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FOOD PACKAGING
TESTS & EQUIPMENTwww.PackTest.com
PackTest
www.PackTest.com
PackagingTesting Equipments
TestTechno Consultants was incorporated in 1989 and has become India’s Leading & Largest manufacturer & exporter
of QualityTesting Equipment for the Paper, Plastic and Packaging Industry.We offer the world’s widest range of
CompressionTesters,TensileTester,TorqueTesters, BurstTesters and many other MaterialTesting Equipment for
Paper, Plastic and converted products used in Packaging.
Whatever the Application…We provideTesting Equipment specially designed to test Packaging Material as well as
Formed Packages & ancillaries for the following :Compression, Crush, Burst Strength,Torque Force,Tensile,
Elongation, Peel, Seal, Friction, Shear, Adhesion,Tackiness,Texture, Drop, Impact,Vibration, Leak, Print, Scuff,
Abrasion, and many more..
Whatever the Industry…Our Equipments form the life line of Quality Assurance / R&D / Packaging Development
departments of almost all sectors of the industry involved in the manufacture of Packaging or heavy users of
Packaging & Packaging Materials.
Solutions
GSMTest
Summary :GSM is one of the most basic tests which stands forGrams per
Square Meter. It is also known as the “grammage” and is actually the
weight of 1 square meter of sample. Most paper is bought and sold in
accordance with its mass per unit area, and therefore the grammage has
greatsignificancebothtotheconsumerandtheproducerindefiningprice.
Applicableto:Paper
Test Method : A sample of 100cm² area (usually a square of 10x10cm or a
round of 11.284cm diameter) is cut and weight accurate to 0.01gm
resolutionandmultipliedby100togiveyoutheresulting/m²orgsm
TestStandard:TAPPIT-410/ISO536/IS1060
www.PackTest.com
ThicknessTest
www.PackTest.com
Summary :Thickness is an important property of paper, paperboard, foil,
filmorLaminates,andvariationsinthicknesscanleadtovariationsintheir
othermechanicalpropertiessuchasstiffness,permeability,etc.
Thickness is defined as the perpendicular distance between the two
principalsurfacesofthesamplesubstrate.
Applicableto:Paper,Paperboards,Film,Foils,Laminates
Test Method : A sample is measured in a Dial Type or Digital Thickness
Gauge mounted on a vertical stand with a weight (called as dead mass) on
top.The weight exerts a constant pressure of 50 kPa (100 kPa as per ISO) at
thecontactsurface(pointofmeasurement).Thisensureshighrepeatability
in test results.Ordinary screw type micrometers are not to be used as they
are highly operator dependent and any amount of excess pressure can
compressthespecimenandgivelowerresults.
TestStandard: TAPPIT-411/ASTMD645/ASTMF2251/ISO534/IS1060
www.PackTest.com
PinholeTest
Summary : Aluminum foils are used in food packaging laminates to
enhance the barrier properties of the package and to protect the contents
from gas / moisture permeation and also from light. Thinner gauges of
aluminum foil contain pinholes through which moisture and oxygen from
theenvironmentcanenterthepackageacceleratingthedegradationofthe
contents.Presenceofexcessivepinholesinthefoilwillsignificantlyhamper
theshelflifeofsuchproducts.
Applicableto:FoilsandFoilLaminates
TestMethod:Asampleoffoilorfoillaminateisplacedonaglassplatewith
lightsunderit.ThisapparatusisalsocalledasaLightBoxandusuallyhasa
hood on top to cover the sample. Pinholes will be visible as white spots as
light from underneath the sample will pass through the holes while the
opaque sample blocks the remaining light. Count the number of pinholes
persquaremeterofsample.
TestStandard:ASTMB926/IS:15392-2003
www.PackTest.com
DelaminationTest (a.k.a. Peel BondTest)
Summary :Laminatesaremadebybondingtogethertwoormorelayersof
materialormaterials.Theirperformanceisoftendependentontheabilityof
the laminate to function as a single unit. If the plies have not been properly
bondedtogether,theperformancemaybeadverselyaffected.
Applicableto:FlexibleLaminates
Test Method : Ply separation is initially started mechanically by the
application of heat or by using a solvent. The separated plies of the test
specimenareplacedintothegripsofatensiletestingmachine.Thegripsare
then separated and the force required to further separate the plies is
defined as bond strength.The most difficult part of the test is the sample
preparation itself which is very time consuming. Some layers of the
laminatearesothinthatyouwillrarelygetaproperpeeltestdone.
TestStandard:ASTMF904
www.PackTest.com
Summary : Seal strength is a quantitative measure for use in process
validation,processcontrolandcapability.Sealstrengthisnotonlyrelevant
to opening force and package integrity, but to measuring the packaging
processes’ ability to produce consistent seals. Seal strength at some
minimum level is a necessary package requirement, and at times it is
desirabletolimitthestrengthofthesealtofacilitateeasyopening.
Applicableto:FlexibleLaminatesandformedPouches.
Test Method : Samples are cut from a formed pouch. Alternatively
laminates can be sealed with controlled temperature, pressure and dwell-
time to create sample seals.The test specimen is then gripped in a tensile
testing machine. The grips are then separated and the force required to
separatethesealisdefinedassealstrength.
You can use a Lab Heat Sealer and aTensileTester to create samples using
different materials, temperature, pressure and dwell-time setting and find
thecombinationofferingthebestsealstrength.
TestStandard:ASTMF88
Seal StrengthTest ( a.k.a Heat SealabilityTest)
www.PackTest.com
For most food applications a permeation
measurement system would have to be able to
detectinameasurementrangeof0.05-2000cm3/
(m2dbar).
OTR Permeation Analyser by PreSens (Germany)
A new measurement system for testing synthetic materials on oxygen
permeabilitywasdeveloped.
Unlike the currently used systems with electrochemical or barometrical
sensorsitwasdesignedforopticalmeasurement.
The Fibox 4 trace together with chemical optical sensors was applied to
detect trace oxygen concentrations and validate the new measurement
system.Apartfromanalreadyavailablesensortypedifferentothertypesof
sensor material were tested to develop an oxygen sensor with an improved
limitofdetectionforhighbarrierpermeationmeasurements.
Thissensortype-PSt9-togetherwiththemeasurementcellsseemstobea
promising solution for easy, cost effective permeation measurements in
technicalapplications.
Pst6Range:10-²to10-⁷cm³ (STP)/(m²dbar)
Pst9Range:10-³and100cm³ (STP)/(m²dbar)
www.PackTest.com
Coefficient of Friction (C.O.F.)Test
Summary : Flexible packaging is usually done on Vertical or Horizontal
Form-Fill-Seal (FFS) machines in which the roll of film or laminate comes in
contact with itself or other metallic /non-metallic components of the FFS
machine.The contact generates friction which can inhibit the material to
runproperlyonthemachinesandachievedesiredproductionspeeds.
Measurements of frictional properties may be made on a film/laminate
whenslidingoveritselforoveranothersubstance(usuallystainlesssteel).
Theamountoffrictionrequiredtobeovercometoinitiatemotioniscalledas
the Static Coefficient of Friction and the amount of friction required to be
overcome to continue the motion is called as the Kinetic Coefficient of
Friction.
Applicableto:PlasticFilmandLaminates.
Test Method : A sled weighing 200 ± 5 g is wrapped around with the test
specimen and made to slide over a similar substrate or stainless steel
surface with a speed of 150 ± 30mm/min.The initial and average drag force
(ingrams)isrecordedanddividedbythesledweight(200g)tocalculatethe
staticandkineticCOFrespectively.
TestStandard:ASTMD1894
www.PackTest.com
Ink RubTest / ScuffTest (Print QualityTest)
Summary:Packagingisknownasa“SilentSalesman”.Thepackagehasto
be attractive enough for the consumer to feel compelled to pick it up from
the shelf. It also has to display technical information about the product,
such are contents, packing dates, expiry info, etc as mandated by law.
However the packaging can get scuffed or rubbed during various stages of
production, transportation and distribution. This test allows us to create
standardized conditions of rubbing to evaluate the performance of
different test specimens. Can also be used to evaluate the efficacy of
varnishingoranyotherspecializedcoatingsontheprintedsurface.
Applicable to :All types of surface printed packaging such as Foils, Labels,
PrintedCartons,andevenbatchcodingonpouches.
Limitation:Canbeusedfortestingmaterialinsheetformonly.Thoughthe
testcanalsobemodifiedforcurvedsurfacesofrigidpackaging.
www.PackTest.com
PATRA RubTest / Sutherland RubTest
TestMethod:Therearetypically2methodoftesting
1)RotaryRubbingusing2circulardiscsofsize2and4.5Inches.
2)LinearRubbingusing2rectangularsamplesofspecifiedsizes.
RotaryRubtestismorecommonlyknownasthePatra/PiraRubTestandis
the preferred test method for Rigid substrates like paperboards.This test
cannot be done successfully on thinner and more flexible substrates which
crumpleuponrotaryrubbing.
Linear Rub test is more commonly known as theSutherland RubTest and is
anall-roundertestsinceitcanbeusedonallthinorthickspecimens.
TestStandard:
RotaryRub:BritishStandardsBS-3110
LinearRub:BritishStandardsBS-3110andASTMD5264
www.PackTest.com
Pouch CompressionTest (aka. Load BurstTest)
Summary : When a shipper carton fails, stacking loads can be transmitted
ontothepackage.Henceaflexibleorsemiflexiblepackage(suchasapouch
orblisterpack)shouldhavetheabilitytowithstandsmallamountsofloads
forshortperiodsoftime.
Applicableto:FlexiblepouchesandBlisterPacks.
Limitation : Applies only to gas or liquid filled packs, or those that can be
filled with water for testing. Cannot be directly used for testing pouches
filledwithpowderorsolidproducts.
TestMethod:Thereare2basicmethodsoftest.
1)StaticCompressionTest,whereapackageisloadeduptoapredetermined
level,heldthereforapredeterminedtimeperiodandthenrelaxed.Thismay
ormaynotleadtoaburst.
2) DynamicCompressionTest, where a package is loaded incrementally till
itcannotbeartheloadanylongerandeventuallyburstsopen.
www.PackTest.com
Summary :This test in principle is similar to the Pouch CompressionTest,
except that the pouches here are subjected to internal air pressure in lieu of
external force. The internal burst test is used as a good overall test for a
hermetic seal including an indication of correct heat sealing conditions and
a measure of the ability of a package to withstand transportation and
handling.
Applicableto:FlexiblepouchesandBlisterPacks.
Limitation : This test is performed on empty packs only and cannot be
performedonproductfilledpacks.
Test Method : Sample is mounted in a burst test which internally and
increasinglypressurizesapackageuntilanareaofthepackagesealaround
the perimeter “bursts” open in responseto pressurization.Visually examine
the tested package and note the position and type of failure, as well as the
pressure at which the failure occurred. If the seals open, then the weakest
seal.Ifthelaminateruptures,notetheresultasaLaminateFailure.
TestStandard:JETRO/CFIA/ASTMF2054
Pouch BurstTest (a.k.a. Internal BurstTest)
Vacuum LeakageTest
www.PackTest.com
Summary : Package integrity is often an important characteristic of
package performance. Breaches of package integrity may permit
substances to enter or contents to escape packages. A Leak means an
opening in a flexible package that, contrary to intention, either lets
contentsescapeorpermitssubstancestoenter.
Applicable to : Any non-porous package such as Pouches, Blister Packs,
Cans, Bottles, etc.This test can also help understand the performance of a
package when transported through non-pressurized air cargo or when it is
usedathighaltitudes(lowatmosphericpressures).
You must have witnessed the puffed up pouches of dairy creamer (milk
powder)orsingle-servemilkblisterpacks,servedwithteainaircrafts.Ifthe
pouches were not strong enough, they would have burst open at these low
pressureconditions.
Limitation : This test is can only detect leaks due to reasonable large
pinholes or gaps which can allow the fluid or gas to pass out and / or water
toenterthepackage.Thistestisnotsuitablefordetectingmicroleakagesor
for testing packages containing high viscosity fluids.This test also cannot
beusedtotestvacuumsealedpacks.
TorqueTest
www.PackTest.com
Summary : Package integrity in rigid packaging such as Bottles has less
chances of being hampered due to pinholes and more chances of leaks due
tolooselyfittingclosures.Itisimportantthatthebottlesclosuresshouldbe
appliedwithanoptimumtorque.
EffectsofApplicationTorque:
LowApplicationTorque=LowRemovalTorque.
This may allow closures will further become loose due to vibrations during
transport and handling. And this will lead to leakages or product
contamination.
HighApplicationTorque=HighRemovalTorque.
This can lead to discomfort to the user in opening the bottle and dispensing
theproduct.
ExtraHighApplicationTorque=ClosureBreakorThreadSlip.
This can lead to the closure cracking or threads overlapping and then
slipping,bothofwhicharebadnews.
Top Load / CompressionTest
www.PackTest.com
Summary : Rigid Packaging such as Plastic Bottles (or Jars) are named so
because they have remain erect and presentable. Poor distribution in
material across the walls of the plastic bottles defines the rigidity of the
bottleatthatparticularweight.
The bottles may or may not be expected to take stacking loads if placed in
corrugated cartons. But bottles will need to take stacking loads if packed in
Shrink-wrappedTrays or Bundles and in this case theirTop Load carrying
capacity(orcompressionstrength)shouldbemuchhigher.
Applicable to : Plastic Bottles / Jars. Can also be used on paperboard
cartons,cups,trays,cansetc
Test Method : The bottle (generally empty) is placed in a compression
tester of suitable capacity and pressed until it cannot bear the load and
buckles.The peak load is captured alongwith the deflection at that point.
Theloadshouldbehighanddeflectionlow.
Magnetic BottleWallThicknessGauge
www.PackTest.com
MagneticThickness Gauges need a small steel ball to be placed inside the
bottleandtheprobeoutside.
The ball gets attracted to the magnetic probe and uses the hall-effect
principletomeasurethedistancebetweentheballandtheprobe.
This is the most versatile equipment and doesnot need re-calibration for
differentsubstrates.
The only limitation is that it cannot measure thickness of ferrous material.
But since ferrous (steel) packaging (drums) is not used commonly, it is not a
problem.There are special Ferrous / Steel Drum wall thickness devices for
thisparticularpurpose.
Headspace Gas Analysis (O2 Measurement)
www.PackTest.com
Summary : Modified Atmosphere Packaging (MAP) is now used commonly to enhance the shelf life of food and
pharmaceuticalproductsthataresensitivetothepresenceofOxygenorothergases.TheprocessofMAPinvolvesflushing
of nitrogen (or other gas / mixes) to displace the air inside the package. Sometimes the flushing happens incorrectly or
inadequately thereby allowing an undesirable amount of oxygen to remain inside the package and reduce the shelf life or
stabilityoftheproduct.
Test Method : A septum seal sticker is applied to the package (pouch / blister / tetra-pack / bottle, etc and a needle in
pushed through it.The gas inside is allowed to come out through the needle and is analysed by anOxygen (or other gas)
sensor.TheinstrumentshowstheO2%directly.
Ambientairhas20.9%oxygen.MAPtargetstoflushoutthisairandbringdowntheO2leveltounder1.5%.PresenceofO2
inexcessof2%canhaveadegradingeffectinproductstabilityandshelflife.
www.PackTest.com
Headspace Gas Analysers
Moisture Measurement (Oven)
www.PackTest.com
SamplesarefirstweighedandthenkeptinanOven@105±2ºCfor2hours.
Thelossinweightisfoundoutandmoisture%calculatedas:
Moisture%=(LossinWeight/OriginalWeight)x100
This test works on the principle called “Loss On Drying” (or LOD in short)
and is the most scientific way to testing moisture content or average
moisture.
Oven method is the most authentic method but takes a lot of time. Test
reportsshouldbebasedonthismethodonly.
www.PackTest.com
Samples are penetrated with an electronic device which measure the
electrical resistance between 2 penetration points. Since electrical
resistance is related to the moisture in the substrate, the correlation can be
established.ThesedevicesareknownastheInstantMoistureMeters.
They are the quickest way to detect moisture %, but it is to be noted that
presence of any contaminant in the paper (usually in recycled paper) will
have an effect on the electrical resistance. Also paper from different wood
types will have slightly different properties and hence the moisture meter
willnotbeaveryaccuratetestmethod.
Further when testing corrugated boards, the moisture meter will tend to
give you the peak moisture (because it measures the least electrical
resistance)fromamongstallthelayers/pliesoftheboard.
Eg. If we test a 5 ply corrugated board which as 12-10-10-10-10moisture %
in its layers, the Instant Moisture Meter will show a reading of 12%,
whereastheOven(LODmethod)willgiveyouaresultof10.4%
Instant Moisture Meters are not the most correct method but offer quick
results which may be good enough for in-process decisions and quick
checks.
Moisture Measurement (Instant Meters)
www.PackTest.com
Bursting StrengthTest of Corrugated Board
Summary : One of the most common test methods of the packaging industry in India is the Bursting StrengthTest.The
bursting strength of combined board is primarily an indication of the character of the materials used in manufacturing a
fiberboardboxandhasvalueinthisrespect.
ThereisageneralmisconceptionthatahigherBSmeansabettercarton.
Unfortunately this is a “Material Test” only and doesnot in any way guarantee the performance of the shipper carton
formed out of such material.You can have a lower BS corrugated carton having a better compression strength than a high
BScarton.
International standard specify thatTriple-wall corrugated board (7 Ply) cannot be tested suitably by the bursting method.
Testing of double-wall board (5 Ply) is of questionable accuracy since it is rarely possible to get sufficiently simultaneous
bursts of the multiple facings.The test is simple and rapid to execute, but it must be recognized that it is subject to serious
errorsifinstrument,diaphragm,andgagesarenotproperlymaintainedorifimproperproceduresareused.
Bursting StrengthTest of Corrugated Board
www.PackTest.com
TestMethod:
The test specimen is clamped in a BS Tester and gradually increasing
hydrostatic pressure is applied perpendicular to the face of the sample
through a rubber diaphragm till the sample cannot bear the pressure and
bursts.
ThepeakburstpressureisrecordedastheBurstingStrength.
TestStandard:TAPPIT-810
CompressionTest of CorrugatedShippers
-
www.PackTest.com
Summary:Acorrugatedshipper/carton’sprimarypurposeistoprotectthe
unit packaging inside and prevent any undue stress to reach the product.
The carton has to withstand the stress of stack load in warehousing and
transportation. If the carton is stronger than the stack load, the products
will survive. If the carton is weak, the carton will collapse and pass on the
loadtotheinnerpacks.
CartonCompressionSpecification=StackingLoadxSafetyFactor.
Safety factor is usually between 3-7 and depends on a lot of factors
including product fragility, product cost, distribution cycle, transit period,
transportationmethods,etc.
This test is a typical “PerformanceTest” and a good compression strength
directlysignifiesagoodcarton.
Test Method :The test specimen is placed between 2 parallel platens of a
compression tester and pressed.The max load it can bear before the carton
collapsesisrecordedastheCompressionStrength.
TestStandard:TAPPIT-804/ASTMD642/ISO12048/IS7028
www.PackTest.com
Summary :Generally a product is placed in its primary packaging and then
in a secondary packaging before being dispatched in truck or similar
transport vehicle.Sometimes the transportation is also through Rail orAir.
Inorderfortheproducttoreachtheconsumerintactithastobedesignedto
withstandthehazardsofaroad/rail/airjourney.
Themostcommonfailuresareseenasbreakages,leakages,scratches,etc.
Vibration tests are generally done on filled shipping containers. Such tests
may be used to assess the performance of a container, with its interior
packing and means of closure, both in terms of its strength and of the
protectionitprovidesitscontentswhenitissubjectedtovibrationsuchasit
experiences in transportation. These procedures are suitable for testing
containers of any form, material, kind, design of interior packing, means of
closure,andanysizeandweight.Theyarenotintendedfordeterminingthe
response of products to vibration for product design purposes, nor are they
intended for tests of products in their operational configuration as other
moresuitableproceduresareavailableforthesepurposes.
TransportWorthinessTest /VibrationTest
DropTest
www.PackTest.com
Summary : Another important requirement for packaging is to be able to bear accidental drops which are the most
commoneffectsofincorrecthandlingpractices.Unitpacksmaygetsubjectedtodropsduringvariousstagesofproduction,
packing and even while being loaded on store shelves by the store staff or while being picked up from the shelf by the
consumer.The package must keep the contents intact. Similarly, the Secondary orTransport Packs may get subjected to
accidentaldropsduringtransportandwarehousingactivities.
This test is intended for use in evaluating the capability of a container to withstand the sudden shock resulting from a free
fall, or to evaluate the capability of a container and its inner packing to protect its contents during the sudden shock
resultingfromafreefall.Thistestmethodmayalsobeusedtocomparetheperformanceofdifferentpackagedesigns.This
testmethodmayalsopermitobservationoftheprogressivefailureofacontainerandthedamagetoitscontents.
Thetesthelpassess:
1) Durabilityofinternalpackages
2) EffectivenessofPartitioningandCushioningarrangements
3) ProductFragility
4) DropFailureHeight(whichcanbeusedtospecifythemaxstorageheightoftheproduct)
DropTest
TestMethod:
Individual Unit Packages or Secondary Packages are dropped at different
heightsanddifferentorientationstoassessfordurability.
Thetestheightisgenerallytheexpectedheighttheproductcanbedropped
from in real life or slightly higher. Heavier packages are generally handled
at lower heights and hence dropped from lower heights. Likewise, light
weights products are placed higher in shelfs or stacked higher, hence they
needtobedroppedfromhigherheights.
TestStandard:ASTMD5276
www.PackTest.com
Our Client worldwide
Austria
Bahrain
Bangladesh
Denmark
Egypt
France
Germany
India
Indonesia
Jordan
Kazakhstan
Kenya
Kuwait
Malaysia
Mexico
Nepal
New Zealand
Nigeria
Oman
Pakistan
Philippines
Poland
Qatar
Russia
Saudi Arabia
South Africa
Sri Lanka
Syria
Tanzania
Thailand
Turkey
Uganda
United Arab Emirates
United Kingdom
United States of America
Vietnam
Yemen
Zambia
TEST TECHNO CONSULTANTS
K-1, 23/2, G.I.D.C Ranoli, Vadodara - 391 350, Gujarat, INDIA
www.PackTest.com
PackTest

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Food Packaging Testing Equipment by PackTest

  • 1. FOOD PACKAGING TESTS & EQUIPMENTwww.PackTest.com PackTest
  • 2. www.PackTest.com PackagingTesting Equipments TestTechno Consultants was incorporated in 1989 and has become India’s Leading & Largest manufacturer & exporter of QualityTesting Equipment for the Paper, Plastic and Packaging Industry.We offer the world’s widest range of CompressionTesters,TensileTester,TorqueTesters, BurstTesters and many other MaterialTesting Equipment for Paper, Plastic and converted products used in Packaging. Whatever the Application…We provideTesting Equipment specially designed to test Packaging Material as well as Formed Packages & ancillaries for the following :Compression, Crush, Burst Strength,Torque Force,Tensile, Elongation, Peel, Seal, Friction, Shear, Adhesion,Tackiness,Texture, Drop, Impact,Vibration, Leak, Print, Scuff, Abrasion, and many more.. Whatever the Industry…Our Equipments form the life line of Quality Assurance / R&D / Packaging Development departments of almost all sectors of the industry involved in the manufacture of Packaging or heavy users of Packaging & Packaging Materials. Solutions
  • 3. GSMTest Summary :GSM is one of the most basic tests which stands forGrams per Square Meter. It is also known as the “grammage” and is actually the weight of 1 square meter of sample. Most paper is bought and sold in accordance with its mass per unit area, and therefore the grammage has greatsignificancebothtotheconsumerandtheproducerindefiningprice. Applicableto:Paper Test Method : A sample of 100cm² area (usually a square of 10x10cm or a round of 11.284cm diameter) is cut and weight accurate to 0.01gm resolutionandmultipliedby100togiveyoutheresulting/m²orgsm TestStandard:TAPPIT-410/ISO536/IS1060 www.PackTest.com
  • 4. ThicknessTest www.PackTest.com Summary :Thickness is an important property of paper, paperboard, foil, filmorLaminates,andvariationsinthicknesscanleadtovariationsintheir othermechanicalpropertiessuchasstiffness,permeability,etc. Thickness is defined as the perpendicular distance between the two principalsurfacesofthesamplesubstrate. Applicableto:Paper,Paperboards,Film,Foils,Laminates Test Method : A sample is measured in a Dial Type or Digital Thickness Gauge mounted on a vertical stand with a weight (called as dead mass) on top.The weight exerts a constant pressure of 50 kPa (100 kPa as per ISO) at thecontactsurface(pointofmeasurement).Thisensureshighrepeatability in test results.Ordinary screw type micrometers are not to be used as they are highly operator dependent and any amount of excess pressure can compressthespecimenandgivelowerresults. TestStandard: TAPPIT-411/ASTMD645/ASTMF2251/ISO534/IS1060
  • 5. www.PackTest.com PinholeTest Summary : Aluminum foils are used in food packaging laminates to enhance the barrier properties of the package and to protect the contents from gas / moisture permeation and also from light. Thinner gauges of aluminum foil contain pinholes through which moisture and oxygen from theenvironmentcanenterthepackageacceleratingthedegradationofthe contents.Presenceofexcessivepinholesinthefoilwillsignificantlyhamper theshelflifeofsuchproducts. Applicableto:FoilsandFoilLaminates TestMethod:Asampleoffoilorfoillaminateisplacedonaglassplatewith lightsunderit.ThisapparatusisalsocalledasaLightBoxandusuallyhasa hood on top to cover the sample. Pinholes will be visible as white spots as light from underneath the sample will pass through the holes while the opaque sample blocks the remaining light. Count the number of pinholes persquaremeterofsample. TestStandard:ASTMB926/IS:15392-2003
  • 6. www.PackTest.com DelaminationTest (a.k.a. Peel BondTest) Summary :Laminatesaremadebybondingtogethertwoormorelayersof materialormaterials.Theirperformanceisoftendependentontheabilityof the laminate to function as a single unit. If the plies have not been properly bondedtogether,theperformancemaybeadverselyaffected. Applicableto:FlexibleLaminates Test Method : Ply separation is initially started mechanically by the application of heat or by using a solvent. The separated plies of the test specimenareplacedintothegripsofatensiletestingmachine.Thegripsare then separated and the force required to further separate the plies is defined as bond strength.The most difficult part of the test is the sample preparation itself which is very time consuming. Some layers of the laminatearesothinthatyouwillrarelygetaproperpeeltestdone. TestStandard:ASTMF904
  • 7. www.PackTest.com Summary : Seal strength is a quantitative measure for use in process validation,processcontrolandcapability.Sealstrengthisnotonlyrelevant to opening force and package integrity, but to measuring the packaging processes’ ability to produce consistent seals. Seal strength at some minimum level is a necessary package requirement, and at times it is desirabletolimitthestrengthofthesealtofacilitateeasyopening. Applicableto:FlexibleLaminatesandformedPouches. Test Method : Samples are cut from a formed pouch. Alternatively laminates can be sealed with controlled temperature, pressure and dwell- time to create sample seals.The test specimen is then gripped in a tensile testing machine. The grips are then separated and the force required to separatethesealisdefinedassealstrength. You can use a Lab Heat Sealer and aTensileTester to create samples using different materials, temperature, pressure and dwell-time setting and find thecombinationofferingthebestsealstrength. TestStandard:ASTMF88 Seal StrengthTest ( a.k.a Heat SealabilityTest)
  • 8. www.PackTest.com For most food applications a permeation measurement system would have to be able to detectinameasurementrangeof0.05-2000cm3/ (m2dbar). OTR Permeation Analyser by PreSens (Germany) A new measurement system for testing synthetic materials on oxygen permeabilitywasdeveloped. Unlike the currently used systems with electrochemical or barometrical sensorsitwasdesignedforopticalmeasurement. The Fibox 4 trace together with chemical optical sensors was applied to detect trace oxygen concentrations and validate the new measurement system.Apartfromanalreadyavailablesensortypedifferentothertypesof sensor material were tested to develop an oxygen sensor with an improved limitofdetectionforhighbarrierpermeationmeasurements. Thissensortype-PSt9-togetherwiththemeasurementcellsseemstobea promising solution for easy, cost effective permeation measurements in technicalapplications. Pst6Range:10-²to10-⁷cm³ (STP)/(m²dbar) Pst9Range:10-³and100cm³ (STP)/(m²dbar)
  • 9. www.PackTest.com Coefficient of Friction (C.O.F.)Test Summary : Flexible packaging is usually done on Vertical or Horizontal Form-Fill-Seal (FFS) machines in which the roll of film or laminate comes in contact with itself or other metallic /non-metallic components of the FFS machine.The contact generates friction which can inhibit the material to runproperlyonthemachinesandachievedesiredproductionspeeds. Measurements of frictional properties may be made on a film/laminate whenslidingoveritselforoveranothersubstance(usuallystainlesssteel). Theamountoffrictionrequiredtobeovercometoinitiatemotioniscalledas the Static Coefficient of Friction and the amount of friction required to be overcome to continue the motion is called as the Kinetic Coefficient of Friction. Applicableto:PlasticFilmandLaminates. Test Method : A sled weighing 200 ± 5 g is wrapped around with the test specimen and made to slide over a similar substrate or stainless steel surface with a speed of 150 ± 30mm/min.The initial and average drag force (ingrams)isrecordedanddividedbythesledweight(200g)tocalculatethe staticandkineticCOFrespectively. TestStandard:ASTMD1894
  • 10. www.PackTest.com Ink RubTest / ScuffTest (Print QualityTest) Summary:Packagingisknownasa“SilentSalesman”.Thepackagehasto be attractive enough for the consumer to feel compelled to pick it up from the shelf. It also has to display technical information about the product, such are contents, packing dates, expiry info, etc as mandated by law. However the packaging can get scuffed or rubbed during various stages of production, transportation and distribution. This test allows us to create standardized conditions of rubbing to evaluate the performance of different test specimens. Can also be used to evaluate the efficacy of varnishingoranyotherspecializedcoatingsontheprintedsurface. Applicable to :All types of surface printed packaging such as Foils, Labels, PrintedCartons,andevenbatchcodingonpouches. Limitation:Canbeusedfortestingmaterialinsheetformonly.Thoughthe testcanalsobemodifiedforcurvedsurfacesofrigidpackaging.
  • 11. www.PackTest.com PATRA RubTest / Sutherland RubTest TestMethod:Therearetypically2methodoftesting 1)RotaryRubbingusing2circulardiscsofsize2and4.5Inches. 2)LinearRubbingusing2rectangularsamplesofspecifiedsizes. RotaryRubtestismorecommonlyknownasthePatra/PiraRubTestandis the preferred test method for Rigid substrates like paperboards.This test cannot be done successfully on thinner and more flexible substrates which crumpleuponrotaryrubbing. Linear Rub test is more commonly known as theSutherland RubTest and is anall-roundertestsinceitcanbeusedonallthinorthickspecimens. TestStandard: RotaryRub:BritishStandardsBS-3110 LinearRub:BritishStandardsBS-3110andASTMD5264
  • 12. www.PackTest.com Pouch CompressionTest (aka. Load BurstTest) Summary : When a shipper carton fails, stacking loads can be transmitted ontothepackage.Henceaflexibleorsemiflexiblepackage(suchasapouch orblisterpack)shouldhavetheabilitytowithstandsmallamountsofloads forshortperiodsoftime. Applicableto:FlexiblepouchesandBlisterPacks. Limitation : Applies only to gas or liquid filled packs, or those that can be filled with water for testing. Cannot be directly used for testing pouches filledwithpowderorsolidproducts. TestMethod:Thereare2basicmethodsoftest. 1)StaticCompressionTest,whereapackageisloadeduptoapredetermined level,heldthereforapredeterminedtimeperiodandthenrelaxed.Thismay ormaynotleadtoaburst. 2) DynamicCompressionTest, where a package is loaded incrementally till itcannotbeartheloadanylongerandeventuallyburstsopen.
  • 13. www.PackTest.com Summary :This test in principle is similar to the Pouch CompressionTest, except that the pouches here are subjected to internal air pressure in lieu of external force. The internal burst test is used as a good overall test for a hermetic seal including an indication of correct heat sealing conditions and a measure of the ability of a package to withstand transportation and handling. Applicableto:FlexiblepouchesandBlisterPacks. Limitation : This test is performed on empty packs only and cannot be performedonproductfilledpacks. Test Method : Sample is mounted in a burst test which internally and increasinglypressurizesapackageuntilanareaofthepackagesealaround the perimeter “bursts” open in responseto pressurization.Visually examine the tested package and note the position and type of failure, as well as the pressure at which the failure occurred. If the seals open, then the weakest seal.Ifthelaminateruptures,notetheresultasaLaminateFailure. TestStandard:JETRO/CFIA/ASTMF2054 Pouch BurstTest (a.k.a. Internal BurstTest)
  • 14. Vacuum LeakageTest www.PackTest.com Summary : Package integrity is often an important characteristic of package performance. Breaches of package integrity may permit substances to enter or contents to escape packages. A Leak means an opening in a flexible package that, contrary to intention, either lets contentsescapeorpermitssubstancestoenter. Applicable to : Any non-porous package such as Pouches, Blister Packs, Cans, Bottles, etc.This test can also help understand the performance of a package when transported through non-pressurized air cargo or when it is usedathighaltitudes(lowatmosphericpressures). You must have witnessed the puffed up pouches of dairy creamer (milk powder)orsingle-servemilkblisterpacks,servedwithteainaircrafts.Ifthe pouches were not strong enough, they would have burst open at these low pressureconditions. Limitation : This test is can only detect leaks due to reasonable large pinholes or gaps which can allow the fluid or gas to pass out and / or water toenterthepackage.Thistestisnotsuitablefordetectingmicroleakagesor for testing packages containing high viscosity fluids.This test also cannot beusedtotestvacuumsealedpacks.
  • 15. TorqueTest www.PackTest.com Summary : Package integrity in rigid packaging such as Bottles has less chances of being hampered due to pinholes and more chances of leaks due tolooselyfittingclosures.Itisimportantthatthebottlesclosuresshouldbe appliedwithanoptimumtorque. EffectsofApplicationTorque: LowApplicationTorque=LowRemovalTorque. This may allow closures will further become loose due to vibrations during transport and handling. And this will lead to leakages or product contamination. HighApplicationTorque=HighRemovalTorque. This can lead to discomfort to the user in opening the bottle and dispensing theproduct. ExtraHighApplicationTorque=ClosureBreakorThreadSlip. This can lead to the closure cracking or threads overlapping and then slipping,bothofwhicharebadnews.
  • 16. Top Load / CompressionTest www.PackTest.com Summary : Rigid Packaging such as Plastic Bottles (or Jars) are named so because they have remain erect and presentable. Poor distribution in material across the walls of the plastic bottles defines the rigidity of the bottleatthatparticularweight. The bottles may or may not be expected to take stacking loads if placed in corrugated cartons. But bottles will need to take stacking loads if packed in Shrink-wrappedTrays or Bundles and in this case theirTop Load carrying capacity(orcompressionstrength)shouldbemuchhigher. Applicable to : Plastic Bottles / Jars. Can also be used on paperboard cartons,cups,trays,cansetc Test Method : The bottle (generally empty) is placed in a compression tester of suitable capacity and pressed until it cannot bear the load and buckles.The peak load is captured alongwith the deflection at that point. Theloadshouldbehighanddeflectionlow.
  • 17. Magnetic BottleWallThicknessGauge www.PackTest.com MagneticThickness Gauges need a small steel ball to be placed inside the bottleandtheprobeoutside. The ball gets attracted to the magnetic probe and uses the hall-effect principletomeasurethedistancebetweentheballandtheprobe. This is the most versatile equipment and doesnot need re-calibration for differentsubstrates. The only limitation is that it cannot measure thickness of ferrous material. But since ferrous (steel) packaging (drums) is not used commonly, it is not a problem.There are special Ferrous / Steel Drum wall thickness devices for thisparticularpurpose.
  • 18. Headspace Gas Analysis (O2 Measurement) www.PackTest.com Summary : Modified Atmosphere Packaging (MAP) is now used commonly to enhance the shelf life of food and pharmaceuticalproductsthataresensitivetothepresenceofOxygenorothergases.TheprocessofMAPinvolvesflushing of nitrogen (or other gas / mixes) to displace the air inside the package. Sometimes the flushing happens incorrectly or inadequately thereby allowing an undesirable amount of oxygen to remain inside the package and reduce the shelf life or stabilityoftheproduct. Test Method : A septum seal sticker is applied to the package (pouch / blister / tetra-pack / bottle, etc and a needle in pushed through it.The gas inside is allowed to come out through the needle and is analysed by anOxygen (or other gas) sensor.TheinstrumentshowstheO2%directly. Ambientairhas20.9%oxygen.MAPtargetstoflushoutthisairandbringdowntheO2leveltounder1.5%.PresenceofO2 inexcessof2%canhaveadegradingeffectinproductstabilityandshelflife.
  • 20. Moisture Measurement (Oven) www.PackTest.com SamplesarefirstweighedandthenkeptinanOven@105±2ºCfor2hours. Thelossinweightisfoundoutandmoisture%calculatedas: Moisture%=(LossinWeight/OriginalWeight)x100 This test works on the principle called “Loss On Drying” (or LOD in short) and is the most scientific way to testing moisture content or average moisture. Oven method is the most authentic method but takes a lot of time. Test reportsshouldbebasedonthismethodonly.
  • 21. www.PackTest.com Samples are penetrated with an electronic device which measure the electrical resistance between 2 penetration points. Since electrical resistance is related to the moisture in the substrate, the correlation can be established.ThesedevicesareknownastheInstantMoistureMeters. They are the quickest way to detect moisture %, but it is to be noted that presence of any contaminant in the paper (usually in recycled paper) will have an effect on the electrical resistance. Also paper from different wood types will have slightly different properties and hence the moisture meter willnotbeaveryaccuratetestmethod. Further when testing corrugated boards, the moisture meter will tend to give you the peak moisture (because it measures the least electrical resistance)fromamongstallthelayers/pliesoftheboard. Eg. If we test a 5 ply corrugated board which as 12-10-10-10-10moisture % in its layers, the Instant Moisture Meter will show a reading of 12%, whereastheOven(LODmethod)willgiveyouaresultof10.4% Instant Moisture Meters are not the most correct method but offer quick results which may be good enough for in-process decisions and quick checks. Moisture Measurement (Instant Meters)
  • 22. www.PackTest.com Bursting StrengthTest of Corrugated Board Summary : One of the most common test methods of the packaging industry in India is the Bursting StrengthTest.The bursting strength of combined board is primarily an indication of the character of the materials used in manufacturing a fiberboardboxandhasvalueinthisrespect. ThereisageneralmisconceptionthatahigherBSmeansabettercarton. Unfortunately this is a “Material Test” only and doesnot in any way guarantee the performance of the shipper carton formed out of such material.You can have a lower BS corrugated carton having a better compression strength than a high BScarton. International standard specify thatTriple-wall corrugated board (7 Ply) cannot be tested suitably by the bursting method. Testing of double-wall board (5 Ply) is of questionable accuracy since it is rarely possible to get sufficiently simultaneous bursts of the multiple facings.The test is simple and rapid to execute, but it must be recognized that it is subject to serious errorsifinstrument,diaphragm,andgagesarenotproperlymaintainedorifimproperproceduresareused.
  • 23. Bursting StrengthTest of Corrugated Board www.PackTest.com TestMethod: The test specimen is clamped in a BS Tester and gradually increasing hydrostatic pressure is applied perpendicular to the face of the sample through a rubber diaphragm till the sample cannot bear the pressure and bursts. ThepeakburstpressureisrecordedastheBurstingStrength. TestStandard:TAPPIT-810
  • 24. CompressionTest of CorrugatedShippers - www.PackTest.com Summary:Acorrugatedshipper/carton’sprimarypurposeistoprotectthe unit packaging inside and prevent any undue stress to reach the product. The carton has to withstand the stress of stack load in warehousing and transportation. If the carton is stronger than the stack load, the products will survive. If the carton is weak, the carton will collapse and pass on the loadtotheinnerpacks. CartonCompressionSpecification=StackingLoadxSafetyFactor. Safety factor is usually between 3-7 and depends on a lot of factors including product fragility, product cost, distribution cycle, transit period, transportationmethods,etc. This test is a typical “PerformanceTest” and a good compression strength directlysignifiesagoodcarton. Test Method :The test specimen is placed between 2 parallel platens of a compression tester and pressed.The max load it can bear before the carton collapsesisrecordedastheCompressionStrength. TestStandard:TAPPIT-804/ASTMD642/ISO12048/IS7028
  • 25. www.PackTest.com Summary :Generally a product is placed in its primary packaging and then in a secondary packaging before being dispatched in truck or similar transport vehicle.Sometimes the transportation is also through Rail orAir. Inorderfortheproducttoreachtheconsumerintactithastobedesignedto withstandthehazardsofaroad/rail/airjourney. Themostcommonfailuresareseenasbreakages,leakages,scratches,etc. Vibration tests are generally done on filled shipping containers. Such tests may be used to assess the performance of a container, with its interior packing and means of closure, both in terms of its strength and of the protectionitprovidesitscontentswhenitissubjectedtovibrationsuchasit experiences in transportation. These procedures are suitable for testing containers of any form, material, kind, design of interior packing, means of closure,andanysizeandweight.Theyarenotintendedfordeterminingthe response of products to vibration for product design purposes, nor are they intended for tests of products in their operational configuration as other moresuitableproceduresareavailableforthesepurposes. TransportWorthinessTest /VibrationTest
  • 26. DropTest www.PackTest.com Summary : Another important requirement for packaging is to be able to bear accidental drops which are the most commoneffectsofincorrecthandlingpractices.Unitpacksmaygetsubjectedtodropsduringvariousstagesofproduction, packing and even while being loaded on store shelves by the store staff or while being picked up from the shelf by the consumer.The package must keep the contents intact. Similarly, the Secondary orTransport Packs may get subjected to accidentaldropsduringtransportandwarehousingactivities. This test is intended for use in evaluating the capability of a container to withstand the sudden shock resulting from a free fall, or to evaluate the capability of a container and its inner packing to protect its contents during the sudden shock resultingfromafreefall.Thistestmethodmayalsobeusedtocomparetheperformanceofdifferentpackagedesigns.This testmethodmayalsopermitobservationoftheprogressivefailureofacontainerandthedamagetoitscontents. Thetesthelpassess: 1) Durabilityofinternalpackages 2) EffectivenessofPartitioningandCushioningarrangements 3) ProductFragility 4) DropFailureHeight(whichcanbeusedtospecifythemaxstorageheightoftheproduct)
  • 27. DropTest TestMethod: Individual Unit Packages or Secondary Packages are dropped at different heightsanddifferentorientationstoassessfordurability. Thetestheightisgenerallytheexpectedheighttheproductcanbedropped from in real life or slightly higher. Heavier packages are generally handled at lower heights and hence dropped from lower heights. Likewise, light weights products are placed higher in shelfs or stacked higher, hence they needtobedroppedfromhigherheights. TestStandard:ASTMD5276 www.PackTest.com
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