -0.5 0
H
r
[nm]
0 0.01 0.02 0.03 0.04
100
50
0
Fit1 Avg.Abs.Res.
0 0.05 0.1 0.15 0.2
200
100
0
Fit1 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
100
50
0
Fit2 Avg.Abs.Res.
0 0.5 1 1.5
100
50
0
Fit2 Max.Abs.Res.
0 0.2 0.4 0.6 0.8
100
50
0
h change [nm/nm]
100
50
0
0.1 0.2 0.3 0.4 0.5 0.6
P change [mN/mN]
4 5 6 7 8
-3
x 10
100
50
0
Fit4 Avg.Abs.Res.
100
50
0
0.012 0.014 0.016 0.018 0.02 0.022
Fit4 Max.Abs.Res.
100
50
0
0.2 0.4 0.6 0.8 1
P* [mN]
100
50
0
14 16 18 20 22 24
h* [nm]
0 1 2 3 4
-3
x 10
40
20
0
dP [mN]
100
50
0
-0.6 -0.4 -0.2 0 0.2 0.4
dH [nm]
effective
sample
Fit1
Fit2
Fit3

7. AR_ 100micron tip_ test 003
Estat =
mean: 72.8881
median: 72.7568
stdev: 1.7132
min: 70.0032
max: 75.9966
Ystat =
mean: 0.5726
median: 0.5718
stdev: 0.0247
min: 0.4797
max: 0.6337
Hstat =
mean: 25.9397
median: 25.8888
stdev: 0.6667
min: 24.6468
max: 27.2296
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4139; Bunge=0, 0, 0; Strength=0.58068; Hardening=25.8184
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2 2.5
5
x 10
1
0
-1
-2
-3
-4
-5
-6
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

8. AR_ 100micron tip_ test 004
20
10
0
65 70 75 80
Modulus [GPa]
40
20
0
0.99 0.995 1 1.005
R2
40
20
0
110 120 130 140 150
Modulus Length [#points]
20
10
0
-1.4 -1.2 -1 -0.8 -0.6
H
r
[nm]
40
20
0
0.008 0.01 0.012 0.014
Fit1 Avg.Abs.Res.
40
20
0
0.02 0.04 0.06 0.08
Fit1 Max.Abs.Res.
0.2 0.25 0.3 0.35
40
20
0
Fit2 Avg.Abs.Res.
40
20
0
0.5 1 1.5
Fit2 Max.Abs.Res.
40
20
0
-0.1 0 0.1 0.2 0.3
h change [nm/nm]
0 0.05 0.1 0.15 0.2
20
10
0
P change [mN/mN]
20
10
3.8 4 4.2 4.4 4.6
-3
x 10
0
Fit4 Avg.Abs.Res.
50
0
0.011 0.012 0.013 0.014 0.015
Fit4 Max.Abs.Res.
40
20
0
0.35 0.4 0.45 0.5
P* [mN]
40
20
0
22 22.5 23 23.5 24
h* [nm]
0 1 2 3 4
-3
x 10
20
10
0
dP [mN]
40
20
0
-0.2 0 0.2 0.4 0.6
dH [nm]
effective
sample
Fit1
Fit2
Fit3

9. AR_ 100micron tip_ test 004
Estat =
mean: 72.9264
median: 72.7957
stdev: 1.7328
min: 70.0236
max: 75.9430
Ystat =
mean: 0.5620
median: 0.5603
stdev: 0.0253
min: 0.5206
max: 0.6081
Hstat =
mean: 25.3096
median: 25.2949
stdev: 0.6958
min: 24.1726
max: 26.5177
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=69.3459; Bunge=0, 0, 0; Strength=0.55924; Hardening=25.3294
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
1
0
-1
-2
-3
-4
-5
-6
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

10. AR_ 100micron tip_ test 005
20
10
0
66 68 70 72 74 76
Modulus [GPa]
100
50
0
0.95 0.96 0.97 0.98 0.99 1
R2
40
20
0
20 40 60 80 100 120
Modulus Length [#points]
50
0
-0.7 -0.6 -0.5 -0.4 -0.3
H
r
[nm]
4 6 8 10
-3
x 10
50
0
Fit1 Avg.Abs.Res.
100
50
0
0.01 0.02 0.03 0.04 0.05
Fit1 Max.Abs.Res.
100
50
0
0.08 0.1 0.12 0.14 0.16
Fit2 Avg.Abs.Res.
200
100
0
0.25 0.3 0.35 0.4 0.45
Fit2 Max.Abs.Res.
0 0.2 0.4 0.6 0.8
40
20
0
h change [nm/nm]
0 0.1 0.2 0.3 0.4 0.5
40
20
0
P change [mN/mN]
4 5 6 7 8
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
40
20
0
0.016 0.018 0.02 0.022
Fit4 Max.Abs.Res.
50
0
0.25 0.3 0.35 0.4 0.45
P* [mN]
100
50
0
18.5 19 19.5 20 20.5 21
h* [nm]
0 1 2 3 4
-3
x 10
20
10
0
dP [mN]
40
20
0
-0.4 -0.2 0 0.2 0.4
dH [nm]
effective
sample
Fit1
Fit2
Fit3

11. AR_ 100micron tip_ test 005
Estat =
mean: 72.9738
median: 73.0464
stdev: 1.7727
min: 70.0284
max: 75.9751
Ystat =
mean: 0.5677
median: 0.5668
stdev: 0.0264
min: 0.5105
max: 0.6133
Hstat =
mean: 24.2864
median: 24.3030
stdev: 0.6177
min: 23.2218
max: 25.3615
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4103; Bunge=0, 0, 0; Strength=0.56771; Hardening=24.2611
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 5 10 15
4
x 10
0.5
0
-0.5
-1
-1.5
-2
-2.5
-3
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1
10
8
6
4
2
0
-2
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

12. AR_ 100micron tip_ test 006
10
5
0
65 70 75 80
Modulus [GPa]
20
10
0
0.94 0.96 0.98 1
R2
10
5
0
20 30 40 50 60
Modulus Length [#points]
20
10
0
-0.6 -0.5 -0.4 -0.3 -0.2
H
r
[nm]
4 5 6 7
-3
x 10
20
10
0
Fit1 Avg.Abs.Res.
20
10
0
0.005 0.01 0.015 0.02 0.025
Fit1 Max.Abs.Res.
20
10
0
0.08 0.1 0.12 0.14
Fit2 Avg.Abs.Res.
10
5
0
0.2 0.3 0.4 0.5
Fit2 Max.Abs.Res.
20
10
0
-0.5 0 0.5 1
h change [nm/nm]
0 0.2 0.4 0.6 0.8
20
10
0
P change [mN/mN]
4 5 6 7
-3
x 10
20
10
0
Fit4 Avg.Abs.Res.
10
5
0
0.01 0.015 0.02
Fit4 Max.Abs.Res.
20
10
0
0.2 0.25 0.3 0.35 0.4
P* [mN]
20
10
0
10 11 12 13 14
h* [nm]
0 1 2 3 4
-3
x 10
10
5
0
dP [mN]
20
10
0
-0.2 0 0.2 0.4 0.6
dH [nm]
effective
sample
Fit1
Fit2
Fit3

13. AR_ 100micron tip_ test 006
Estat =
mean: 72.7770
median: 72.6317
stdev: 1.6269
min: 70.0297
max: 75.9841
Ystat =
mean: 1.3887
median: 0.5726
stdev: 0.8684
min: 0.4794
max: 2.3706
Hstat =
mean: -20.5747
median: 24.3717
stdev: 46.3225
min: -68.8533
max: 25.6614
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
Ind. Strain
Ind. Stress [GPa]
Es=69.1032; Bunge=0, 0, 0; Strength=0.55979; Hardening=25.303
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
300
250
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 5 10 15
4
x 10
0
-0.5
-1
-1.5
-2
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8
10
8
6
4
2
0
-2
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

14. AR_ 100micron tip_ test 007
20
10
0
65 70 75 80
Modulus [GPa]
40
20
0
0.985 0.99 0.995 1 1.005
R2
20
10
0
90 100 110 120
Modulus Length [#points]
20
10
0
-0.9 -0.8 -0.7 -0.6 -0.5
H
r
[nm]
20
10
0
0.01 0.015 0.02
Fit1 Avg.Abs.Res.
20
10
0
0.03 0.04 0.05 0.06
Fit1 Max.Abs.Res.
0.2 0.25 0.3 0.35
20
10
0
Fit2 Avg.Abs.Res.
0 0.5 1 1.5
20
10
0
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
20
10
0
h change [nm/nm]
0 0.05 0.1 0.15 0.2
20
10
0
P change [mN/mN]
40
20
5.5 6 6.5 7
-3
x 10
0
Fit4 Avg.Abs.Res.
20
10
0
0.016 0.018 0.02 0.022
Fit4 Max.Abs.Res.
20
10
0
0.48 0.5 0.52 0.54 0.56
P* [mN]
20
10
0
18 18.5 19 19.5
h* [nm]
0 2 4 6
-3
x 10
20
10
0
dP [mN]
40
20
0
-0.5 0 0.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

15. AR_ 100micron tip_ test 007
Estat =
mean: 72.2464
median: 71.9764
stdev: 1.6662
min: 70.0129
max: 75.9662
Ystat =
mean: 0.5074
median: 0.5047
stdev: 0.0193
min: 0.4798
max: 0.5531
Hstat =
mean: 25.7443
median: 25.7191
stdev: 0.7086
min: 24.5450
max: 27.1741
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=68.7734; Bunge=0, 0, 0; Strength=0.50939; Hardening=25.8316
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
1
0
-1
-2
-3
-4
-5
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

16. AR_ 100micron tip_ test 009
20
10
0
66 68 70 72 74 76
Modulus [GPa]
40
20
0
0.96 0.97 0.98 0.99 1 1.01
R2
20
10
0
40 60 80 100 120
Modulus Length [#points]
20
10
0
-0.8 -0.6 -0.4 -0.2 0
H
r
[nm]
5 6 7 8 9 10
-3
x 10
20
10
0
Fit1 Avg.Abs.Res.
50
0
0.01 0.02 0.03 0.04 0.05
Fit1 Max.Abs.Res.
20
10
0
0.11 0.12 0.13 0.14 0.15 0.16
Fit2 Avg.Abs.Res.
20
10
0
0.2 0.4 0.6 0.8 1
Fit2 Max.Abs.Res.
10
5
0
-0.05 0 0.05 0.1 0.15 0.2
h change [nm/nm]
0 0.05 0.1 0.15 0.2
10
5
0
P change [mN/mN]
4 5 6 7
-3
x 10
20
10
0
Fit4 Avg.Abs.Res.
10
5
0
0.014 0.016 0.018 0.02 0.022 0.024
Fit4 Max.Abs.Res.
40
20
0
0.25 0.3 0.35 0.4 0.45
P* [mN]
40
20
0
14 15 16 17 18
h* [nm]
0 1 2 3 4
-3
x 10
10
5
0
dP [mN]
40
20
0
-0.4 -0.2 0 0.2 0.4
dH [nm]
effective
sample
Fit1
Fit2
Fit3

17. AR_ 100micron tip_ test 009
Estat =
mean: 72.3650
median: 72.3985
stdev: 1.6707
min: 70.0855
max: 75.9545
Ystat =
mean: 0.6027
median: 0.6021
stdev: 0.0314
min: 0.5364
max: 0.6666
Hstat =
mean: 25.0466
median: 25.0440
stdev: 0.5939
min: 24.1868
max: 26.2760
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=68.8635; Bunge=0, 0, 0; Strength=0.60705; Hardening=25.0446
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
1
0
-1
-2
-3
-4
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5
14
12
10
8
6
4
2
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

18. AR_ 100micron tip_ test 010

19. AR_ 100micron tip_ test 010
Estat =
mean: 72.5138
median: 72.2047
stdev: 1.5804
min: 70.0063
max: 75.9970
Ystat =
mean: 1.1205
median: 1.1902
stdev: 0.2391
min: 0.3946
max: 1.3185
Hstat =
mean: 10.6983
median: 8.5662
stdev: 5.5002
min: 8.2477
max: 27.3548

20. 400F_ 100micron tip_ test 001
40
20
0
66 68 70 72 74 76
Modulus [GPa]
400
200
0
0.95 0.96 0.97 0.98 0.99 1
R2
40
20
0
60 80 100 120
Modulus Length [#points]
40
20
0
-6 -4 -2 0
H
r
[nm]
0 0.05 0.1 0.15 0.2 0.25
100
50
0
Fit1 Avg.Abs.Res.
0 0.2 0.4 0.6 0.8
100
50
0
Fit1 Max.Abs.Res.
0 0.2 0.4 0.6 0.8 1
100
50
0
Fit2 Avg.Abs.Res.
0 1 2 3 4
50
0
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
50
0
h change [nm/nm]
0 0.1 0.2 0.3 0.4
50
0
P change [mN/mN]
100
50
0
0.005 0.01 0.015 0.02
Fit4 Avg.Abs.Res.
40
20
0
0.01 0.02 0.03 0.04 0.05
Fit4 Max.Abs.Res.
0 2 4 6 8
50
0
P* [mN]
0 20 40 60
50
0
h* [nm]
0 0.01 0.02 0.03 0.04 0.05
40
20
0
dP [mN]
40
20
0
-1.5 -1 -0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

21. 400F_ 100micron tip_ test 001
Estat =
mean: 72.7560
median: 72.6725
stdev: 1.7194
min: 70.0141
max: 75.9311
Ystat =
mean: 0.5800
median: 0.5799
stdev: 0.0273
min: 0.5142
max: 0.6424
Hstat =
mean: 25.7733
median: 25.7376
stdev: 0.8190
min: 23.9460
max: 27.7413
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=69.1823; Bunge=0, 0, 0; Strength=0.60068; Hardening=25.4006
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
5
0
-5
-10
6
-1 0 1 2 3
5
x 10
-15
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 4
50
40
30
20
10
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.02 0.04 0.06 0.08 0.1
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

22. 400F_ 100micron tip_ test 002
40
20
0
66 68 70 72 74 76
Modulus [GPa]
200
100
0
0.95 0.96 0.97 0.98 0.99 1
R2
50
0
60 80 100 120
Modulus Length [#points]
50
0
-6 -4 -2 0
H
r
[nm]
0 0.05 0.1 0.15 0.2
100
50
0
Fit1 Avg.Abs.Res.
0 0.2 0.4 0.6 0.8
50
0
Fit1 Max.Abs.Res.
0 0.2 0.4 0.6 0.8 1
100
50
0
Fit2 Avg.Abs.Res.
0 1 2 3 4
50
0
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4 0.5
50
0
h change [nm/nm]
0 0.1 0.2 0.3 0.4
50
0
P change [mN/mN]
100
50
0
0.005 0.01 0.015 0.02
Fit4 Avg.Abs.Res.
40
20
0
0.015 0.02 0.025 0.03 0.035 0.04
Fit4 Max.Abs.Res.
0 2 4 6
40
20
0
P* [mN]
0 10 20 30 40 50
40
20
0
h* [nm]
0 0.01 0.02 0.03 0.04 0.05
40
20
0
dP [mN]
40
20
0
-2 -1 0 1 2
dH [nm]
effective
sample
Fit1
Fit2
Fit3

23. 400F_ 100micron tip_ test 002
Estat =
mean: 72.5480
median: 72.3265
stdev: 1.7056
min: 70.0063
max: 75.9879
Ystat =
mean: 0.6048
median: 0.6052
stdev: 0.0245
min: 0.5445
max: 0.6608
Hstat =
mean: 26.2425
median: 26.1201
stdev: 0.7859
min: 24.9040
max: 28.0767
1.5
1
0.5
0
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
Ind. Strain
Ind. Stress [GPa]
Es=68.8711; Bunge=0, 0, 0; Strength=0.61391; Hardening=25.8814
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
2
0
-2
-4
-6
-8
-10
6
-1 0 1 2 3
5
x 10
-12
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 4
40
30
20
10
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.2 0.4 0.6
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

24. 400F_ 100micron tip_ test 003
20
10
0
65 70 75 80
Modulus [GPa]
100
50
0
0.94 0.96 0.98 1
R2
40
20
0
80 90 100 110 120
Modulus Length [#points]
40
20
0
-4 -3 -2 -1 0
H
r
[nm]
0 0.02 0.04 0.06 0.08
40
20
0
Fit1 Avg.Abs.Res.
0 0.1 0.2 0.3 0.4
40
20
0
Fit1 Max.Abs.Res.
0 0.2 0.4 0.6 0.8
50
0
Fit2 Avg.Abs.Res.
0 1 2 3
40
20
0
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
40
20
0
h change [nm/nm]
0 0.05 0.1 0.15 0.2
100
50
0
P change [mN/mN]
40
20
0
0.005 0.01 0.015
Fit4 Avg.Abs.Res.
40
20
0
0.01 0.02 0.03 0.04
Fit4 Max.Abs.Res.
0 1 2 3 4
20
10
0
P* [mN]
0 10 20 30 40
40
20
0
h* [nm]
0 0.02 0.04 0.06
40
20
0
dP [mN]
20
10
0
-0.5 0 0.5 1 1.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

25. 400F_ 100micron tip_ test 003
Estat =
mean: 73.0235
median: 73.0678
stdev: 1.7908
min: 70.0025
max: 75.9985
Ystat =
mean: 0.5911
median: 0.5877
stdev: 0.0241
min: 0.5384
max: 0.6472
Hstat =
mean: 26.7180
median: 26.7403
stdev: 0.7762
min: 25.1076
max: 28.2214
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.6973; Bunge=0, 0, 0; Strength=0.57997; Hardening=27.0297
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
5
0
-5
-10
-15
6
-2 0 2 4
5
x 10
-20
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 2 4 6
50
40
30
20
10
0
-10
P 2/3
h
Modulus Fit
Data
Elastic
0 0.1 0.2 0.3
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

26. 400F_ 100micron tip_ test 004
20
10
0
66 68 70 72 74 76
Modulus [GPa]
40
20
0
0.97 0.98 0.99 1 1.01
R2
40
20
0
80 90 100 110 120
Modulus Length [#points]
40
20
0
-3.5 -3 -2.5 -2 -1.5 -1
H
r
[nm]
40
20
0
0.02 0.04 0.06 0.08
Fit1 Avg.Abs.Res.
40
20
0
0.05 0.1 0.15 0.2 0.25
Fit1 Max.Abs.Res.
40
20
0
0.2 0.3 0.4 0.5 0.6 0.7
Fit2 Avg.Abs.Res.
1 1.5 2 2.5 3
40
20
0
Fit2 Max.Abs.Res.
0 0.05 0.1 0.15 0.2 0.25
40
20
0
h change [nm/nm]
0 0.05 0.1 0.15 0.2
40
20
0
P change [mN/mN]
4 6 8 10 12
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
40
20
0
0.01 0.015 0.02 0.025 0.03
Fit4 Max.Abs.Res.
40
20
0
0.5 1 1.5 2 2.5 3
P* [mN]
40
20
0
10 15 20 25 30
h* [nm]
0 0.005 0.01 0.015 0.02
40
20
0
dP [mN]
40
20
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

27. 400F_ 100micron tip_ test 004
Estat =
mean: 72.9889
median: 73.1361
stdev: 1.8000
min: 70.0546
max: 75.9991
Ystat =
mean: 0.6103
median: 0.6072
stdev: 0.0260
min: 0.5609
max: 0.6650
Hstat =
mean: 26.9273
median: 26.9275
stdev: 0.7568
min: 25.5735
max: 28.3435
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4253; Bunge=0, 0, 0; Strength=0.6109; Hardening=26.7417
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
2
0
-2
-4
-6
6
-1 0 1 2 3
5
x 10
-8
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3
30
25
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.05 0.1
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

28. 400F_ 100micron tip_ test 005
40
20
0
66 68 70 72 74 76
Modulus [GPa]
100
50
0
0.95 0.96 0.97 0.98 0.99 1
R2
40
20
0
60 80 100 120
Modulus Length [#points]
100
50
0
-4 -3 -2 -1 0
H
r
[nm]
0 0.02 0.04 0.06 0.08 0.1
100
50
0
Fit1 Avg.Abs.Res.
0 0.05 0.1 0.15 0.2 0.25
100
50
0
Fit1 Max.Abs.Res.
0 0.2 0.4 0.6 0.8
100
50
0
Fit2 Avg.Abs.Res.
0 1 2 3 4
40
20
0
Fit2 Max.Abs.Res.
40
20
0
-0.1 0 0.1 0.2 0.3
h change [nm/nm]
0 0.05 0.1 0.15 0.2
40
20
0
P change [mN/mN]
4 6 8 10 12
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
40
20
0
0.01 0.015 0.02 0.025
Fit4 Max.Abs.Res.
0 1 2 3 4
100
50
0
P* [mN]
0 10 20 30 40
100
50
0
h* [nm]
0 0.005 0.01 0.015 0.02
50
0
dP [mN]
40
20
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

29. 400F_ 100micron tip_ test 005
Estat =
mean: 72.4187
median: 72.3209
stdev: 1.5646
min: 70.0299
max: 75.9694
Ystat =
mean: 0.5981
median: 0.5954
stdev: 0.0208
min: 0.5477
max: 0.6574
Hstat =
mean: 25.8628
median: 25.7550
stdev: 0.6907
min: 24.7395
max: 27.5316
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=68.8299; Bunge=0, 0, 0; Strength=0.58431; Hardening=25.9528
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 1 2 3
5
x 10
2
0
-2
-4
-6
-8
-10
-12
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 4
40
30
20
10
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

30. 400F_ 100micron tip_ test 006
20
10
0
66 68 70 72 74 76
Modulus [GPa]
200
100
0
0.95 0.96 0.97 0.98 0.99 1
R2
20
10
0
60 70 80 90 100 110
Modulus Length [#points]
40
20
0
-4 -3 -2 -1 0
H
r
[nm]
0 0.02 0.04 0.06 0.08
40
20
0
Fit1 Avg.Abs.Res.
0 0.05 0.1 0.15 0.2 0.25
40
20
0
Fit1 Max.Abs.Res.
0 0.2 0.4 0.6 0.8
100
50
0
Fit2 Avg.Abs.Res.
0 1 2 3
40
20
0
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4 0.5
100
50
0
h change [nm/nm]
0 0.1 0.2 0.3 0.4
100
50
0
P change [mN/mN]
5 6 7 8 9 10
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
40
20
0
0.015 0.02 0.025 0.03
Fit4 Max.Abs.Res.
0 1 2 3 4
40
20
0
P* [mN]
0 10 20 30 40
40
20
0
h* [nm]
0 0.005 0.01 0.015 0.02
40
20
0
dP [mN]
40
20
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

31. 400F_ 100micron tip_ test 006
Estat =
mean: 72.5387
median: 72.3448
stdev: 1.6706
min: 70.0031
max: 75.9708
Ystat =
mean: 0.6235
median: 0.6197
stdev: 0.0376
min: 0.5521
max: 0.7019
Hstat =
mean: 25.2648
median: 25.1910
stdev: 0.6441
min: 24.1051
max: 26.5741
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
Ind. Strain
Ind. Stress [GPa]
Es=68.9125; Bunge=0, 0, 0; Strength=0.64253; Hardening=25.1394
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 1 2 3
5
x 10
5
0
-5
-10
-15
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 4
40
30
20
10
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

32. 400F_ 100micron tip_ test 007
20
10
0
66 68 70 72 74 76
Modulus [GPa]
40
20
0
0.95 0.96 0.97 0.98 0.99 1
R2
20
10
0
95 100 105 110 115 120
Modulus Length [#points]
20
10
0
-3 -2.5 -2 -1.5 -1
H
r
[nm]
20
10
0
0.02 0.03 0.04 0.05 0.06
Fit1 Avg.Abs.Res.
20
10
0
0.05 0.1 0.15 0.2 0.25
Fit1 Max.Abs.Res.
0.35 0.4 0.45 0.5 0.55 0.6
20
10
0
Fit2 Avg.Abs.Res.
1 1.5 2 2.5 3
20
10
0
Fit2 Max.Abs.Res.
40
20
0
-0.05 0 0.05 0.1 0.15
h change [nm/nm]
0 0.02 0.04 0.06 0.08 0.1
40
20
0
P change [mN/mN]
5 6 7 8 9 10
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
20
10
0
0.015 0.02 0.025 0.03
Fit4 Max.Abs.Res.
20
10
0
0.5 1 1.5 2 2.5
P* [mN]
20
10
0
10 15 20 25
h* [nm]
0 0.005 0.01 0.015 0.02
20
10
0
dP [mN]
20
10
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

33. 400F_ 100micron tip_ test 007
Estat =
mean: 72.5940
median: 72.4691
stdev: 1.6808
min: 70.0073
max: 75.9954
Ystat =
mean: 0.6301
median: 0.6262
stdev: 0.0239
min: 0.5901
max: 0.6833
Hstat =
mean: 24.2083
median: 24.1450
stdev: 0.6232
min: 23.2490
max: 25.4870
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=68.9381; Bunge=0, 0, 0; Strength=0.62268; Hardening=24.145
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 1 2 3
5
x 10
5
0
-5
-10
-15
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 4
50
40
30
20
10
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

34. 400F_ 100micron tip_ test 008
10
5
0
65 70 75 80
Modulus [GPa]
10
5
0
0.94 0.96 0.98 1
R2
10
5
0
70 75 80 85 90
Modulus Length [#points]
20
10
0
-3 -2.5 -2 -1.5 -1
H
r
[nm]
10
5
0
0.03 0.04 0.05 0.06
Fit1 Avg.Abs.Res.
10
5
0
0.08 0.1 0.12 0.14 0.16
Fit1 Max.Abs.Res.
0.35 0.4 0.45 0.5
10
5
0
Fit2 Avg.Abs.Res.
1 1.5 2 2.5
20
10
0
Fit2 Max.Abs.Res.
0 0.05 0.1 0.15 0.2
20
10
0
h change [nm/nm]
0 0.05 0.1 0.15 0.2
40
20
0
P change [mN/mN]
6 8 10 12
-3
x 10
10
5
0
Fit4 Avg.Abs.Res.
10
5
0
0.018 0.02 0.022 0.024 0.026
Fit4 Max.Abs.Res.
10
5
0
1.4 1.6 1.8 2 2.2
P* [mN]
10
5
0
16 18 20 22 24
h* [nm]
0 0.005 0.01 0.015 0.02
10
5
0
dP [mN]
10
5
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

35. 400F_ 100micron tip_ test 008
Estat =
mean: 72.8347
median: 72.7764
stdev: 1.7629
min: 70.0515
max: 75.9819
Ystat =
mean: 0.6153
median: 0.6150
stdev: 0.0243
min: 0.5745
max: 0.6635
Hstat =
mean: 25.5687
median: 25.5641
stdev: 0.6504
min: 24.5436
max: 26.8152
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.3031; Bunge=0, 0, 0; Strength=0.61882; Hardening=25.6051
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
2
0
-2
-4
-6
-8
6
-1 0 1 2 3
5
x 10
-10
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3
40
30
20
10
0
-10
P 2/3
h
Modulus Fit
Data
Elastic
0 0.1 0.2
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

36. 400F_ 100micron tip_ test 009
20
10
0
65 70 75 80
Modulus [GPa]
20
10
0
0.94 0.96 0.98 1
R2
40
20
0
90 100 110 120
Modulus Length [#points]
20
10
0
-2 -1.5 -1 -0.5
H
r
[nm]
40
20
0
0.02 0.03 0.04 0.05
Fit1 Avg.Abs.Res.
20
10
0
0.05 0.1 0.15
Fit1 Max.Abs.Res.
0.35 0.4 0.45 0.5
20
10
0
Fit2 Avg.Abs.Res.
1 1.5 2 2.5
20
10
0
Fit2 Max.Abs.Res.
20
10
0
-0.05 0 0.05 0.1 0.15
h change [nm/nm]
0 0.05 0.1
20
10
0
P change [mN/mN]
4 6 8 10
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
20
10
0
0.015 0.02 0.025 0.03
Fit4 Max.Abs.Res.
20
10
0
0.5 1 1.5 2
P* [mN]
20
10
0
10 15 20
h* [nm]
0 0.005 0.01 0.015 0.02
20
10
0
dP [mN]
40
20
0
0.2 0.4 0.6 0.8 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

37. 400F_ 100micron tip_ test 009
Estat =
mean: 72.7375
median: 72.5867
stdev: 1.7351
min: 70.0108
max: 75.9380
Ystat =
mean: 0.5990
median: 0.5987
stdev: 0.0244
min: 0.5534
max: 0.6502
Hstat =
mean: 25.0370
median: 25.0045
stdev: 0.6484
min: 23.9826
max: 26.3593
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=69.186; Bunge=0, 0, 0; Strength=0.60556; Hardening=25.147
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
300
250
200
150
100
50
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
2
0
-2
-4
-6
-8
6
-1 0 1 2 3
5
x 10
-10
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3
35
30
25
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.2 0.4 0.6 0.8
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

38. 400F_ 100micron tip_ test 010
20
10
0
65 70 75 80
Modulus [GPa]
20
10
0
0.94 0.96 0.98 1
R2
40
20
0
10 20 30 40 50
Modulus Length [#points]
20
10
0
-2 -1.5 -1 -0.5
H
r
[nm]
0 0.02 0.04 0.06
40
20
0
Fit1 Avg.Abs.Res.
0 0.05 0.1 0.15 0.2
20
10
0
Fit1 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
20
10
0
Fit2 Avg.Abs.Res.
20
10
0
0.2 0.4 0.6 0.8 1
Fit2 Max.Abs.Res.
20
10
0
0.5 0.6 0.7 0.8 0.9
h change [nm/nm]
40
20
0
0.4 0.6 0.8 1
P change [mN/mN]
20
10
0
0.006 0.008 0.01 0.012 0.014
Fit4 Avg.Abs.Res.
20
10
0
0.015 0.02 0.025 0.03
Fit4 Max.Abs.Res.
0 0.5 1 1.5
20
10
0
P* [mN]
5 10 15 20 25
20
10
0
h* [nm]
0 0.005 0.01 0.015 0.02
20
10
0
dP [mN]
40
20
0
-1 -0.5 0 0.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

39. 400F_ 100micron tip_ test 010
Estat =
mean: 72.9543
median: 72.9222
stdev: 1.6266
min: 70.0865
max: 75.9163
Ystat =
mean: 0.4556
median: 0.4465
stdev: 0.0448
min: 0.3839
max: 0.5389
Hstat =
mean: 28.2196
median: 28.1243
stdev: 0.8397
min: 26.5468
max: 29.9858
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1.5
1
0.5
0
Ind. Strain
Ind. Stress [GPa]
Es=69.3707; Bunge=0, 0, 0; Strength=0.53241; Hardening=27.4405
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
300
250
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
0
-2
-4
-6
6
0.5 1 1.5 2 2.5
5
x 10
-8
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2 2.5
25
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

40. 525F_ 100micron tip_ test 001
20
10
0
65 70 75 80
Modulus [GPa]
40
20
0
0.94 0.96 0.98 1
R2
40
20
0
80 90 100 110 120
Modulus Length [#points]
20
10
0
-1 -0.8 -0.6 -0.4 -0.2
H
r
[nm]
20
10
0
0.005 0.01 0.015 0.02
Fit1 Avg.Abs.Res.
20
10
0
0.02 0.03 0.04 0.05 0.06
Fit1 Max.Abs.Res.
40
20
0
0.1 0.15 0.2 0.25
Fit2 Avg.Abs.Res.
0.4 0.5 0.6 0.7
20
10
0
Fit2 Max.Abs.Res.
20
10
0
0.2 0.3 0.4 0.5
h change [nm/nm]
0.2 0.25 0.3 0.35
40
20
0
P change [mN/mN]
7 8 9 10
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
40
20
0
0.02 0.025 0.03 0.035 0.04
Fit4 Max.Abs.Res.
40
20
0
0.05 0.1 0.15 0.2 0.25
P* [mN]
3 4 5 6 7
40
20
0
h* [nm]
0 0.5 1 1.5 2
-3
x 10
20
10
0
dP [mN]
40
20
0
-0.6 -0.4 -0.2 0 0.2
dH [nm]
effective
sample
Fit1
Fit2
Fit3

41. 525F_ 100micron tip_ test 001
Estat =
mean: 72.8279
median: 73.1006
stdev: 1.7629
min: 70.0003
max: 75.9999
Ystat =
mean: 0.3439
median: 0.3420
stdev: 0.0158
min: 0.3150
max: 0.3783
Hstat =
mean: 17.3318
median: 17.3867
stdev: 0.4754
min: 16.5865
max: 18.4025
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.2875; Bunge=0, 0, 0; Strength=0.34963; Hardening=17.2816
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
0
-0.5
-1
-1.5
-2
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8 1
10
8
6
4
2
0
-2
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

42. 525F_ 100micron tip_ test 002
40
20
0
66 68 70 72 74 76
Modulus [GPa]
200
100
0
0.95 0.96 0.97 0.98 0.99 1
R2
100
50
0
50 100 150
Modulus Length [#points]
100
50
0
-1.2 -1 -0.8 -0.6 -0.4 -0.2
H
r
[nm]
100
50
0
0.005 0.01 0.015 0.02
Fit1 Avg.Abs.Res.
0 0.02 0.04 0.06 0.08 0.1
200
100
0
Fit1 Max.Abs.Res.
100
50
0
0.1 0.15 0.2 0.25 0.3 0.35
Fit2 Avg.Abs.Res.
200
100
0
0.2 0.4 0.6 0.8 1 1.2
Fit2 Max.Abs.Res.
200
100
0
-0.2 0 0.2 0.4 0.6
h change [nm/nm]
0 0.1 0.2 0.3 0.4
200
100
0
P change [mN/mN]
5 6 7 8 9 10
-3
x 10
100
50
0
Fit4 Avg.Abs.Res.
100
50
0
0.01 0.02 0.03 0.04 0.05 0.06
Fit4 Max.Abs.Res.
100
50
0
0.1 0.2 0.3 0.4 0.5
P* [mN]
6 7 8 9 10 11
100
50
0
h* [nm]
0 0.5 1 1.5 2 2.5
-3
x 10
50
0
dP [mN]
100
50
0
-0.4 -0.2 0 0.2 0.4 0.6
dH [nm]
effective
sample
Fit1
Fit2
Fit3

43. 525F_ 100micron tip_ test 002
Estat =
mean: 73.0168
median: 72.9951
stdev: 1.7580
min: 70.0013
max: 75.9956
Ystat =
mean: 0.3923
median: 0.3923
stdev: 0.0185
min: 0.3468
max: 0.4306
Hstat =
mean: 18.0153
median: 17.8977
stdev: 0.6708
min: 17.0777
max: 19.5268
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4679; Bunge=0, 0, 0; Strength=0.36933; Hardening=18.023
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 500 1000
250
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
0
-0.5
-1
-1.5
-2
-2.5
-3
-3.5
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

44. 525F_ 100micron tip_ test 003
20
10
0
65 70 75 80
Modulus [GPa]
50
0
0.94 0.96 0.98 1
R2
20
10
0
50 100 150
Modulus Length [#points]
20
10
0
-0.9 -0.8 -0.7 -0.6 -0.5
H
r
[nm]
40
20
0
0.005 0.01 0.015
Fit1 Avg.Abs.Res.
40
20
0
0.025 0.03 0.035 0.04 0.045
Fit1 Max.Abs.Res.
40
20
0
0.1 0.11 0.12 0.13
Fit2 Avg.Abs.Res.
0.4 0.5 0.6 0.7
40
20
0
Fit2 Max.Abs.Res.
40
20
0
0.1 0.2 0.3 0.4 0.5
h change [nm/nm]
20
10
0
0.1 0.2 0.3 0.4 0.5
P change [mN/mN]
6 7 8 9 10
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
100
50
0
0.025 0.03 0.035 0.04
Fit4 Max.Abs.Res.
20
10
0
0.12 0.14 0.16 0.18
P* [mN]
20
10
0
4.5 5 5.5 6
h* [nm]
0 0.5 1 1.5 2
-3
x 10
20
10
0
dP [mN]
40
20
0
-1 -0.5 0 0.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

45. 525F_ 100micron tip_ test 003
Estat =
mean: 72.8329
median: 72.6625
stdev: 1.6899
min: 70.0091
max: 75.9662
Ystat =
mean: 0.4241
median: 0.4226
stdev: 0.0182
min: 0.3933
max: 0.4577
Hstat =
mean: 17.1184
median: 17.0781
stdev: 0.4141
min: 16.4184
max: 17.9105
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.3119; Bunge=0, 0, 0; Strength=0.42218; Hardening=17.1288
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
250
200
150
100
50
0
-500 0 500 1000
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
5
0 5 10 15
4
x 10
2
0
-2
-4
-6
-8
-10
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8
5
4
3
2
1
0
-1
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

46. 525F_ 100micron tip_ test 004
30
20
10
65 70 75 80
Modulus [GPa]
200
100
0
0.94 0.96 0.98 1
R2
0 50 100 150
50
0
Modulus Length [#points]
100
50
0
-1.5 -1 -0.5 0
H
r
[nm]
0 0.01 0.02 0.03
100
50
0
Fit1 Avg.Abs.Res.
0 0.02 0.04 0.06 0.08
100
50
0
Fit1 Max.Abs.Res.
100
50
0
0.05 0.1 0.15 0.2 0.25
Fit2 Avg.Abs.Res.
50
0
0.2 0.4 0.6 0.8 1
Fit2 Max.Abs.Res.
50
0
0.2 0.4 0.6 0.8
h change [nm/nm]
50
0
0.1 0.2 0.3 0.4 0.5
P change [mN/mN]
4 6 8 10
-3
x 10
100
50
0
Fit4 Avg.Abs.Res.
100
50
0
0.01 0.02 0.03 0.04
Fit4 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
100
50
0
P* [mN]
6 8 10 12
100
50
0
h* [nm]
0 1 2 3 4
-3
x 10
40
20
0
dP [mN]
100
50
0
-1 -0.5 0 0.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

47. 525F_ 100micron tip_ test 004
Estat =
mean: 72.9655
median: 72.8722
stdev: 1.7495
min: 70.0414
max: 75.9761
Ystat =
mean: 0.3900
median: 0.3888
stdev: 0.0169
min: 0.3590
max: 0.4202
Hstat =
mean: 17.9959
median: 17.9677
stdev: 0.4532
min: 17.2153
max: 18.7965
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1
0.8
0.6
0.4
0.2
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4561; Bunge=0, 0, 0; Strength=0.38674; Hardening=18.0079
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
0
-1
-2
-3
-4
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

48. 525F_ 100micron tip_ test 005
20
10
0
66 68 70 72 74 76
Modulus [GPa]
40
20
0
0.95 0.96 0.97 0.98 0.99 1
R2
40
20
0
70 80 90 100 110 120
Modulus Length [#points]
40
20
0
-1.5 -1 -0.5 0
H
r
[nm]
40
20
0
0.005 0.01 0.015 0.02
Fit1 Avg.Abs.Res.
40
20
0
0.02 0.04 0.06 0.08 0.1
Fit1 Max.Abs.Res.
50
0
0.1 0.15 0.2 0.25 0.3 0.35
Fit2 Avg.Abs.Res.
40
20
0
0.2 0.4 0.6 0.8 1 1.2
Fit2 Max.Abs.Res.
20
10
0
0.2 0.3 0.4 0.5
h change [nm/nm]
0.2 0.25 0.3 0.35
40
20
0
P change [mN/mN]
7 8 9 10
-3
x 10
40
20
0
Fit4 Avg.Abs.Res.
50
0
0.02 0.025 0.03 0.035 0.04
Fit4 Max.Abs.Res.
0 0.1 0.2 0.3 0.4 0.5
50
0
P* [mN]
2 4 6 8 10
40
20
0
h* [nm]
0 1 2 3 4 5
-3
x 10
40
20
0
dP [mN]
40
20
0
-0.6 -0.4 -0.2 0 0.2 0.4
dH [nm]
effective
sample
Fit1
Fit2
Fit3

49. 525F_ 100micron tip_ test 005
Estat =
mean: 72.9610
median: 73.1697
stdev: 1.8039
min: 70.0003
max: 75.9999
Ystat =
mean: 0.3449
median: 0.3440
stdev: 0.0155
min: 0.3150
max: 0.3783
Hstat =
mean: 17.3682
median: 17.4043
stdev: 0.4815
min: 16.5865
max: 18.4025
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4314; Bunge=0, 0, 0; Strength=0.3375; Hardening=17.4237
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
200
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2
5
x 10
0
-0.5
-1
-1.5
-2
-2.5
-3
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

50. 650F_ 100micron tip_ test 002
20
10
0
65 70 75 80
Modulus [GPa]
50
0
0.98 0.99 1 1.01
R2
20
10
0
20 40 60 80
Modulus Length [#points]
20
10
0
-2 -1 0 1
H
r
[nm]
40
20
0
0.08 0.1 0.12 0.14 0.16
Fit1 Avg.Abs.Res.
40
20
0
0.2 0.3 0.4 0.5
Fit1 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
20
10
0
Fit2 Avg.Abs.Res.
0 0.5 1 1.5
20
10
0
Fit2 Max.Abs.Res.
20
10
0
0.7 0.8 0.9 1
h change [nm/nm]
40
20
0
0.4 0.5 0.6 0.7 0.8
P change [mN/mN]
20
10
0
0.02 0.03 0.04 0.05
Fit4 Avg.Abs.Res.
20
10
0
0.04 0.05 0.06 0.07 0.08
Fit4 Max.Abs.Res.
0.8 1 1.2 1.4
20
10
0
P* [mN]
20
10
0
30 35 40 45
h* [nm]
0 0.005 0.01 0.015
20
10
0
dP [mN]
20
10
0
-0.5 0 0.5 1 1.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

51. 650F_ 100micron tip_ test 002
Estat =
mean: 73.0756
median: 72.9917
stdev: 1.6628
min: 70.1255
max: 75.9698
Ystat =
mean: 0.2518
median: 0.2515
stdev: 0.0119
min: 0.2208
max: 0.2790
Hstat =
mean: 12.9052
median: 12.8873
stdev: 0.7722
min: 11.7981
max: 14.2977
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.4988; Bunge=0, 0, 0; Strength=0.25718; Hardening=12.4377
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
140
120
100
80
60
40
20
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 1 2 3
5
x 10
0
-2
-4
-6
-8
-10
-12
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
25
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

52. 650F_ 100micron tip_ test 003

53. 650F_ 100micron tip_ test 003
Estat =
mean: 72.8141
median: 72.5877
stdev: 1.7410
min: 70.0232
max: 75.9629
Ystat =
mean: 0.2503
median: 0.2504
stdev: 0.0100
min: 0.2326
max: 0.2741
Hstat =
mean: 13.3240
median: 13.2591
stdev: 0.4620
min: 12.0619
max: 14.2475
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.2711; Bunge=0, 0, 0; Strength=0.25215; Hardening=13.2591
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 500 1000
150
100
50
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 1 2 3
5
x 10
0
-2
-4
-6
-8
-10
-12
-14
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
25
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.04
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

54. 650F_ 100micron tip_ test 004
10
5
0
65 70 75 80
Modulus [GPa]
40
20
0
0.98 0.99 1 1.01
R2
20
10
0
20 40 60 80
Modulus Length [#points]
20
10
0
-2 -1 0 1
H
r
[nm]
40
20
0
0.1 0.12 0.14 0.16
Fit1 Avg.Abs.Res.
20
10
0
0.25 0.3 0.35 0.4 0.45
Fit1 Max.Abs.Res.
0 0.1 0.2 0.3 0.4
20
10
0
Fit2 Avg.Abs.Res.
0 0.5 1 1.5
20
10
0
Fit2 Max.Abs.Res.
10
5
0
0.75 0.8 0.85 0.9 0.95
h change [nm/nm]
20
10
0
0.4 0.5 0.6 0.7 0.8
P change [mN/mN]
10
5
0
0.02 0.03 0.04 0.05
Fit4 Avg.Abs.Res.
10
5
0
0.045 0.05 0.055 0.06
Fit4 Max.Abs.Res.
10
5
0
0.7 0.8 0.9 1
P* [mN]
10
5
0
54 56 58 60
h* [nm]
0 0.005 0.01
20
10
0
dP [mN]
20
10
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

55. 650F_ 100micron tip_ test 004
Estat =
mean: 72.7263
median: 72.4234
stdev: 1.7910
min: 70.0506
max: 75.9400
Ystat =
mean: 0.2271
median: 0.2261
stdev: 0.0108
min: 0.1959
max: 0.2459
Hstat =
mean: 12.3714
median: 12.0507
stdev: 0.6598
min: 11.5263
max: 13.4687
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.1896; Bunge=0, 0, 0; Strength=0.23049; Hardening=12.0506
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
140
120
100
80
60
40
20
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 1 2 3
5
x 10
0
-2
-4
-6
-8
-10
-12
-14
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
25
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

56. 650F_ 100micron tip_ test 005
10
5
0
65 70 75 80
Modulus [GPa]
40
20
0
0.96 0.98 1 1.02
R2
10
5
0
20 40 60 80
Modulus Length [#points]
10
5
0
-1 -0.5 0 0.5
H
r
[nm]
20
10
0
0.08 0.1 0.12 0.14 0.16
Fit1 Avg.Abs.Res.
20
10
0
0.2 0.25 0.3 0.35 0.4
Fit1 Max.Abs.Res.
10
5
0
0.05 0.1 0.15 0.2 0.25
Fit2 Avg.Abs.Res.
0 0.5 1
20
10
0
Fit2 Max.Abs.Res.
10
5
0
0.75 0.8 0.85 0.9 0.95
h change [nm/nm]
10
5
0
0.4 0.5 0.6 0.7 0.8
P change [mN/mN]
10
5
0
0.025 0.03 0.035 0.04 0.045
Fit4 Avg.Abs.Res.
10
5
0
0.05 0.055 0.06 0.065
Fit4 Max.Abs.Res.
10
5
0
0.55 0.6 0.65 0.7 0.75
P* [mN]
10
5
0
31 32 33 34 35
h* [nm]
0 2 4 6 8
-3
x 10
10
5
0
dP [mN]
10
5
0
-0.5 0 0.5 1
dH [nm]
effective
sample
Fit1
Fit2
Fit3

57. 650F_ 100micron tip_ test 005
Estat =
mean: 73.0497
median: 72.7548
stdev: 1.8111
min: 70.0597
max: 75.9970
Ystat =
mean: 0.2244
median: 0.2263
stdev: 0.0123
min: 0.1897
max: 0.2476
Hstat =
mean: 13.1493
median: 13.0770
stdev: 0.4404
min: 12.2847
max: 13.9221
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.467; Bunge=0, 0, 0; Strength=0.23406; Hardening=12.931
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600
100
80
60
40
20
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2 2.5
5
x 10
0
-2
-4
-6
-8
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

58. 650F_ 100micron tip_ test 006
20
10
0
66 68 70 72 74 76
Modulus [GPa]
40
20
0
0.95 0.96 0.97 0.98 0.99 1
R2
20
10
0
20 25 30 35 40 45
Modulus Length [#points]
20
10
0
-1 -0.5 0 0.5 1
H
r
[nm]
20
10
0
0.1 0.2 0.3 0.4 0.5
Fit1 Avg.Abs.Res.
0 0.5 1 1.5 2
20
10
0
Fit1 Max.Abs.Res.
20
10
0
0.1 0.2 0.3 0.4 0.5 0.6
Fit2 Avg.Abs.Res.
0 0.5 1 1.5 2
20
10
0
Fit2 Max.Abs.Res.
40
20
0
0.75 0.8 0.85 0.9 0.95
h change [nm/nm]
0.65 0.7 0.75 0.8
20
10
0
P change [mN/mN]
20
10
0
0.045 0.05 0.055 0.06 0.065 0.07
Fit4 Avg.Abs.Res.
20
10
0
0.06 0.07 0.08 0.09 0.1 0.11
Fit4 Max.Abs.Res.
0 1 2 3 4 5
20
10
0
P* [mN]
20
10
0
60 70 80 90 100 110
h* [nm]
0 0.01 0.02 0.03
20
10
0
dP [mN]
0 0.5 1 1.5 2 2.5
20
10
0
dH [nm]
effective
sample
Fit1
Fit2
Fit3

59. 650F_ 100micron tip_ test 006
Estat =
mean: 72.5025
median: 72.0208
stdev: 1.7646
min: 70.0303
max: 75.9951
Ystat =
mean: 0.1528
median: 0.1565
stdev: 0.0120
min: 0.1219
max: 0.1704
Hstat =
mean: 14.1212
median: 13.9646
stdev: 0.8057
min: 12.9491
max: 15.8711
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=68.9422; Bunge=0, 0, 0; Strength=0.16582; Hardening=13.5432
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
140
120
100
80
60
40
20
0
-200 0 200 400 600 800
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
7
0 1 2 3 4
5
x 10
0.5
0
-0.5
-1
-1.5
-2
-2.5
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
25
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

60. 775F_ 100micron tip_ test 002
10
5
0
66 68 70 72 74 76
Modulus [GPa]
20
10
0
0.95 0.96 0.97 0.98 0.99 1
R2
10
5
0
30 35 40 45 50 55
Modulus Length [#points]
10
5
0
-1 -0.5 0 0.5 1
H
r
[nm]
20
10
0
0.08 0.1 0.12 0.14 0.16
Fit1 Avg.Abs.Res.
0.3 0.32 0.34 0.36 0.38
20
10
0
Fit1 Max.Abs.Res.
10
5
0
0.1 0.15 0.2 0.25
Fit2 Avg.Abs.Res.
20
10
0
0.2 0.4 0.6 0.8 1
Fit2 Max.Abs.Res.
10
5
0
0.86 0.88 0.9 0.92 0.94
h change [nm/nm]
10
5
0
0.55 0.6 0.65 0.7 0.75
P change [mN/mN]
10
5
0
0.02 0.03 0.04 0.05 0.06 0.07
Fit4 Avg.Abs.Res.
20
10
0
0.04 0.06 0.08 0.1
Fit4 Max.Abs.Res.
10
5
0
0.5 0.6 0.7 0.8 0.9 1
P* [mN]
10
5
0
56 58 60 62 64 66
h* [nm]
0 0.002 0.004 0.006 0.008 0.01
10
5
0
dP [mN]
10
5
0
-0.5 0 0.5 1 1.5 2
dH [nm]
effective
sample
Fit1
Fit2
Fit3

61. 775F_ 100micron tip_ test 002
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.0392; Bunge=0, 0, 0; Strength=0.15987; Hardening=11.39
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
120
100
80
60
40
20
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2 2.5
5
x 10
0
-2
-4
-6
-8
-10
-12
-14
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5
20
15
10
5
0
-5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03
8000
6000
4000
2000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic
Estat =
mean: 72.6774
median: 72.4660
stdev: 1.5328
min: 70.1452
max: 75.7897
Ystat =
mean: 0.1801
median: 0.1808
stdev: 0.0080
min: 0.1588
max: 0.2022
Hstat =
mean: 10.8999
median: 10.8444
stdev: 0.3716
min: 10.1605
max: 11.7637

62. 775F_ 100micron tip_ test 004
10
5
0
66 68 70 72 74 76
Modulus [GPa]
20
10
0
0.96 0.97 0.98 0.99 1 1.01
R2
10
5
0
20 30 40 50 60 70
Modulus Length [#points]
10
5
0
-1.5 -1 -0.5 0 0.5 1
H
r
[nm]
10
5
0
0.1 0.12 0.14 0.16
Fit1 Avg.Abs.Res.
10
5
0
0.25 0.3 0.35 0.4 0.45
Fit1 Max.Abs.Res.
10
5
0
0.1 0.15 0.2 0.25
Fit2 Avg.Abs.Res.
0.4 0.5 0.6 0.7
10
5
0
Fit2 Max.Abs.Res.
4
2
0
0.8 0.85 0.9 0.95 1
h change [nm/nm]
10
5
0
0.5 0.6 0.7 0.8 0.9
P change [mN/mN]
20
10
0
0.02 0.03 0.04 0.05 0.06 0.07
Fit4 Avg.Abs.Res.
20
10
0
0.04 0.05 0.06 0.07 0.08 0.09
Fit4 Max.Abs.Res.
0.7 0.8 0.9 1 1.1
20
10
0
P* [mN]
10
5
0
44 46 48 50 52 54
h* [nm]
0 0.002 0.004 0.006 0.008 0.01
10
5
0
dP [mN]
10
5
0
-1 -0.5 0 0.5 1 1.5
dH [nm]
effective
sample
Fit1
Fit2
Fit3

63. 775F_ 100micron tip_ test 004
Estat =
mean: 72.9440
median: 72.5348
stdev: 1.7310
min: 70.2726
max: 75.8985
Ystat =
mean: 0.1815
median: 0.1793
stdev: 0.0162
min: 0.1483
max: 0.2122
Hstat =
mean: 11.4562
median: 11.0910
stdev: 0.7168
min: 10.4900
max: 12.6142
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04
0.6
0.5
0.4
0.3
0.2
0.1
0
Ind. Strain
Ind. Stress [GPa]
Es=69.1715; Bunge=0, 0, 0; Strength=0.18232; Hardening=10.8001
Stress-Strain
Modulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit Data
Yield Point
0 200 400 600 800
120
100
80
60
40
20
0
displacement / nm
load / mN
Load Vs. Displacement
Raw Data
0 Pt. Data
6
0 0.5 1 1.5 2 2.5
5
x 10
0
-2
-4
-6
-8
-10
-12
x 10
S
P2/3-Sh
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5
20
15
10
5
0
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03
7000
6000
5000
4000
3000
2000
1000
0
Strain
Contact Radius / nm
Strain Vs. Contact Radius
Data
Elastic

64. 775F_ 100micron tip_ test 005

65. 775F_ 100micron tip_ test 005
Estat =
mean: 73.0240
median: 73.0903
stdev: 1.7293
min: 70.0061
max: 75.9250
Ystat =
mean: 0.2102
median: 0.2100
stdev: 0.0102
min: 0.1834
max: 0.2314
Hstat =
mean: 9.9928
median: 9.9663
stdev: 0.2857
min: 9.4651
max: 10.6556

66. 775F_ 100micron tip_ test 007

67. 775F_ 100micron tip_ test 007

68. 775F_ 100micron tip_ test 010

69. 775F_ 100micron tip_ test 010

70. Elastic module Yield strength (GPa) Hardening
As received
400 F 55.73153 0.422567 20.59428
525 F 56.33968 0.2724 14.30632
650 F
775 F