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Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 1
EXPERIMENT NO.4
Rotary dryer
Aim:
a) To study operation of rotary dryer.
b) To study the drying characteristics of a solid material in a rotary dryer.
c) To plot the rate of drying curve.
1. Theory & procedure
1.1 System
In many cases, the drying of materials is the final operation in manufacturing process
carried out immediately prior to packaging and dispatch. Drying refers to final
removal of water, and the operation follows evaporation, filtration or crystallization.
Drying is carried out for one or more of the following reasons:
• To reduce the transportation cost.
• To make a material more suitable for handling, for example soap powders,
dyestuffs, fertilizers.
• To provide definite properties, such as maintaining free flowing nature of
salt.
• To remove moisture, which may otherwise lead to corrosion, for example
the drying of coal gas or benzene prior to chlorination.
Almost all drying processes involve the removal of the water by vaporization, and
thus require the addition of heat.
The rotary dryer is a type of industrial dryer to employed to reduce or minimize the
liquid moisture content of the material by bringing it in direct contact with heated gas.
The dryer is made up of large rotating cylinder which slopes slightly so that the
discharge end is lower than the material feed end in order to covey the material under
gravity. Material to be dried enters the dryers and as the dryer rotates, the material is
lifted up by a series of internal fins lining the inner wall of the dryer. Heating options
include steam, gas, oil, thermal oil, and auxiliary biomass burner system [1]
.
Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 2
Fig. 1 Rotary dryer system [1]
1.2 Mechanism
Consider a rotary continues counter-current dryer fed with a non-porous material
having all moisture as unbound moisture. As this material enters the dryer, its first
heated to drying temperature. It will then pass through the length of the dryer at nearly
the wet bulb temperature and theoretically at the end of the dryer, the material shall be
discharged as dry material nearly at the wet bulb temperature.
Fig. 2 Co-Current process of rotary dryer
Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 3
Assumptions:
a) No heat losses from the dryer.
b) Heat is applied to the material only from the air, not by conduction from the
dryer shell.
c) All the moisture present is free moisture.
d) There is no evaporation of moisture in the preliminary heating period.
Drying proceed at a constant wet bulb temperature until desired amount of water has
been removed. The entering air is assumed to be 100% saturated so its temperature
need to be raised so as to decrease the relative saturation. This would enable the air to
absorb moisture from wet solid feed. In turn the exiting air is more saturated than the
entering one.
The continues dryer at steady state operating condition,
F (X1-X2) = G (Y1-Y2) …………………………. (1)
This assume that the dry gas flow (G) and dry solids flow (F) do not change between
dryer inlet and outlet. Mass balances can also be performed on the overall gas and
solids entrainment in the exhaust gas stream.
The required solid flow rate, the inlet moisture content (X1) and outlet moisture (X2)
are normally specified, and the evaporation rate and outlet gas flow are calculated.
For batch dryer with a dry mass (m) of solids, a mass balance only gives a snapshot at
one point during the drying cycle and an instantaneous drying rate given by:
= G( ……..…....………………. (2)
………………..…………. (3)
Where:
Is called rate of drying.
Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 4
1.3 Description
The set-up consists of a long resolving cylindrical shell slightly inclined toward the
outlet. The shell is fitted with two brackets for support. Air from a blower pass
through a heating chamber serves the purpose of drying agent. An arrangement is
provided for rotating the dryer shell connected with electric motor and a reduction
gear box. Flow control valve and by-pass valve fitted to regulate the airflow. The
present setup has a facility to interface the system with computer which enable to log
the experimental data using computer. The educational software and data-logging
package has been developed per unit. This software is capable to tabulate the sample
readings according to the requirement of experiment under study and results obtained
can be compared.
1.4 Observation and calculation
1.4.1 Data
Table 1
Technical Detail Parameters
Area of duct (A) 0.011 m2
Density of air (𝜌a) 1.21 kg/m3
Molecular weight of air (Ma) 29 g/mole
Molecular weight of water (Mw) 18 g/mole
1.4.2 Observations
Table 2
S.No. T1 (⸰C) T2 (⸰C) T3 (⸰C) T4 (⸰C) V (m/s)
1 40 24 30 19 1
2 45 28 35 22 2
3 50 30 40 23 3
Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 5
1.4.3 Calculations
G = V. 𝜌a . A (kg/s) …………………… (4)
To calculate the humidity (y1, y2) of air at temperature (T1, T2) and (T3, T4)
respectively by psychometric chart.
No. of Experiment y1 y2
1 0.017 0.012
2 0.028 0.014
3 0.039 0.015
(kg of moisture / kg of dry air) …………………………………. (5)
(kg of moisture / kg of dry air) …………………………………. (6)
N = G (Y1 – Y2) (kg of moisture / sec) ………………..………………… (7)
Table 3
S.NO. G (kg/sec) Y1 (kg
moisture/sec)
Y2 (kg
moisture/sec)
N (kg
moisture/sec)
1 0.0133 0.010 0.0074 0.000034
2 0.0266 0.017 0.0086 0.00022
3 0.0399 0.024 0.0093 0.00058
Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 6
1.5 Nomenclature
Nom Heading Units
F Mass flowrate of material Kg/s
G Mass flowrate of air Kg/s
V Velocity m/s
N Rate of Drying kg of moisture /
sec
T1 Inlet dry bulb temperature of air ⸰C
T2 Outlet dry bulb temperature of air ⸰C
T3 Inlet wet bulb temperature of air ⸰C
T4 Outlet wet bulb temperature of air ⸰C
Y Absolute humidity difference kg of moisture /
kg of dry air
Y1 Absolute humidity of air at the inlet of dryer kg of moisture /
kg of dry air
Y2 Absolute humidity of air at the outlet of dryer kg of moisture /
kg of dry air
y1 Moisture content of the air at the inlet of dryer kg of moisture /
kg of dry air
y2 Moisture content of the air at the outlet of dryer kg of moisture /
kg of dry air
Mass Transfer Laboratory
E x p e r i m e n t N o . 4 Page 7
Fig. 3 Psychrometric chart [2]
2. Discussion questions
a) Plot the rate of drying curve for all experiment.
b) What are the parameters that effect on the rate of drying?
References
1. Micro Technologies, The Computer Controlled Bench Rotary Dryer, Model:
MT-MT-143/DL.
2. Perry, R.H. and D.W. Green (eds.), Chemical Engineer’s Handbook, 7th ed.,
McGraw-Hill, 1997.
Barhm Abdullah Mohamad
Erbil Polytechnic University
LinkedIn: https://www.linkedin.com/in/barhm-mohamad-900b1b138/
Google Scholar: https://scholar.google.com/citations?user=KRQ96qgAAAAJ&hl=en
ResearchGate: https://www.researchgate.net/profile/Barhm_Mohamad
YouTube channel: https://www.youtube.com/channel/UC16-u0i4mxe6TmAUQH0kmNw

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Rotary Dryer Rate of Drying Experiment

  • 1. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 1 EXPERIMENT NO.4 Rotary dryer Aim: a) To study operation of rotary dryer. b) To study the drying characteristics of a solid material in a rotary dryer. c) To plot the rate of drying curve. 1. Theory & procedure 1.1 System In many cases, the drying of materials is the final operation in manufacturing process carried out immediately prior to packaging and dispatch. Drying refers to final removal of water, and the operation follows evaporation, filtration or crystallization. Drying is carried out for one or more of the following reasons: • To reduce the transportation cost. • To make a material more suitable for handling, for example soap powders, dyestuffs, fertilizers. • To provide definite properties, such as maintaining free flowing nature of salt. • To remove moisture, which may otherwise lead to corrosion, for example the drying of coal gas or benzene prior to chlorination. Almost all drying processes involve the removal of the water by vaporization, and thus require the addition of heat. The rotary dryer is a type of industrial dryer to employed to reduce or minimize the liquid moisture content of the material by bringing it in direct contact with heated gas. The dryer is made up of large rotating cylinder which slopes slightly so that the discharge end is lower than the material feed end in order to covey the material under gravity. Material to be dried enters the dryers and as the dryer rotates, the material is lifted up by a series of internal fins lining the inner wall of the dryer. Heating options include steam, gas, oil, thermal oil, and auxiliary biomass burner system [1] .
  • 2. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 2 Fig. 1 Rotary dryer system [1] 1.2 Mechanism Consider a rotary continues counter-current dryer fed with a non-porous material having all moisture as unbound moisture. As this material enters the dryer, its first heated to drying temperature. It will then pass through the length of the dryer at nearly the wet bulb temperature and theoretically at the end of the dryer, the material shall be discharged as dry material nearly at the wet bulb temperature. Fig. 2 Co-Current process of rotary dryer
  • 3. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 3 Assumptions: a) No heat losses from the dryer. b) Heat is applied to the material only from the air, not by conduction from the dryer shell. c) All the moisture present is free moisture. d) There is no evaporation of moisture in the preliminary heating period. Drying proceed at a constant wet bulb temperature until desired amount of water has been removed. The entering air is assumed to be 100% saturated so its temperature need to be raised so as to decrease the relative saturation. This would enable the air to absorb moisture from wet solid feed. In turn the exiting air is more saturated than the entering one. The continues dryer at steady state operating condition, F (X1-X2) = G (Y1-Y2) …………………………. (1) This assume that the dry gas flow (G) and dry solids flow (F) do not change between dryer inlet and outlet. Mass balances can also be performed on the overall gas and solids entrainment in the exhaust gas stream. The required solid flow rate, the inlet moisture content (X1) and outlet moisture (X2) are normally specified, and the evaporation rate and outlet gas flow are calculated. For batch dryer with a dry mass (m) of solids, a mass balance only gives a snapshot at one point during the drying cycle and an instantaneous drying rate given by: = G( ……..…....………………. (2) ………………..…………. (3) Where: Is called rate of drying.
  • 4. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 4 1.3 Description The set-up consists of a long resolving cylindrical shell slightly inclined toward the outlet. The shell is fitted with two brackets for support. Air from a blower pass through a heating chamber serves the purpose of drying agent. An arrangement is provided for rotating the dryer shell connected with electric motor and a reduction gear box. Flow control valve and by-pass valve fitted to regulate the airflow. The present setup has a facility to interface the system with computer which enable to log the experimental data using computer. The educational software and data-logging package has been developed per unit. This software is capable to tabulate the sample readings according to the requirement of experiment under study and results obtained can be compared. 1.4 Observation and calculation 1.4.1 Data Table 1 Technical Detail Parameters Area of duct (A) 0.011 m2 Density of air (𝜌a) 1.21 kg/m3 Molecular weight of air (Ma) 29 g/mole Molecular weight of water (Mw) 18 g/mole 1.4.2 Observations Table 2 S.No. T1 (⸰C) T2 (⸰C) T3 (⸰C) T4 (⸰C) V (m/s) 1 40 24 30 19 1 2 45 28 35 22 2 3 50 30 40 23 3
  • 5. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 5 1.4.3 Calculations G = V. 𝜌a . A (kg/s) …………………… (4) To calculate the humidity (y1, y2) of air at temperature (T1, T2) and (T3, T4) respectively by psychometric chart. No. of Experiment y1 y2 1 0.017 0.012 2 0.028 0.014 3 0.039 0.015 (kg of moisture / kg of dry air) …………………………………. (5) (kg of moisture / kg of dry air) …………………………………. (6) N = G (Y1 – Y2) (kg of moisture / sec) ………………..………………… (7) Table 3 S.NO. G (kg/sec) Y1 (kg moisture/sec) Y2 (kg moisture/sec) N (kg moisture/sec) 1 0.0133 0.010 0.0074 0.000034 2 0.0266 0.017 0.0086 0.00022 3 0.0399 0.024 0.0093 0.00058
  • 6. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 6 1.5 Nomenclature Nom Heading Units F Mass flowrate of material Kg/s G Mass flowrate of air Kg/s V Velocity m/s N Rate of Drying kg of moisture / sec T1 Inlet dry bulb temperature of air ⸰C T2 Outlet dry bulb temperature of air ⸰C T3 Inlet wet bulb temperature of air ⸰C T4 Outlet wet bulb temperature of air ⸰C Y Absolute humidity difference kg of moisture / kg of dry air Y1 Absolute humidity of air at the inlet of dryer kg of moisture / kg of dry air Y2 Absolute humidity of air at the outlet of dryer kg of moisture / kg of dry air y1 Moisture content of the air at the inlet of dryer kg of moisture / kg of dry air y2 Moisture content of the air at the outlet of dryer kg of moisture / kg of dry air
  • 7. Mass Transfer Laboratory E x p e r i m e n t N o . 4 Page 7 Fig. 3 Psychrometric chart [2] 2. Discussion questions a) Plot the rate of drying curve for all experiment. b) What are the parameters that effect on the rate of drying? References 1. Micro Technologies, The Computer Controlled Bench Rotary Dryer, Model: MT-MT-143/DL. 2. Perry, R.H. and D.W. Green (eds.), Chemical Engineer’s Handbook, 7th ed., McGraw-Hill, 1997. Barhm Abdullah Mohamad Erbil Polytechnic University LinkedIn: https://www.linkedin.com/in/barhm-mohamad-900b1b138/ Google Scholar: https://scholar.google.com/citations?user=KRQ96qgAAAAJ&hl=en ResearchGate: https://www.researchgate.net/profile/Barhm_Mohamad YouTube channel: https://www.youtube.com/channel/UC16-u0i4mxe6TmAUQH0kmNw