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Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288
                    Delamination Detection By Thermography
 Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky
                             E. El-Soaly
                   *Libyan Army, mechanical engineering department, Benghazi, Libya,
               **Military Technical College, mechanical engineering department, Cairo, Egypt,
         ***Military Technical College, Head of mechanical engineering department, Cairo, Egypt,
   ****10th of Ramadan Higher Institute of Technology, mechanical engineering department, Cairo , Egypt ,

Abstract
         Infrared thermography is a two-                  front propagates, by diffusion, under the surface and
dimensional, non-contact technique allowing               also because of radiation and convection losses. The
surface temperature mapping by providing                  presence of a defect reduces the diffusion rate so
colourful images easy to interpret through the            that when observing the surface temperature, defects
use of an external energy source and an infrared          appear as areas of different temperatures with
detector. The attention of the present study was          respect to surrounding sound areas once the thermal
focused on the aid provided by active                     front has reached them. Consequently, deeper
thermography for non-destructive evaluation of            defects will be observed later and with a reduced
composite material. In present work the                   contrast [4].
experimental analysis was performed by testing
several specimens, which were made of E glass                       Thermography is now a popular non
woven with epoxy which included the most                  destructive testing method for detecting defects in
commonly encountered kinds of damage called               composite structures. Active thermography method
delamination artificially created in composite            for composites is well reported in literature [5-6].
laminate specimens. From the experimental                 An active thermography system consists of a heater
investigations, the effects of delamination area on       unit for controlled heating of the test specimen, an
the detection were elucidated. Also the                   infrared camera for capturing the surface
applicability of the present thermograph method           temperature evolution of the specimen, and a data
depends on a relative difference of thermal               acquisition system for acquiring the corresponding
property between the delamination and its                 infrared images over a specific period of time.
surrounding was explained.
                                                                    Delamination is one of the most common
Keywords:     Active infrared          thermography,      defects for composite materials. It leads to the
Composite material, Delamination.                         degradation of mechanical properties and also
                                                          causes the failure of the overall composite
1. Introduction                                           component. To detect delaminations and ensure the
         Non-destructive inspection methods must          safe operation of composite components, non
be reliable, efficient, non expensive, fast and easy to   destructive evaluation techniques are used. An
use. Moreover, as materials and processes are             extremely promising technique is thermography,
constantly changing, inspection techniques should         which has the advantage of good fault detection
adapt to this evolution, too. Among various non           possibility along with the capacity to inspect a large
destructive inspection techniques currently used is       area within a short time. Thermography is also
infrared thermography which a non-contact                 applicable to a wide range of materials, including
inspection tool. It is relevant whenever there is a       glass fibre, carbon fibre composites and metallic
thermal contrast between the inspected object and         materials, where specific excitation techniques are
the surrounding area of interest [1-3].                   needed for each application. To inspect defects over
                                                          a large scale and at large stand-off distances,
           Thermography is a technique of producing       integration of thermography has been investigated
a live thermal picture of an object based on the          [7].
infrared radiation received from it (emitted by any
object). In pulse thermography, a thermal pulse is                 The present paper describes experiments
applied to the material to be inspected. Following        conducted with the active thermographic procedure,
the application of this thermal pulse, a measurement      which consists in sending a controlled heat flux
of the temporal evolution of the specimen surface         using an external heat source (hot air blower) to the
temperature is performed with an infrared camera          inspected composite laminate plate. The objective of
allowing subsurface defects to be revealed. The           this paper is to present results from some
temperature of the material changes rapidly after the     experiments using active thermographic inspection
initial thermal perturbation because the thermal          procedure on composite material consist of E glass
                                                          woven and matrix with deliberately inserted


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Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
                  International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
                             www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288
                artificial delamination. Effect of delamination area     Cross ply 8-layered plates include E glass fibres
                and variation of thermal properties between              embedded in an epoxy matrix were used in present
                delamination and basic material were studied by          experimental work, with an overall laminate
                analyzing the surface temperature profiles and           thickness of 2.5 mm. The dimensions of square
                thermal contrasts obtained from experimental active      specimens were (200x200) mm2. Aluminum foils as
                thermal imaging system.                                  the man-made delaminations were manufactured
                                                                         with different areas (50x50, 100x100, 150x150)
                2. Experiment 1                                          mm2 inserted in the central mid plane of some plates
                2.1 Samples preparation                                  as          shown             in           Figure.1.




                                                                                                    50mm




                                                                               200mm




                                                                                                            50mm
        200mm




                                  200mm                                                             200mm

                   a) Healthy plate (no delamination)                                  b) Delamination area (50x50) mm2


                                                                                                    150mm


                                  100mm




                                                                                                                          150mm
                                               100mm




                                                                              200mm
200mm




                                  200mm
                                                                                                  200mm

                 c) Delamination area (100x100) mm2                                    d) Delamination area (150x150) mm2
                                                           Figure.1 Test specimens

                2.2 Active thermography experimental set-up              infrared thermography is shown in Figure.2. The
                         The investigation of composite materials        infrared camera measures the thermal transient at
                most often demands the active method. The active         the surface of the plates resulting from the heating
                approach requires an external heat source to             of the plates. The infrared camera captures the
                stimulate    tested    materials.   The     present      thermal information and generates two dimensional
                experimentation was carried out by using a hot air       thermogram which was saved in the camera memory
                blower to heat the sample with 2.5 kW output power       and then transferred to the computer for further
                uniformly. The heat source was kept 30 cm from the       processing. The emissivity was set at 1 (black
                investigated plate and the camera was held 70 cm         body), a value which offered the image with the best
                from the sample. The experimental setup for active       contrast with the background.




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Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
  International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
             www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288

                                               Specimen



                                                      Hot air blower
                                   IR camera




                             Figure.2 Active thermography experimental set-up

2.3 Results and discussion                                delamination, an extension of deterioration during
         The surface temperature distribution             the manufacturing process. Thermal contrast was
images over the laminated composite plates were           obtained from the fact that, the Aluminum foil at the
obtained after the end of heating time 7 seconds          place of delaminations behaves like a barrier which
using experimental set-up. All thermograms                makes surface temperature above the delaminated
highlight the delaminations in the composite plates       surface slightly warmer than the round healthy
according to their areas but with various accuracy.       region. Present thermal contrast value was measured
Some of them are being influenced by non-uniform          by thermography to detect delaminations which
heating, because the heating time is short. In the        were used to analyze for varying areas. The surface
thermograms associated to these delaminated plates,       temperature distributions obtained from active
one can observe, besides the central induced              thermography experiment are shown in Figure.3.




                a) Healthy plate                                       b) Delamination area (50x50) mm2




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Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288




       c) Delamination area (100x100) mm2                          d) Delamination area (150x150) mm2

                 Figure.3 Surface temperature distributions for healthy and delaminated plates

The temperature profiles across the centre lines of the healthy and delaminated plates are shown in Figure.4.




                                               a) Healthy plate




                                         b) Delamination area (50x50) mm2




                                          c) Delamination area (100x100) mm2




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Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288




                                     d) Delamination area (150x150) mm2

                    Figure.4 Surface temperature profiles across the centre line of the plate

Figure.3 (a) and Figure.4 (a) show that the                 delamination increases, the thermal contrast was
temperature was almost uniform throughout the               also increased except for largest delamination area
surface of healthy plate. From the Figure.4 (a) the         (150x150) mm2 the maximum contrast decrease to
average temperature across the length of the healthy        3.85°C because of the short time of heating, also in
plate is 22.4°C experimentally. Figures.3 (b, c, d)         the case of the largest delamination, there was more
and Figures.4 (b, c, d) show that there are some non-       air trapped between the inserted foil and the resin
uniform temperature distributions at the specific           promoting the dissipation of heat in this delaminated
location of simulated delaminations, revealing that         area, but when the time of pre heating increased to
the plate does have delamination. The                       10 seconds instead of 7 seconds, the contrast
approximately maximum thermal contrasts obtained            increases to 6.1°C as shown in Figure.5. However
experimentally at the delamination locations were           the localized contrast regions are clearly identified
5.1°C and 5.7°C for delamination areas (50x50 and           even for small delamination area.
100x100) mm2 respectively. When the area of the




Figure.5 Surface temperature profile across the centre line of plate with delamination area (150x150) mm 2 after
                                              heating 10 seconds




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Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288
It was observed that after the end of the pre-heating                                                   are of course other limitations, mostly concerned
process, temperature profiles revealed the internal                                                     with the size of the delamination, the resolution of
delamination. Because of different thermal                                                              the infrared camera, the timing image capturing
conductivity between delamination and healthy                                                           during the transient phase and the thermal
area existence the defect was manifested by higher                                                      properties of the examined material. These
temperature in the delaminated region. It is possible                                                   limitations should be account for the significant
to vary heat input and heating time to obtain best                                                      accuracy to estimate the delamination shape in
delamination detectability, which depends on the                                                        laminated composite structure. Generally all
material being tested, its thickness, depth and area                                                    objects radiate energy continuously in the form of
of the delamination. In order to get a clear picture                                                    electromagnetic waves mainly in infrared region
of searched delaminations the pre-heating time                                                          produced by thermal vibrations of the molecules.
cannot be too long. Long-time pre-heating led to                                                        The relationship governing radiation power from
even temperature distribution over entire searched                                                      hot objects according to the Stefan-Boltzmann law
surface. This effect was observed independently on                                                      is:
type of a heat source (flash or heater radiator) and
on the position of the heat source. After many trials                                                   P = ε σ AT4                   (1)
it was stated that an appropriate warm-up time in                                                       Where,
present case of composite laminate materials                                                            P = Radiated power (watts)
should be about 7 seconds. It is also worth                                                             A = Radiating area (m2)
mentioning that although the best possible results                                                      σ = Stefan-Boltzmann constant (5.6703 x 10-8
concerning the clearest images (high thermal                                                            W/m2K4)
contrast) were acquired at relatively short periods                                                     ε = Emissivity (=0.03for Aluminum foil)
during the cooling down process (composites have                                                        T=Temperature of radiator (in Kelvin)
relatively low thermal conductivity values). There


The total radiated power from delaminated specimens can be calculated according to Eq1, that showing below in
Table 1

                                                                    Table 1 Total radiation power from delaminated samples

               Delamination area (mm2 )                                                                         Total radiation power (w)
                       50x50                                                                                             0.0322
                      100x100                                                                                             0.129
                      150x150                                                                                             0.290

The relation between total radiation power and the delamination areas shown in Figure.6.

                                                          1.1
                                                           1
                    Normalized total radiation power
                       Normalized total radiation power




                                                          0.9
                                                          0.8
                                                          0.7
                                                          0.6

                                                          0.5
                                                          0.4
                                                          0.3
                                                          0.2

                                                          0.1
                                                           0
                                                                0         50x50
                                                                            1         2         100x100
                                                                                                   3           4       150x150
                                                                                                                          5          6
                                                                                            Delaminated area
                                                                                   Delaminated area (mm2)


                                                          Figure.6 Variation of total radiation power with delaminated areas




                                                                                                                                             284 | P a g e
Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288
3. Experiment 2
3.1 Specimens preparation                                     experiment consist of different delamination thermal
         E glass woven with epoxy specimens were              properties, such as sample 1 contains simulated
fabricated including artificial delaminations located         delamination Aluminum foil coated with special
at same depth 1.25 mm Figure.7.The areas of these             isolated wax and sample 2 with simulated
test samples were (205x205) mm2, number of layers             delamination air gap. All these simulated
was 8 and the area of delamination was (60x205)               delaminations have different thermal properties.
mm2.The simulated test plates used in present                                    205 mm
                                                                                 60 mm




                                                          205 mm

          a) Sample 1 (Aluminum delamination)                       b) Sample 2 (Air gap delamination)

                                             Figure.7 Test specimens

3.2 Delaminations description                                 3.3 Experimental set-up
          A brief description of different anomalies                   The schematic of the experimental setup is
in the previous test specimens is provided below:             shown in Figure.8. A heat blower was used as a heat
1. Air gap delamination, a manufacturing defect               source to all samples. The distance between the
where air was trapped between layers of fiber glass           heating element and the test plate for each
so that there was glass fiber but no resin to bond it.        experiment was kept constant. A gap of
2. Aluminum alloy delamination, an area of                    approximately 30 cm was maintained between the
specimen whereby one layer of fiber glass has                 heat source and the test sample.
separated from the adjacent layer, by using an
Aluminum foil coated with special wax.


                                                  Sample 2



                                                             Hot air blower



                                    IR camera




                               Figure.8 Active thermography experimental set-up




                                                                                                   285 | P a g e
Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288

3.4 Results and discussion                                                               temperature and time elapsing after pre-heating
          All samples considered in present                                              interruption achieved in delamination area, were
experiment were heated for different time periods,                                       characterized by a higher temperature in connection
i.e. 3 seconds, 7 seconds, 12 seconds, and 1 min. A                                      to the rest of the specimen, also the cooling process
thermal camera was used to record the thermal                                            in the area with delamination runs much longer.
intensity decay data with cooling time, following the                                    Figure.9, gives a direct impression of the behaviour
removal of the heat source. When the test samples                                        of the temperature at the surface of the test samples,
were heated for 3 seconds, no significant                                                after the maximum value of the temperature was
temperature rise was observed whereas, when                                              reached. The Figure shows the temperature decay of
heated for 1 minute, the thermal camera produces                                         different simulated delamination samples after
saturated images. Hence, for the cases considered in                                     heating each one uniformly and separately for 7
the present experiment it was observed that the                                          seconds. However, it was observed that, temperature
optimal heating times for delamination detection of                                      decays in sample 1 and sample 2 cases have similar
different thermal properties were 7 and 12 seconds.                                      decreasing trends over the cooling cycle and were
Generally in present case, relation between                                              difficult to distinguish when heated for 7 seconds.

                                              23.9
                             Temperature °C




                                              23.8                                                          Sample 1 Aluminum
                                              23.7                                                          delamination
                                              23.6                                                          Sample 2 air gap
                                              23.5                                                          delamination
                                              23.4
                                              23.3
                                                         0       5       10        15        20        25
                                                                       Time (second)
         Figure.9 Temperature decay for different delamination thermal properties heated for 7 seconds

The thermal images show prominent thermal decay when heated for 12 seconds, compared to the case of heating
for 7 seconds, the corresponding temperature decay is shown in Figure.10. Sample 1 attains maximum
temperature when heated for 12 seconds followed by sample 2.

                                         25.3
                     Temperature °C




                                              25
                                         24.7
                                                                                                            Sample 1 Aluminum
                                         24.4                                                               delamination
                                                                                                            Sample 2 air gap
                                         24.1
                                                                                                            delamination
                                         23.8
                                         23.5
                                                     0       5         10     15        20        25
                                                                     Time (second)

       Figure.10 Temperature decay for different delamination thermal properties heated for 12 seconds

Thermal camera images for sample 1 and sample 2 are shown in Figure.11 and Figure.12. In the following
thermograms associated to delaminated samples, one can observe, besides the central artificial delamination, a
little deterioration at upper portion of the artificial delaminations during the manufacturing process.




                                                                                                                                286 | P a g e
Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
   International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
              www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288




              a) Sample 1 (Aluminum delamination)             b) Sample 2 (Air gap delamination)

                           Figure.11 Thermal camera images after 7 seconds of heating




               a) Sample 1 (Aluminum delamination)            b) Sample 2 (Air gap delamination)

                          Figure.12 Thermal camera images after 12 seconds of heating

As heating time increases, the contrast between             basic material. The present experiment confirmed
delamination and healthy area increases and                 that thermal properties of a delamination material
delamination of both samples show different                 can be concluded from sequential recording of
contrast depending on its thermal properties as             thermograms including temperature distribution on
shown before in Figure 11 and Figure 12. The                the surface of the plate under test starting at the
heating time of 12 seconds instead of 7 seconds             beginning of the cool down phase. Thermal images
leads to increase of the heating energy, because the        allowed determination of whether specific material
heating energy must be enough to creat thermal              of delamination was of higher or lower thermal
contrast between healthy and delaminated area,              properties than the healthy material.
which can be sensed by infrared camera. If the
energy is not enough as introduced before at                4. Conclusions
heating time 7 seconds, the delamination may be                       In this work, the study of delaminations in
difficult to extinguish, especially when the                composite laminate plates using thermography
comparing of delamination appearance was                    technique was done experimentally. The
according to the type of delamination thermal               experiments were intended to detect delamination
properties. Therefore the delamination visibility           of variable areas and thermal properties existing in
depends strongly on the thermal properties of both          composite laminate plates. The following
the basic material and the delamination itself. It is       conclusions can be drawn:
demonstrated that the heating temperature plays an          1. Thermographic images analysis is an effective
important role in the detection of delamination             method for revealing delamination in the composite
which increase amount of thermal radiation that the         materials.
camera received from surface, also by increasing            2. Thermography methods require specific skills to
heating time, minimized the effects of non-uniform          achieve good results in delamination detection for
temperature distribution, one of the main problem           composite material.
that affect the quality of this type of non destructive     3. Because of different thermal conductivity
test. The suitability of infrared thermography to           between delamination and healthy area existence
non destructive testing depends on the ability to           the defect was manifested by higher temperature in
detection of the temperature variation or thermal           the delaminated region.
contrast induced by a delamination which greatly            4. It is possible to vary heat input and heating time
effected by thermal properties of delamination and          to obtain best defect detectability, which depends



                                                                                                 287 | P a g e
Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly /
  International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622
             www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288
on the material being tested, its thickness, depth,         aerospace     materials     with    lock-in
area of the delamination, the timing image                  thermography”       Engineering      failure
capturing during the transient phase and the                analysis, volume 13, issue 3, p.p 380–
resolution of thermal camera.                               388, April 2006.
5. The heating temperature plays an important role    [4]   Clemente Ibarra Castanedo “Quantitative
in the detection of delamination which increase             subsurface defect evaluation by pulsed
amount of thermal radiation that the camera                 phase thermography: depth retrieval with
received from surface.                                      the phase” Thèse présentée à la Faculté
6. The delamination visibility depends strongly on          des études supérieures de l’Université
the thermal properties of both the basic material           Laval dans le cadre du programme de
and the delamination itself.                                doctorat en génie électrique pour
                                                            l’obtention du grade de Philosophiae
References                                                  Doctor (Ph.D.) 2005.
  [1]   G. Wróbel a, Z. Rdzawski b,c, G. Muzia b,     [5]   X.Maldague and S.Marinetti “Pulse phase
        S. Pawlak a,” Transient thermography in             infrared thermography” Journal of applied
        the assessment of local fibre content in            physics, volume 79 , issue, 5.1995.
        CFRP laminates”Journal of achievements        [6]   X.P.V. Maldague ” Introduction to NDT
        in     materials   and      manufacturing           by active       infrared    thermography”
        engineering,volume 31, issue 2, December            Materials Evaluation,. 60, No. 9. pp. 1060-
        2008.                                               1073 Key: citeulike: 6541620, September
  [2]   M. Krishnapillai, R. Jones, I.H. Marshall,          2002.
        M. Bannister, N. Rajic “Thermography as       [7]   Liang      Cheng and Gui      Yun      Tian
        a tool for damage assessment” Composite             “Comparison of non destructive testing
        structures, 2005.                                   methods on detection of delaminations in
  [3]   Carosena       Meola, Giovanni     Maria            composites” Journal of sensors, vol 2012,
        Carlomagno, Antonino Squillace, Antonio             article ID 408437.2012.
        Vitiello “Non-destructive evaluation of




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Ao31279288

  • 1. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 Delamination Detection By Thermography Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly *Libyan Army, mechanical engineering department, Benghazi, Libya, **Military Technical College, mechanical engineering department, Cairo, Egypt, ***Military Technical College, Head of mechanical engineering department, Cairo, Egypt, ****10th of Ramadan Higher Institute of Technology, mechanical engineering department, Cairo , Egypt , Abstract Infrared thermography is a two- front propagates, by diffusion, under the surface and dimensional, non-contact technique allowing also because of radiation and convection losses. The surface temperature mapping by providing presence of a defect reduces the diffusion rate so colourful images easy to interpret through the that when observing the surface temperature, defects use of an external energy source and an infrared appear as areas of different temperatures with detector. The attention of the present study was respect to surrounding sound areas once the thermal focused on the aid provided by active front has reached them. Consequently, deeper thermography for non-destructive evaluation of defects will be observed later and with a reduced composite material. In present work the contrast [4]. experimental analysis was performed by testing several specimens, which were made of E glass Thermography is now a popular non woven with epoxy which included the most destructive testing method for detecting defects in commonly encountered kinds of damage called composite structures. Active thermography method delamination artificially created in composite for composites is well reported in literature [5-6]. laminate specimens. From the experimental An active thermography system consists of a heater investigations, the effects of delamination area on unit for controlled heating of the test specimen, an the detection were elucidated. Also the infrared camera for capturing the surface applicability of the present thermograph method temperature evolution of the specimen, and a data depends on a relative difference of thermal acquisition system for acquiring the corresponding property between the delamination and its infrared images over a specific period of time. surrounding was explained. Delamination is one of the most common Keywords: Active infrared thermography, defects for composite materials. It leads to the Composite material, Delamination. degradation of mechanical properties and also causes the failure of the overall composite 1. Introduction component. To detect delaminations and ensure the Non-destructive inspection methods must safe operation of composite components, non be reliable, efficient, non expensive, fast and easy to destructive evaluation techniques are used. An use. Moreover, as materials and processes are extremely promising technique is thermography, constantly changing, inspection techniques should which has the advantage of good fault detection adapt to this evolution, too. Among various non possibility along with the capacity to inspect a large destructive inspection techniques currently used is area within a short time. Thermography is also infrared thermography which a non-contact applicable to a wide range of materials, including inspection tool. It is relevant whenever there is a glass fibre, carbon fibre composites and metallic thermal contrast between the inspected object and materials, where specific excitation techniques are the surrounding area of interest [1-3]. needed for each application. To inspect defects over a large scale and at large stand-off distances, Thermography is a technique of producing integration of thermography has been investigated a live thermal picture of an object based on the [7]. infrared radiation received from it (emitted by any object). In pulse thermography, a thermal pulse is The present paper describes experiments applied to the material to be inspected. Following conducted with the active thermographic procedure, the application of this thermal pulse, a measurement which consists in sending a controlled heat flux of the temporal evolution of the specimen surface using an external heat source (hot air blower) to the temperature is performed with an infrared camera inspected composite laminate plate. The objective of allowing subsurface defects to be revealed. The this paper is to present results from some temperature of the material changes rapidly after the experiments using active thermographic inspection initial thermal perturbation because the thermal procedure on composite material consist of E glass woven and matrix with deliberately inserted 279 | P a g e
  • 2. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 artificial delamination. Effect of delamination area Cross ply 8-layered plates include E glass fibres and variation of thermal properties between embedded in an epoxy matrix were used in present delamination and basic material were studied by experimental work, with an overall laminate analyzing the surface temperature profiles and thickness of 2.5 mm. The dimensions of square thermal contrasts obtained from experimental active specimens were (200x200) mm2. Aluminum foils as thermal imaging system. the man-made delaminations were manufactured with different areas (50x50, 100x100, 150x150) 2. Experiment 1 mm2 inserted in the central mid plane of some plates 2.1 Samples preparation as shown in Figure.1. 50mm 200mm 50mm 200mm 200mm 200mm a) Healthy plate (no delamination) b) Delamination area (50x50) mm2 150mm 100mm 150mm 100mm 200mm 200mm 200mm 200mm c) Delamination area (100x100) mm2 d) Delamination area (150x150) mm2 Figure.1 Test specimens 2.2 Active thermography experimental set-up infrared thermography is shown in Figure.2. The The investigation of composite materials infrared camera measures the thermal transient at most often demands the active method. The active the surface of the plates resulting from the heating approach requires an external heat source to of the plates. The infrared camera captures the stimulate tested materials. The present thermal information and generates two dimensional experimentation was carried out by using a hot air thermogram which was saved in the camera memory blower to heat the sample with 2.5 kW output power and then transferred to the computer for further uniformly. The heat source was kept 30 cm from the processing. The emissivity was set at 1 (black investigated plate and the camera was held 70 cm body), a value which offered the image with the best from the sample. The experimental setup for active contrast with the background. 280 | P a g e
  • 3. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 Specimen Hot air blower IR camera Figure.2 Active thermography experimental set-up 2.3 Results and discussion delamination, an extension of deterioration during The surface temperature distribution the manufacturing process. Thermal contrast was images over the laminated composite plates were obtained from the fact that, the Aluminum foil at the obtained after the end of heating time 7 seconds place of delaminations behaves like a barrier which using experimental set-up. All thermograms makes surface temperature above the delaminated highlight the delaminations in the composite plates surface slightly warmer than the round healthy according to their areas but with various accuracy. region. Present thermal contrast value was measured Some of them are being influenced by non-uniform by thermography to detect delaminations which heating, because the heating time is short. In the were used to analyze for varying areas. The surface thermograms associated to these delaminated plates, temperature distributions obtained from active one can observe, besides the central induced thermography experiment are shown in Figure.3. a) Healthy plate b) Delamination area (50x50) mm2 281 | P a g e
  • 4. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 c) Delamination area (100x100) mm2 d) Delamination area (150x150) mm2 Figure.3 Surface temperature distributions for healthy and delaminated plates The temperature profiles across the centre lines of the healthy and delaminated plates are shown in Figure.4. a) Healthy plate b) Delamination area (50x50) mm2 c) Delamination area (100x100) mm2 282 | P a g e
  • 5. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 d) Delamination area (150x150) mm2 Figure.4 Surface temperature profiles across the centre line of the plate Figure.3 (a) and Figure.4 (a) show that the delamination increases, the thermal contrast was temperature was almost uniform throughout the also increased except for largest delamination area surface of healthy plate. From the Figure.4 (a) the (150x150) mm2 the maximum contrast decrease to average temperature across the length of the healthy 3.85°C because of the short time of heating, also in plate is 22.4°C experimentally. Figures.3 (b, c, d) the case of the largest delamination, there was more and Figures.4 (b, c, d) show that there are some non- air trapped between the inserted foil and the resin uniform temperature distributions at the specific promoting the dissipation of heat in this delaminated location of simulated delaminations, revealing that area, but when the time of pre heating increased to the plate does have delamination. The 10 seconds instead of 7 seconds, the contrast approximately maximum thermal contrasts obtained increases to 6.1°C as shown in Figure.5. However experimentally at the delamination locations were the localized contrast regions are clearly identified 5.1°C and 5.7°C for delamination areas (50x50 and even for small delamination area. 100x100) mm2 respectively. When the area of the Figure.5 Surface temperature profile across the centre line of plate with delamination area (150x150) mm 2 after heating 10 seconds 283 | P a g e
  • 6. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 It was observed that after the end of the pre-heating are of course other limitations, mostly concerned process, temperature profiles revealed the internal with the size of the delamination, the resolution of delamination. Because of different thermal the infrared camera, the timing image capturing conductivity between delamination and healthy during the transient phase and the thermal area existence the defect was manifested by higher properties of the examined material. These temperature in the delaminated region. It is possible limitations should be account for the significant to vary heat input and heating time to obtain best accuracy to estimate the delamination shape in delamination detectability, which depends on the laminated composite structure. Generally all material being tested, its thickness, depth and area objects radiate energy continuously in the form of of the delamination. In order to get a clear picture electromagnetic waves mainly in infrared region of searched delaminations the pre-heating time produced by thermal vibrations of the molecules. cannot be too long. Long-time pre-heating led to The relationship governing radiation power from even temperature distribution over entire searched hot objects according to the Stefan-Boltzmann law surface. This effect was observed independently on is: type of a heat source (flash or heater radiator) and on the position of the heat source. After many trials P = ε σ AT4 (1) it was stated that an appropriate warm-up time in Where, present case of composite laminate materials P = Radiated power (watts) should be about 7 seconds. It is also worth A = Radiating area (m2) mentioning that although the best possible results σ = Stefan-Boltzmann constant (5.6703 x 10-8 concerning the clearest images (high thermal W/m2K4) contrast) were acquired at relatively short periods ε = Emissivity (=0.03for Aluminum foil) during the cooling down process (composites have T=Temperature of radiator (in Kelvin) relatively low thermal conductivity values). There The total radiated power from delaminated specimens can be calculated according to Eq1, that showing below in Table 1 Table 1 Total radiation power from delaminated samples Delamination area (mm2 ) Total radiation power (w) 50x50 0.0322 100x100 0.129 150x150 0.290 The relation between total radiation power and the delamination areas shown in Figure.6. 1.1 1 Normalized total radiation power Normalized total radiation power 0.9 0.8 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 0 50x50 1 2 100x100 3 4 150x150 5 6 Delaminated area Delaminated area (mm2) Figure.6 Variation of total radiation power with delaminated areas 284 | P a g e
  • 7. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 3. Experiment 2 3.1 Specimens preparation experiment consist of different delamination thermal E glass woven with epoxy specimens were properties, such as sample 1 contains simulated fabricated including artificial delaminations located delamination Aluminum foil coated with special at same depth 1.25 mm Figure.7.The areas of these isolated wax and sample 2 with simulated test samples were (205x205) mm2, number of layers delamination air gap. All these simulated was 8 and the area of delamination was (60x205) delaminations have different thermal properties. mm2.The simulated test plates used in present 205 mm 60 mm 205 mm a) Sample 1 (Aluminum delamination) b) Sample 2 (Air gap delamination) Figure.7 Test specimens 3.2 Delaminations description 3.3 Experimental set-up A brief description of different anomalies The schematic of the experimental setup is in the previous test specimens is provided below: shown in Figure.8. A heat blower was used as a heat 1. Air gap delamination, a manufacturing defect source to all samples. The distance between the where air was trapped between layers of fiber glass heating element and the test plate for each so that there was glass fiber but no resin to bond it. experiment was kept constant. A gap of 2. Aluminum alloy delamination, an area of approximately 30 cm was maintained between the specimen whereby one layer of fiber glass has heat source and the test sample. separated from the adjacent layer, by using an Aluminum foil coated with special wax. Sample 2 Hot air blower IR camera Figure.8 Active thermography experimental set-up 285 | P a g e
  • 8. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 3.4 Results and discussion temperature and time elapsing after pre-heating All samples considered in present interruption achieved in delamination area, were experiment were heated for different time periods, characterized by a higher temperature in connection i.e. 3 seconds, 7 seconds, 12 seconds, and 1 min. A to the rest of the specimen, also the cooling process thermal camera was used to record the thermal in the area with delamination runs much longer. intensity decay data with cooling time, following the Figure.9, gives a direct impression of the behaviour removal of the heat source. When the test samples of the temperature at the surface of the test samples, were heated for 3 seconds, no significant after the maximum value of the temperature was temperature rise was observed whereas, when reached. The Figure shows the temperature decay of heated for 1 minute, the thermal camera produces different simulated delamination samples after saturated images. Hence, for the cases considered in heating each one uniformly and separately for 7 the present experiment it was observed that the seconds. However, it was observed that, temperature optimal heating times for delamination detection of decays in sample 1 and sample 2 cases have similar different thermal properties were 7 and 12 seconds. decreasing trends over the cooling cycle and were Generally in present case, relation between difficult to distinguish when heated for 7 seconds. 23.9 Temperature °C 23.8 Sample 1 Aluminum 23.7 delamination 23.6 Sample 2 air gap 23.5 delamination 23.4 23.3 0 5 10 15 20 25 Time (second) Figure.9 Temperature decay for different delamination thermal properties heated for 7 seconds The thermal images show prominent thermal decay when heated for 12 seconds, compared to the case of heating for 7 seconds, the corresponding temperature decay is shown in Figure.10. Sample 1 attains maximum temperature when heated for 12 seconds followed by sample 2. 25.3 Temperature °C 25 24.7 Sample 1 Aluminum 24.4 delamination Sample 2 air gap 24.1 delamination 23.8 23.5 0 5 10 15 20 25 Time (second) Figure.10 Temperature decay for different delamination thermal properties heated for 12 seconds Thermal camera images for sample 1 and sample 2 are shown in Figure.11 and Figure.12. In the following thermograms associated to delaminated samples, one can observe, besides the central artificial delamination, a little deterioration at upper portion of the artificial delaminations during the manufacturing process. 286 | P a g e
  • 9. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 a) Sample 1 (Aluminum delamination) b) Sample 2 (Air gap delamination) Figure.11 Thermal camera images after 7 seconds of heating a) Sample 1 (Aluminum delamination) b) Sample 2 (Air gap delamination) Figure.12 Thermal camera images after 12 seconds of heating As heating time increases, the contrast between basic material. The present experiment confirmed delamination and healthy area increases and that thermal properties of a delamination material delamination of both samples show different can be concluded from sequential recording of contrast depending on its thermal properties as thermograms including temperature distribution on shown before in Figure 11 and Figure 12. The the surface of the plate under test starting at the heating time of 12 seconds instead of 7 seconds beginning of the cool down phase. Thermal images leads to increase of the heating energy, because the allowed determination of whether specific material heating energy must be enough to creat thermal of delamination was of higher or lower thermal contrast between healthy and delaminated area, properties than the healthy material. which can be sensed by infrared camera. If the energy is not enough as introduced before at 4. Conclusions heating time 7 seconds, the delamination may be In this work, the study of delaminations in difficult to extinguish, especially when the composite laminate plates using thermography comparing of delamination appearance was technique was done experimentally. The according to the type of delamination thermal experiments were intended to detect delamination properties. Therefore the delamination visibility of variable areas and thermal properties existing in depends strongly on the thermal properties of both composite laminate plates. The following the basic material and the delamination itself. It is conclusions can be drawn: demonstrated that the heating temperature plays an 1. Thermographic images analysis is an effective important role in the detection of delamination method for revealing delamination in the composite which increase amount of thermal radiation that the materials. camera received from surface, also by increasing 2. Thermography methods require specific skills to heating time, minimized the effects of non-uniform achieve good results in delamination detection for temperature distribution, one of the main problem composite material. that affect the quality of this type of non destructive 3. Because of different thermal conductivity test. The suitability of infrared thermography to between delamination and healthy area existence non destructive testing depends on the ability to the defect was manifested by higher temperature in detection of the temperature variation or thermal the delaminated region. contrast induced by a delamination which greatly 4. It is possible to vary heat input and heating time effected by thermal properties of delamination and to obtain best defect detectability, which depends 287 | P a g e
  • 10. Rashed A.Sultan, Samer W. Guirguis, Mahmoud M. Younes, El-Dessouky E. El-Soaly / International Journal of Engineering Research and Applications (IJERA) ISSN: 2248-9622 www.ijera.com Vol. 3, Issue 1, January -February 2013, pp.279-288 on the material being tested, its thickness, depth, aerospace materials with lock-in area of the delamination, the timing image thermography” Engineering failure capturing during the transient phase and the analysis, volume 13, issue 3, p.p 380– resolution of thermal camera. 388, April 2006. 5. The heating temperature plays an important role [4] Clemente Ibarra Castanedo “Quantitative in the detection of delamination which increase subsurface defect evaluation by pulsed amount of thermal radiation that the camera phase thermography: depth retrieval with received from surface. the phase” Thèse présentée à la Faculté 6. The delamination visibility depends strongly on des études supérieures de l’Université the thermal properties of both the basic material Laval dans le cadre du programme de and the delamination itself. doctorat en génie électrique pour l’obtention du grade de Philosophiae References Doctor (Ph.D.) 2005. [1] G. Wróbel a, Z. Rdzawski b,c, G. Muzia b, [5] X.Maldague and S.Marinetti “Pulse phase S. Pawlak a,” Transient thermography in infrared thermography” Journal of applied the assessment of local fibre content in physics, volume 79 , issue, 5.1995. CFRP laminates”Journal of achievements [6] X.P.V. Maldague ” Introduction to NDT in materials and manufacturing by active infrared thermography” engineering,volume 31, issue 2, December Materials Evaluation,. 60, No. 9. pp. 1060- 2008. 1073 Key: citeulike: 6541620, September [2] M. Krishnapillai, R. Jones, I.H. Marshall, 2002. M. Bannister, N. Rajic “Thermography as [7] Liang Cheng and Gui Yun Tian a tool for damage assessment” Composite “Comparison of non destructive testing structures, 2005. methods on detection of delaminations in [3] Carosena Meola, Giovanni Maria composites” Journal of sensors, vol 2012, Carlomagno, Antonino Squillace, Antonio article ID 408437.2012. Vitiello “Non-destructive evaluation of 288 | P a g e