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SHEET EXTRUSION
World Class Extrusion Systems   Process Troubleshooting Guidelines
SHEET EXTRUSION                                Table of Contents
Process Troubleshooting Guidelines             Problem Type                                                                                                                                      Page
PTi’s Sheet Extrusion Process Trouble-         Brittleness in Sheet ............................................................................................................................2
shooting Guidelines offers solutions to        Contamination On Sheet .....................................................................................................................2
many of the problems that sheet produc-        Curled Sheet in the Transverse Direction..............................................................................................3
ers face in their day-to-day operations.       Curled Sheet in the Machine Direction .................................................................................................3
We trust this guide will assist you in         Degradation On One Layer..................................................................................................................3
creating quality products for today’s chal-    Dimples on the Sheet Surface .............................................................................................................4
lenging sheet extrusion applications.          Discolored Sheet ................................................................................................................................6
                                               Herringbone Patterns .........................................................................................................................6
                                               High or Inconsistent Sheet Orientation .................................................................................................7
                                               Inconsistent or Patchy Gloss ...............................................................................................................7
                                               Insufficient Sheet Toughness...............................................................................................................8
                                               Layers Do Not Adhere.........................................................................................................................9
PROCESSING TECHNOLOGIES, LLC                   Layer Too Thick ..................................................................................................................................9
                                               Layer Too Thin ...................................................................................................................................9
2655 White Oak Circle                          Lines in the Machine Direction of the Sheet .........................................................................................9
Aurora, IL 60502-9674                          Lines in the Transverse Direction of the Sheet ......................................................................................10
                                               Low Gloss on Sheet ...........................................................................................................................11
ph 630.585.5800
                                               Non-Uniform Sheet Color ....................................................................................................................11
fx 630.585.5855                                Parabolic Lines in the Machine Direction .............................................................................................12
www.ptiextruders.com                           Poor Transparency .............................................................................................................................12
                                               Rough Surface Texture .......................................................................................................................13
© 2007 Processing Technologies, LLC            Surging .............................................................................................................................................14
PTi reserves the right to make changes to      Thickness Variation in the Machine Direction .......................................................................................15
this document without prior notice.            Thickness Variation in the Transverse Direction ....................................................................................16
                                               Uneven Layer Thickness in the Transverse Direction .............................................................................16
Note: This document is not intended as a       Uneven Layer Thickness in the Machine Direction ................................................................................17
substitute for professional judgement and      Vent Flow ..........................................................................................................................................18
operational expertise of the user. No war-     Wave Instability ..................................................................................................................................18
ranty is implied. Actual results may vary.
                                               Zigzag Instability ................................................................................................................................18


                                              Sheet Extrusion Process Troubleshooting Guidelines
Problem                  Cause                        Solution
Brittleness in Sheet     Too Much Orientation         Adjust roll gap to proper setting. ( Typically the first gap is
                                                      aproximately 0.001” to 0.002” UNDER the desired sheet
                                                      thickness and the second gap should be the same or larger
                                                      than the desired sheet thickness)
                                                      See solutions to Orientation.


                         Cold Rolls                   Increase roll temperatures.

                         Poor Melt Consistency        Use static mixer in the transfer line.

                                                      Reduce regrind levels.

                                                      Increase head pressure to improve mixing.

                                                      Reduce additives, i.e. color concentrate.

Contamination On Sheet   Equipment Problem            Check for ruptured screens.

                                                      Check for loss of plating, which can result in black specks.

                                                      See solutions to Discolored Sheet.

                         Material Problem             Check regrind stream for contamination.

                                                      Check airway system and hopper loading procedures for
                                                      contamination.

                                                      Check incoming resin for dirt, packaging scraps, gels, etc.

                                                      Remove excess fines from resin.


                         Static Electricity           Thoroughly clean all the areas around the line.

                                                      Dissipate static charge on sheet.



                          Sheet Extrusion Process Troubleshooting Guidelines                                            2
Problem                    Cause                           Solution
Contamination              Equipment Contamination         Clean conveyor idler rolls.
On Sheet, Cont’d.
                                                           Clean surface of chill rolls.
                           Degraded Material               Clean buildup from surface around die.
                           Falling On Sheet
                                                           Clean die lips.
Curled Sheet in the        Improper Roll Temperature       Raise temperature of the concave sheet surface.
Transverse Direction                                       (If sheet edges curl down and curling occurs “down stack,”
                                                           raise middle roll temperature. If sheet edges curl up, lower
                                                           middle roll temperature. Reverse recommendations when curl-
                                                           ing occurs “up stack.” In both cases change third roll tempera-
                                                           ture opposite to middle roll temperature changes.)

Curled Sheet in the Ma-    Excessive Pull-Roll Tension     Reduce pull roll speed.
chine Direction
                                                           Reduce pull roll tension.
Degradation On One Layer   Thermal Decomposition           Reduce head pressure to make screw more efficient by clean-
                                                           ing the screens, using a coarser mesh opening the die lip,
                                                           and/or shortening the transfer lines.

                                                           Reduce temperature at the end of extruder barrel and down-
                                                           stream equipment.

                                                           Check for dead spots and streamline flow passages by
                                                           employing sweep elbows and/or removing melt immersion
                                                           thermocouples.

                                                           Arrange sheet so that heat-sensitive layer is cooled on the chill
                                                           roll first.

                                                           Reduce contact with hot equipment--for example, encapsulate
                                                           heat sensitive polymer with another polymer.


                           Chemical Reaction               Use additives to stabilize the composition.


                            Sheet Extrusion Process Troubleshooting Guidelines                                             3
Problem                           Cause                           Solution
Degradation On One Layer,         Chemical Reaction               Remove troublesome additive such as color or regrind from the
Cont’d.                                                           extruder feed.

                                                                  Check for material compatibility in the coex structure.
Dimples on the Sheet Surface      Air Entrapment                  Decrease screw speed.
(Also called pits, depressions,   (Air collected in pockets
pock marks, buck shot and         causes voids in the hot         Reduce temperatures in the first and second barrel zones.
craters.)                         sheet which contract upon
                                  sheet cooling leaving se-       Unplug the vent if using two-stage screw.
                                  vere depressions. Can be
                                  more severe on vacuum           Remove fines from regrind.
                                  forming because depres-
                                  sions become drawn out.)        Check vacuum system for proper operation.

                                                                  Reduce hopper drying temperature.

                                                                  Maintain proper hopper level.

                                                                  Raise back pressure if using two-stage screw.

                                  Regrind feed stock              Change regrind particle size.

                                                                  Reduce regrind level to control bulk density factor.
                                  Moisture                        Increase drying time.

                                                                  Check dryer operation for proper dew point and desiccant
                                                                  regeneration.

                                                                  Increase drying temperature.

                                                                  Check vacuum system for proper operation.

                                                                  Use nitrogen blanket on the feed hopper.

                                                                  Use a drying hopper.

                                                                  Unplug the vent if using two-stage screw.

                                   Sheet Extrusion Process Troubleshooting Guidelines                                         4
Problem                         Cause                           Solution
Dimples on the Sheet Surface,   Volatiles                       Unplug the vent if using two-stage screw.
Cont’d.
                                                                Check vacuum system for proper operation.

                                                                Cool the melt to minimize volatilization due to decomposition.
                                Volatiles Entrapped             Adjust die-roll height to minimize the draping of the sheet
                                Between the Sheet and           on the roll.
                                the Roll
                                                                Check for hot spots on the die.

                                                                Increase or decrease roll temperature.

                                                                Increase ventilation to prevent entrapment.

                                                                Reduce melt temperature.

                                                                Unplug the vent if using two-stage screw.

                                                                Check vacuum system for proper operation.

                                                                Adjust die lips in region corresponding to the entrapment.

                                Insufficient Melt               Increase extrusion rate to fill the bank.
                                Bank at the Roll Tip
                                                                Adjust die restrictor bar and/or die lips to optimize flow
                                                                uniformity from die.

                                                                Decrease roll speed to build bank at the roll nip.

                                                                Optimize die temperatures to improve die flow.

                                                                Check for extruder surging.

                                                                Move die closer to roll nip.

                                                                Increase extrusion rate to fill the bank.


                                 Sheet Extrusion Process Troubleshooting Guidelines                                              5
Problem                         Cause                            Solution
Dimples on the Sheet Surface,   Insufficiently Clean Equipment   Dissipate static electricity to minimize dust pickup.
Cont’d.
                                                                 Clean chill-roll and polishing roll surface.

                                                                 Clean idler rolls in conveyor.
                                Cooling the Sheet too Quickly    Raise temperature of the roll in contact with the problem
                                                                 surface.

Discolored Sheet                Excessive Temperature or         Reduce last one or two barrel zone temperatures and/or
                                Residence Times                  reduce the die temperature.

                                                                 Check for proper operation of the heaters and thermocouples.

                                                                 Reduce the head pressure by changing to clean or coarse
                                                                 screens, and/or by opening up available valving, the die
                                                                 restrictor bar and/or lips.

                                Dirty Scrap or Regrind           Streamline flow path by using smooth transitions and/or el-
                                Re-extrusion Frequency           bows with longer bend ratio.

                                                                 Clean behind deckles on regular basis. If that fails then remove
                                                                 deckles.

                                                                 Check for loss of plating or other corrosion.

                                Insufficient Color Concen-       Add color concentrate at feed throat.
                                trate or Segregation of the
                                Color Concentrate in the         Increase color concentrate to specified level.
                                Feed Hopper
                                                                 Re-design hopper to get mass flow rather than funnel flow.



Herringbone Patterns            Inadequate Drying                Increase hopper drying time and/or hopper temperature to
(or “Chicken Tracks”),                                           improve drying of pellets
Discontinuous Lines


                                 Sheet Extrusion Process Troubleshooting Guidelines                                             6
Problem                           Cause                           Solution
High or Inconsistent Sheet        Roll Speed Too                  Increase extrusion rate.
Orientation (Can reduce physi-    High Relative to Die
cal properties of the sheet,      Throughput Rate                 Reduce chill roll speed.
resulting in localized stress
in the thermoformed part. Also,                                   Decrease die gap.
sheet may pull out of clamps
during thermoforming as the       Excessive Bank Size             Decrease extrusion rate.
sheet shrinks.)
                                                                  Increase chill roll speed.

                                  Incorrect Die/Nip               Align die face with roll center line.
                                  Distance
                                                                  Reduce die-nip distance to minimum settings.

                                  Pull Roll Tension               Increase or decrease pull roll speed.

                                  Incorrect Polymer               If the differential between the melt temperature is too wide,
                                  Cooling Rate                    raise the roll temperature and/or reduce the melt temperature.

                                                                  If melting temperature is too low, raise temperature on the last
                                                                  one or two barrel zones and/or raise die temperatures.

Inconsistent or                   Inconsistent                    Adjust Restrictor Bar.
Patchy Gloss                      Gauge
                                                                  Check for extruder surging.

                                                                  Adjust die lip.
                                  Excessive Melt                  Change screen-changer screens.
                                  Temperature
                                                                  Reduce temperatures in the last one or two barrel zones.

                                                                  Reduce die temperatures.




                                   Sheet Extrusion Process Troubleshooting Guidelines                                                7
Problem                         Cause                          Solution
Inconsistent or Patchy Gloss,   Non-uniform Roll               Check for hot spots on roll circumference and clean flow.
Cont’d.                         Temperatures
                                                               Check the delta temperature across the roll’s face. (Typically,
                                                               the cooling fluid should vary 2°F or less from roll inlet to roll
                                                               outlet.)


                                Volatile Entrapment Between    Adjust die lips in region corresponding to the entrapment.
                                Sheet and Roll
                                                               Increase ventilation.

                                                               Adjust roll height to minimize draping of sheet on roll.

                                                               Reduce melt temperature.

                                                               Check for hot spots on die.

                                                               Unplug vent if using a two stage screw.

                                                               Check for proper operation of vacuum system.

Insufficient Sheet Toughness    Brittle Layers Too Thick       Improve transverse sheet-thickness uniformity, especially at
                                                               edges of the sheet. (See solutions to Uneven Layer Thickness
                                                               in Transverse Direction.)

                                                               Switch to tougher polymers.

                                                               Reduce thickness of brittle layers.


                                Excessive Regrind              Use additives to restore toughness.

                                                               Reduce regrind level.

                                Orientation                    See solutions to Orientation Problems.




                                Sheet Extrusion Process Troubleshooting Guidelines                                                 8
Problem                         Cause                           Solution
  Layers Do Not Adhere           Adhesive Problems               Use an adhesive with higher tensile strength.

                                                                 Increase adhesive layer thickness.

                                                                 Use a separate resin layer for an adhesive or another type of
                                                                 adhesive (a lower viscosity adhesive, for example, will give
                                                                 better wetting).

                                                                 Increase the adhesive melt temperature.

                                                                 Increase the melt contact time.

                                 Improper Equipment Operation    Set chill roll speed to match polymer die-exit speed.


Layer Too Thick                  Over-Pumping                    Decrease output of the extruder feeding the layer.
                                 the Feedblock
                                                                 If output reduction in this extruder is not possible, speed up
                                                                 the other extruders.

Layer Too Thin                   Under-Pumping                   Increase output of the extruder feeding the layer.
                                 the Feedblock
                                                                 If output increase in this extruder is not possible, slow down
                                                                 the other extruders.



Lines in the Machine Direction   Die Imperfections               Disassemble and clean the die.
of the Sheet
                                                                 Clean die lip area with a soft tool (preferably wood or copper).

                                                                 Polish damaged die-lip face.

                                                                 Refinish die lip face to 90 degree angle.

                                                                 Polish or replate die surface.



                                  Sheet Extrusion Process Troubleshooting Guidelines                                                9
Problem                          Cause                           Solution
Lines in the Machine Direction   Moisture                        Increase hopper drying time and/or temperature.
of the Sheet, Cont’d.
                                 Equipment Damage                Check scuffs (see Scuffs section).

                                                                 Polish or re-plate damaged chill rolls.

                                 Unstable Bank Size              Adjust die-to-nip distance.

                                                                 Check for extruder surging.

                                                                 Adjust roll temperatures.

Lines in the Transverse          Sheet Sticking to Roll(s)       Reduce melt temperature.
Direction of the Sheet
                                                                 Reduce roll temperature.

                                                                 Clean the rolls.

                                                                 Move die closer to the rolls to prevent sheet from sagging.


                                 Roll Drive Problem              Raise tension to ensure that the sheet does not drop off the
                                                                 bottom roll.

                                                                 Reduce pull-roll tension to avoid “”pulling”” the sheet across
                                                                 the sheet rolls.

                                                                 Adjust drive chain.

                                 Winder Overpowering             Increase pull roll nip pressure.
                                 the Pull Rolls
                                                                 Decrease winder tension.

                                 Sheet Cut Off                   Install a “hump” section in conveyor between pull rolls and
                                                                 shear.



                                  Sheet Extrusion Process Troubleshooting Guidelines                                              0
Problem                         Cause                            Solution
 Lines in the Transverse         Equipment Variation              Check and dampen variations from all equipment. (First isolate
 Direction of the Sheet,                                          the roll-stack to see if it is at fault.)
 Cont’d.
                                                                  Check for and eliminate electrical voltage variation throughout
                                                                  the line, by isolating each drive’s power supply.

                                 Rolling Bank at                  Reduce extrusion rate by reducing screw rpm.
                                 the Nip Roll
                                                                  Reduce size of bank by increasing polishing roll’s speed.

                                                                  Open roll-nip gap.

 Low Gloss on Sheet (Gloss       Improper Process Conditions or   Increase roll temperatures.
 is partly a material property   Equipment
 and can be affected by the                                       Increase roll nip pressure.
 process temperatures.)
                                                                  Increase melt temperature by raising temperatures in last one
                                                                  or two barrel zones.

                                                                  Raise temperatures to equal the melt temperature.

                                                                  Adjust to obtain uniform flow.

                                                                  Adjust roll gaps to maintain good contact with sheet.

                                 Poor Melt                        Increase head pressure to improve mixing.
                                 Consistency
                                                                  Use a static mixer before die.

Non-Uniform Sheet                Variation in                     Eliminate thin spots in skin layer—see Uneven Skin Layer
Color                            the Skin Layer                   Thickness Problems.
                                 Thickness
                                                                  Increase skin layer thickness.




                                  Sheet Extrusion Process Troubleshooting Guidelines
Problem              Cause                             Solution
Non-Uniform Sheet    Poor Regrind Mixing               Increase head pressure.
Color, Cont’d.
                                                       Use static mixer.

                                                       Add compatibilizer to regrind—see Rough Sheet Surface and
                                                       Discolored Sheet.

Parabolic Lines in   Roll Bank Too Large and           If bank is not uniform, adjust die for better gauge.
the Machine Direc-   Non-Uniform
tion                                                   Reduce pressure on roll where the bank is occurring.


                     Extruder Surging                  Check regrind if used. Variable bulk density causes non-uni-
                                                       form feed.

                     Starved Feeding                   Reduce drying time and/or temperature.

                                                       Check hopper and feed section temperatures and clean out
                                                       plug.

                     Poor Compound Mixing (If          Redesign hopper to prevent stratification.
                     mixing regrind with virgin with
                     inadequate blending the extru-    Eliminate stratification of materials by blending and/or segre-
                     sion rate may vary and pulse.)    gating. (An agitator helps.)



Poor Transparency    Material Contamination            Check regrind for contamination.

                                                       Check incoming resin for dirt, packaging scraps, gels, etc.

                                                       Remove excess of fines from resin.

                                                       Check airway system and hopper loading procedures for
                                                       possible sources of contamination.

                                                       Check for loss of plating which can result in black specks.



                      Sheet Extrusion Process Troubleshooting Guidelines                                              2
Problem                         Cause                           Solution
Poor Transparency,              Poor Equipment                  Clean screw and downstream equipment.
Cont’d.                         Maintenance
                                                                Polish roll surfaces.


                                Improper                        Ensure complete melting of the resin by raising the
                                Temperatures                    temperature of the last one or two barrel zones or by raising
                                                                the die temperatures.

                                                                Adjust roll temperatures for proper cooling and maintaining
                                                                the level of crystallinity.

                                Poor Mixing                     Use static mixer in transfer line.

                                                                Increase head pressure.

                                Rolling Bank                    Reduce the extrusion rate.

                                                                Reduce bank size by increasing polishing roll speeds.

                                                                Open the roll-nip gap.

Rough Surface Texture (This     Rolling Bank                    Reduce the extrusion rate.
is not to be confused with
gloss or sheen. Texture can                                     Reduce bank size by increasing polishing roll speeds.
be seen as microscopic
bumps on the sheet. Grain is                                    Open the roll-nip gap.
a natural property, however
it can be emphasized by the     Material Problem                Increase mixing in extruder with higher head pressure
conditions of processing that                                   from valving or finer screen mesh.
will affect the gloss.)
                                                                Remove any incompatible regrind.

                                                                Use a static mixer.




                                 Sheet Extrusion Process Troubleshooting Guidelines                                             3
Problem                          Cause                           Solution
Rough Surface Texture,           Material Problem                Make sure previous materials have been thoroughly purged.
Cont’d.                                                          (Proper purging covers all melt channels–screw, barrel, screen
                                                                 packs, transfer lines, and die, as well as solids handling
                                                                 equipment - pneumatic conveying system, dryers and grinder.)

                                                                 Eliminate moisture. (See Dimples, Pits, and Pock Marks.)

                                 Roll Setup Condition            Decrease roll gap to polish sheet.

                                                                 Increase roll temperature to slow solidification.

                                                                 Increase roll nip pressure to “roll out” roughness.

                                                                 Clean roll surfaces.

                                                                 Re-surface damaged rolls.

Surging                          Starving Screw                  Check for material blockage. (Note flow of pellets at throat
(This is the most common         (Condition is more prominent    and flow at vent.)
problem in extrusion,            on multistage screws in which
especially when frequent         the forward screw flights are   Lower rear barrel zones. (This moves the melt forward and
material changes are made        not full of melt.)              will increase material flow.)
and/or only one “general
purpose feed screw” is used                                      Lower dryer temperature to reduce the feed temperature.
for all materials. Surging is
present when screw is
not delivering a constant ma-
terial flow and is noted
by gross thickness and/or        Insufficient Back Pressure      Close die manifold and/or R-bar.
width changes in the product.)
                                                                 Close gate valve to increase back pressure.

                                                                 Increase screen pack.

                                                                 Lower heat in the gate and/or the screen changer.




                                  Sheet Extrusion Process Troubleshooting Guidelines                                            4
Problem                      Cause                           Solution
Surging, Cont’d.             Non-Uniform Feed Stock          Check regrind level.
                             Temperatures
                                                             Check dryer.

                             High Stock Temperatures         Lower the barrel temperature profile. (High stock temperatures
                                                             may cause the material to be too soft.)

                             Poor Screw Design               In some cases or for some materials, another screw or a
                                                             recut of the existing one may be required.

Thickness Variation in the   Improper Extruder Operation     Check for extruder surging.
Machine Direction
                             Rolling Bank                    Reduce the extrusion rate.

                                                             Reduce bank size by increasing polishing roll speeds.

                                                             Open the roll-nip gap.

                             Roll Problem                    Check roll bearings for wear.

                                                             Clean rolls.

                                                             Check rolls for concentricity.

                                                             Check roll nip pressure “PLI” to ensure sufficient pressure
                                                             to keep roll gap constant.

                             Surface Temperature Variation   Increase roll coolant circulation rate. (Tip: Cooling fluid
                             Across the Roll Face            temperature should not change more than 2°F from
                                                             inlet to outlet.)

                                                             Decrease extruder output.




                              Sheet Extrusion Process Troubleshooting Guidelines                                           5
Problem                      Cause                           Solution
  Thickness Variation in the   Winder Overpowering             Increase pressure on pull rolls.
  Machine Direction, Cont’d.   the Pull Rolls
                                                               Adjust winder tension.

                               Drive Variations                Adjust roll drive.

  Thickness Variation in the   Die Adjustment                  Adjust die restrictor bar, keeping all the bolts tight.
  Transverse Direction
                                                               Adjust die lip gap. (Typically the starting gap is between
                                                               110-120% of the desired sheet thickness.)

                                                               Cool die in thick areas; heat die in thin areas.

                               Roll Adjustment                 Balance and/or raise the roll nip pressure to better distribute
                                                               inconsistent die flow.

                                                               Adjust roll gap to proper setting. (Typically the first gap is about
                                                               1-2% more than desired sheet thickness. Typical second gap
                                                               is the same or slightly less than desired sheet thickness.)

                                                               Reduce roll pressure to minimize roll bending.

                                                               Check roll bearings for wear.

                               Non-Uniform Bank                Check for extruder surging.

                                                               Adjust die temperatures to optimize flow uniformity from die.

                                                               Adjust restrictor bar and/or die lips to optimize flow uniformity
                                                               from die.

Uneven Layer Thickness in      Non-Uniform Melt                Use a static mixer or add a mixing section to the screw.
Transverse Direction           Temperatures
                                                               Set die, feedblock and transfer line temperatures close to
                                                               melt temperatures.



                                Sheet Extrusion Process Troubleshooting Guidelines                                               6
Problem                         Cause                           Solution
Uneven Layer Thickness in       Non-Uniform Melt                Reduce screw RPM.
Transverse Direction, Cont’d.   Temperatures
                                                                Increase head pressure to improve mixing.


                                Rheology or                     Optimize core-layer rheology by changing the melt temperature
                                Equipment                       in extruder, die and feedblock.
                                Interactions
                                                                Optimize skin-layer rheology by changing the melt temperature
                                                                in extruder, die and feedblock.

                                                                Modify feedblock’s slot shape or flow configuration.

                                                                Modify die design. Multi-manifold die can help.

                                Improper                        Retract the die restrictor bar to minimize flow disruption.
                                Equipment
                                Setup or Op-                    Check for proper operation of the temperature control system.
                                eration
                                                                Remove remaining flow restrictions such as sharp corners,
                                                                melt thermocouples.

                                                                Clean buildup from equipment.

Uneven Layer Thick-             Improper Extrusion              Reduce rolling bank at the chill roll.
ness in the Machine             Operation
Direction (Zigzag and                                           Check for extruder surging.
Wave Instability will
both give machine                                               Check to see that roll stack’s pull rolls are functioning properly.
direction thickness                                             (See roll drive problems in Lines in Transverse Direction.)
variation.)




                                 Sheet Extrusion Process Troubleshooting Guidelines                                              7
Problem                           Cause                           Solution

Vent Flow (Considered the         Output of Screw (First Stage    Reduce output of the first stage by raising temperature of the
opposite of surging. The          Higher than Second Stage        first and/or second extruder barrel zone.
screw is melting and pump-        Can Handle)
ing more material than can                                        Increase output of second stage by opening gate valve or
be handled further down-                                          raising the front barrel zone and die temperature or raise the
stream so the excess mate-                                        restrictor bar.
rial comes out of the vent.)
                                                                  Redesign screw.




Wave Instability (Zigzag and      Mismatch in the Rheological     Increase skin layer viscosity by switching to a lower MFR resin
Wave Instability will both give   Properties of the Different     or lowering the skin layer’s melt temp.
machine direction thickness       Layers at a Given Set of
variation.)                       Process Conditions              Decrease core layer viscosity by changing to a higher MFR
                                                                  resin or by raising the core layer’s melt temp.

                                                                  Make the structure more symmetrical.

                                                                  Use a different die design. (A multi-manifold die helps.)

                                                                  Correct velocity mismatches in the feedblock.

Zigzag Instability (Zigzag and    Excessive Interfacial Shear     Increase die lip opening.
Wave Instability will both give   Stress in Die Land
machine direction thickness                                       Increase relative thickness of skin layer.
variation.)
                                                                  Reduce throughput.

                                                                  Decrease viscosity of skin layer by raising its temperature or by
                                                                  using a resin with a higher MFR.

                                                                  Raise die lip temperature.



                                   Sheet Extrusion Process Troubleshooting Guidelines                                              8
Corporate Headquarters
2655 White Oak Circle
Aurora, IL 60502
T. 630-585-5800
F. 630-585-5855

PTi Europe
Fibichova 4, Jihlava
586 01 Czech Republic
T. +420 567 214 464
F. +420 567 214 474




www.ptiextruders.com




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P Ti Troubleshooting Guidelines

  • 1. SHEET EXTRUSION World Class Extrusion Systems Process Troubleshooting Guidelines
  • 2. SHEET EXTRUSION Table of Contents Process Troubleshooting Guidelines Problem Type Page PTi’s Sheet Extrusion Process Trouble- Brittleness in Sheet ............................................................................................................................2 shooting Guidelines offers solutions to Contamination On Sheet .....................................................................................................................2 many of the problems that sheet produc- Curled Sheet in the Transverse Direction..............................................................................................3 ers face in their day-to-day operations. Curled Sheet in the Machine Direction .................................................................................................3 We trust this guide will assist you in Degradation On One Layer..................................................................................................................3 creating quality products for today’s chal- Dimples on the Sheet Surface .............................................................................................................4 lenging sheet extrusion applications. Discolored Sheet ................................................................................................................................6 Herringbone Patterns .........................................................................................................................6 High or Inconsistent Sheet Orientation .................................................................................................7 Inconsistent or Patchy Gloss ...............................................................................................................7 Insufficient Sheet Toughness...............................................................................................................8 Layers Do Not Adhere.........................................................................................................................9 PROCESSING TECHNOLOGIES, LLC Layer Too Thick ..................................................................................................................................9 Layer Too Thin ...................................................................................................................................9 2655 White Oak Circle Lines in the Machine Direction of the Sheet .........................................................................................9 Aurora, IL 60502-9674 Lines in the Transverse Direction of the Sheet ......................................................................................10 Low Gloss on Sheet ...........................................................................................................................11 ph 630.585.5800 Non-Uniform Sheet Color ....................................................................................................................11 fx 630.585.5855 Parabolic Lines in the Machine Direction .............................................................................................12 www.ptiextruders.com Poor Transparency .............................................................................................................................12 Rough Surface Texture .......................................................................................................................13 © 2007 Processing Technologies, LLC Surging .............................................................................................................................................14 PTi reserves the right to make changes to Thickness Variation in the Machine Direction .......................................................................................15 this document without prior notice. Thickness Variation in the Transverse Direction ....................................................................................16 Uneven Layer Thickness in the Transverse Direction .............................................................................16 Note: This document is not intended as a Uneven Layer Thickness in the Machine Direction ................................................................................17 substitute for professional judgement and Vent Flow ..........................................................................................................................................18 operational expertise of the user. No war- Wave Instability ..................................................................................................................................18 ranty is implied. Actual results may vary. Zigzag Instability ................................................................................................................................18 Sheet Extrusion Process Troubleshooting Guidelines
  • 3. Problem Cause Solution Brittleness in Sheet Too Much Orientation Adjust roll gap to proper setting. ( Typically the first gap is aproximately 0.001” to 0.002” UNDER the desired sheet thickness and the second gap should be the same or larger than the desired sheet thickness) See solutions to Orientation. Cold Rolls Increase roll temperatures. Poor Melt Consistency Use static mixer in the transfer line. Reduce regrind levels. Increase head pressure to improve mixing. Reduce additives, i.e. color concentrate. Contamination On Sheet Equipment Problem Check for ruptured screens. Check for loss of plating, which can result in black specks. See solutions to Discolored Sheet. Material Problem Check regrind stream for contamination. Check airway system and hopper loading procedures for contamination. Check incoming resin for dirt, packaging scraps, gels, etc. Remove excess fines from resin. Static Electricity Thoroughly clean all the areas around the line. Dissipate static charge on sheet. Sheet Extrusion Process Troubleshooting Guidelines 2
  • 4. Problem Cause Solution Contamination Equipment Contamination Clean conveyor idler rolls. On Sheet, Cont’d. Clean surface of chill rolls. Degraded Material Clean buildup from surface around die. Falling On Sheet Clean die lips. Curled Sheet in the Improper Roll Temperature Raise temperature of the concave sheet surface. Transverse Direction (If sheet edges curl down and curling occurs “down stack,” raise middle roll temperature. If sheet edges curl up, lower middle roll temperature. Reverse recommendations when curl- ing occurs “up stack.” In both cases change third roll tempera- ture opposite to middle roll temperature changes.) Curled Sheet in the Ma- Excessive Pull-Roll Tension Reduce pull roll speed. chine Direction Reduce pull roll tension. Degradation On One Layer Thermal Decomposition Reduce head pressure to make screw more efficient by clean- ing the screens, using a coarser mesh opening the die lip, and/or shortening the transfer lines. Reduce temperature at the end of extruder barrel and down- stream equipment. Check for dead spots and streamline flow passages by employing sweep elbows and/or removing melt immersion thermocouples. Arrange sheet so that heat-sensitive layer is cooled on the chill roll first. Reduce contact with hot equipment--for example, encapsulate heat sensitive polymer with another polymer. Chemical Reaction Use additives to stabilize the composition. Sheet Extrusion Process Troubleshooting Guidelines 3
  • 5. Problem Cause Solution Degradation On One Layer, Chemical Reaction Remove troublesome additive such as color or regrind from the Cont’d. extruder feed. Check for material compatibility in the coex structure. Dimples on the Sheet Surface Air Entrapment Decrease screw speed. (Also called pits, depressions, (Air collected in pockets pock marks, buck shot and causes voids in the hot Reduce temperatures in the first and second barrel zones. craters.) sheet which contract upon sheet cooling leaving se- Unplug the vent if using two-stage screw. vere depressions. Can be more severe on vacuum Remove fines from regrind. forming because depres- sions become drawn out.) Check vacuum system for proper operation. Reduce hopper drying temperature. Maintain proper hopper level. Raise back pressure if using two-stage screw. Regrind feed stock Change regrind particle size. Reduce regrind level to control bulk density factor. Moisture Increase drying time. Check dryer operation for proper dew point and desiccant regeneration. Increase drying temperature. Check vacuum system for proper operation. Use nitrogen blanket on the feed hopper. Use a drying hopper. Unplug the vent if using two-stage screw. Sheet Extrusion Process Troubleshooting Guidelines 4
  • 6. Problem Cause Solution Dimples on the Sheet Surface, Volatiles Unplug the vent if using two-stage screw. Cont’d. Check vacuum system for proper operation. Cool the melt to minimize volatilization due to decomposition. Volatiles Entrapped Adjust die-roll height to minimize the draping of the sheet Between the Sheet and on the roll. the Roll Check for hot spots on the die. Increase or decrease roll temperature. Increase ventilation to prevent entrapment. Reduce melt temperature. Unplug the vent if using two-stage screw. Check vacuum system for proper operation. Adjust die lips in region corresponding to the entrapment. Insufficient Melt Increase extrusion rate to fill the bank. Bank at the Roll Tip Adjust die restrictor bar and/or die lips to optimize flow uniformity from die. Decrease roll speed to build bank at the roll nip. Optimize die temperatures to improve die flow. Check for extruder surging. Move die closer to roll nip. Increase extrusion rate to fill the bank. Sheet Extrusion Process Troubleshooting Guidelines 5
  • 7. Problem Cause Solution Dimples on the Sheet Surface, Insufficiently Clean Equipment Dissipate static electricity to minimize dust pickup. Cont’d. Clean chill-roll and polishing roll surface. Clean idler rolls in conveyor. Cooling the Sheet too Quickly Raise temperature of the roll in contact with the problem surface. Discolored Sheet Excessive Temperature or Reduce last one or two barrel zone temperatures and/or Residence Times reduce the die temperature. Check for proper operation of the heaters and thermocouples. Reduce the head pressure by changing to clean or coarse screens, and/or by opening up available valving, the die restrictor bar and/or lips. Dirty Scrap or Regrind Streamline flow path by using smooth transitions and/or el- Re-extrusion Frequency bows with longer bend ratio. Clean behind deckles on regular basis. If that fails then remove deckles. Check for loss of plating or other corrosion. Insufficient Color Concen- Add color concentrate at feed throat. trate or Segregation of the Color Concentrate in the Increase color concentrate to specified level. Feed Hopper Re-design hopper to get mass flow rather than funnel flow. Herringbone Patterns Inadequate Drying Increase hopper drying time and/or hopper temperature to (or “Chicken Tracks”), improve drying of pellets Discontinuous Lines Sheet Extrusion Process Troubleshooting Guidelines 6
  • 8. Problem Cause Solution High or Inconsistent Sheet Roll Speed Too Increase extrusion rate. Orientation (Can reduce physi- High Relative to Die cal properties of the sheet, Throughput Rate Reduce chill roll speed. resulting in localized stress in the thermoformed part. Also, Decrease die gap. sheet may pull out of clamps during thermoforming as the Excessive Bank Size Decrease extrusion rate. sheet shrinks.) Increase chill roll speed. Incorrect Die/Nip Align die face with roll center line. Distance Reduce die-nip distance to minimum settings. Pull Roll Tension Increase or decrease pull roll speed. Incorrect Polymer If the differential between the melt temperature is too wide, Cooling Rate raise the roll temperature and/or reduce the melt temperature. If melting temperature is too low, raise temperature on the last one or two barrel zones and/or raise die temperatures. Inconsistent or Inconsistent Adjust Restrictor Bar. Patchy Gloss Gauge Check for extruder surging. Adjust die lip. Excessive Melt Change screen-changer screens. Temperature Reduce temperatures in the last one or two barrel zones. Reduce die temperatures. Sheet Extrusion Process Troubleshooting Guidelines 7
  • 9. Problem Cause Solution Inconsistent or Patchy Gloss, Non-uniform Roll Check for hot spots on roll circumference and clean flow. Cont’d. Temperatures Check the delta temperature across the roll’s face. (Typically, the cooling fluid should vary 2°F or less from roll inlet to roll outlet.) Volatile Entrapment Between Adjust die lips in region corresponding to the entrapment. Sheet and Roll Increase ventilation. Adjust roll height to minimize draping of sheet on roll. Reduce melt temperature. Check for hot spots on die. Unplug vent if using a two stage screw. Check for proper operation of vacuum system. Insufficient Sheet Toughness Brittle Layers Too Thick Improve transverse sheet-thickness uniformity, especially at edges of the sheet. (See solutions to Uneven Layer Thickness in Transverse Direction.) Switch to tougher polymers. Reduce thickness of brittle layers. Excessive Regrind Use additives to restore toughness. Reduce regrind level. Orientation See solutions to Orientation Problems. Sheet Extrusion Process Troubleshooting Guidelines 8
  • 10. Problem Cause Solution Layers Do Not Adhere Adhesive Problems Use an adhesive with higher tensile strength. Increase adhesive layer thickness. Use a separate resin layer for an adhesive or another type of adhesive (a lower viscosity adhesive, for example, will give better wetting). Increase the adhesive melt temperature. Increase the melt contact time. Improper Equipment Operation Set chill roll speed to match polymer die-exit speed. Layer Too Thick Over-Pumping Decrease output of the extruder feeding the layer. the Feedblock If output reduction in this extruder is not possible, speed up the other extruders. Layer Too Thin Under-Pumping Increase output of the extruder feeding the layer. the Feedblock If output increase in this extruder is not possible, slow down the other extruders. Lines in the Machine Direction Die Imperfections Disassemble and clean the die. of the Sheet Clean die lip area with a soft tool (preferably wood or copper). Polish damaged die-lip face. Refinish die lip face to 90 degree angle. Polish or replate die surface. Sheet Extrusion Process Troubleshooting Guidelines 9
  • 11. Problem Cause Solution Lines in the Machine Direction Moisture Increase hopper drying time and/or temperature. of the Sheet, Cont’d. Equipment Damage Check scuffs (see Scuffs section). Polish or re-plate damaged chill rolls. Unstable Bank Size Adjust die-to-nip distance. Check for extruder surging. Adjust roll temperatures. Lines in the Transverse Sheet Sticking to Roll(s) Reduce melt temperature. Direction of the Sheet Reduce roll temperature. Clean the rolls. Move die closer to the rolls to prevent sheet from sagging. Roll Drive Problem Raise tension to ensure that the sheet does not drop off the bottom roll. Reduce pull-roll tension to avoid “”pulling”” the sheet across the sheet rolls. Adjust drive chain. Winder Overpowering Increase pull roll nip pressure. the Pull Rolls Decrease winder tension. Sheet Cut Off Install a “hump” section in conveyor between pull rolls and shear. Sheet Extrusion Process Troubleshooting Guidelines 0
  • 12. Problem Cause Solution Lines in the Transverse Equipment Variation Check and dampen variations from all equipment. (First isolate Direction of the Sheet, the roll-stack to see if it is at fault.) Cont’d. Check for and eliminate electrical voltage variation throughout the line, by isolating each drive’s power supply. Rolling Bank at Reduce extrusion rate by reducing screw rpm. the Nip Roll Reduce size of bank by increasing polishing roll’s speed. Open roll-nip gap. Low Gloss on Sheet (Gloss Improper Process Conditions or Increase roll temperatures. is partly a material property Equipment and can be affected by the Increase roll nip pressure. process temperatures.) Increase melt temperature by raising temperatures in last one or two barrel zones. Raise temperatures to equal the melt temperature. Adjust to obtain uniform flow. Adjust roll gaps to maintain good contact with sheet. Poor Melt Increase head pressure to improve mixing. Consistency Use a static mixer before die. Non-Uniform Sheet Variation in Eliminate thin spots in skin layer—see Uneven Skin Layer Color the Skin Layer Thickness Problems. Thickness Increase skin layer thickness. Sheet Extrusion Process Troubleshooting Guidelines
  • 13. Problem Cause Solution Non-Uniform Sheet Poor Regrind Mixing Increase head pressure. Color, Cont’d. Use static mixer. Add compatibilizer to regrind—see Rough Sheet Surface and Discolored Sheet. Parabolic Lines in Roll Bank Too Large and If bank is not uniform, adjust die for better gauge. the Machine Direc- Non-Uniform tion Reduce pressure on roll where the bank is occurring. Extruder Surging Check regrind if used. Variable bulk density causes non-uni- form feed. Starved Feeding Reduce drying time and/or temperature. Check hopper and feed section temperatures and clean out plug. Poor Compound Mixing (If Redesign hopper to prevent stratification. mixing regrind with virgin with inadequate blending the extru- Eliminate stratification of materials by blending and/or segre- sion rate may vary and pulse.) gating. (An agitator helps.) Poor Transparency Material Contamination Check regrind for contamination. Check incoming resin for dirt, packaging scraps, gels, etc. Remove excess of fines from resin. Check airway system and hopper loading procedures for possible sources of contamination. Check for loss of plating which can result in black specks. Sheet Extrusion Process Troubleshooting Guidelines 2
  • 14. Problem Cause Solution Poor Transparency, Poor Equipment Clean screw and downstream equipment. Cont’d. Maintenance Polish roll surfaces. Improper Ensure complete melting of the resin by raising the Temperatures temperature of the last one or two barrel zones or by raising the die temperatures. Adjust roll temperatures for proper cooling and maintaining the level of crystallinity. Poor Mixing Use static mixer in transfer line. Increase head pressure. Rolling Bank Reduce the extrusion rate. Reduce bank size by increasing polishing roll speeds. Open the roll-nip gap. Rough Surface Texture (This Rolling Bank Reduce the extrusion rate. is not to be confused with gloss or sheen. Texture can Reduce bank size by increasing polishing roll speeds. be seen as microscopic bumps on the sheet. Grain is Open the roll-nip gap. a natural property, however it can be emphasized by the Material Problem Increase mixing in extruder with higher head pressure conditions of processing that from valving or finer screen mesh. will affect the gloss.) Remove any incompatible regrind. Use a static mixer. Sheet Extrusion Process Troubleshooting Guidelines 3
  • 15. Problem Cause Solution Rough Surface Texture, Material Problem Make sure previous materials have been thoroughly purged. Cont’d. (Proper purging covers all melt channels–screw, barrel, screen packs, transfer lines, and die, as well as solids handling equipment - pneumatic conveying system, dryers and grinder.) Eliminate moisture. (See Dimples, Pits, and Pock Marks.) Roll Setup Condition Decrease roll gap to polish sheet. Increase roll temperature to slow solidification. Increase roll nip pressure to “roll out” roughness. Clean roll surfaces. Re-surface damaged rolls. Surging Starving Screw Check for material blockage. (Note flow of pellets at throat (This is the most common (Condition is more prominent and flow at vent.) problem in extrusion, on multistage screws in which especially when frequent the forward screw flights are Lower rear barrel zones. (This moves the melt forward and material changes are made not full of melt.) will increase material flow.) and/or only one “general purpose feed screw” is used Lower dryer temperature to reduce the feed temperature. for all materials. Surging is present when screw is not delivering a constant ma- terial flow and is noted by gross thickness and/or Insufficient Back Pressure Close die manifold and/or R-bar. width changes in the product.) Close gate valve to increase back pressure. Increase screen pack. Lower heat in the gate and/or the screen changer. Sheet Extrusion Process Troubleshooting Guidelines 4
  • 16. Problem Cause Solution Surging, Cont’d. Non-Uniform Feed Stock Check regrind level. Temperatures Check dryer. High Stock Temperatures Lower the barrel temperature profile. (High stock temperatures may cause the material to be too soft.) Poor Screw Design In some cases or for some materials, another screw or a recut of the existing one may be required. Thickness Variation in the Improper Extruder Operation Check for extruder surging. Machine Direction Rolling Bank Reduce the extrusion rate. Reduce bank size by increasing polishing roll speeds. Open the roll-nip gap. Roll Problem Check roll bearings for wear. Clean rolls. Check rolls for concentricity. Check roll nip pressure “PLI” to ensure sufficient pressure to keep roll gap constant. Surface Temperature Variation Increase roll coolant circulation rate. (Tip: Cooling fluid Across the Roll Face temperature should not change more than 2°F from inlet to outlet.) Decrease extruder output. Sheet Extrusion Process Troubleshooting Guidelines 5
  • 17. Problem Cause Solution Thickness Variation in the Winder Overpowering Increase pressure on pull rolls. Machine Direction, Cont’d. the Pull Rolls Adjust winder tension. Drive Variations Adjust roll drive. Thickness Variation in the Die Adjustment Adjust die restrictor bar, keeping all the bolts tight. Transverse Direction Adjust die lip gap. (Typically the starting gap is between 110-120% of the desired sheet thickness.) Cool die in thick areas; heat die in thin areas. Roll Adjustment Balance and/or raise the roll nip pressure to better distribute inconsistent die flow. Adjust roll gap to proper setting. (Typically the first gap is about 1-2% more than desired sheet thickness. Typical second gap is the same or slightly less than desired sheet thickness.) Reduce roll pressure to minimize roll bending. Check roll bearings for wear. Non-Uniform Bank Check for extruder surging. Adjust die temperatures to optimize flow uniformity from die. Adjust restrictor bar and/or die lips to optimize flow uniformity from die. Uneven Layer Thickness in Non-Uniform Melt Use a static mixer or add a mixing section to the screw. Transverse Direction Temperatures Set die, feedblock and transfer line temperatures close to melt temperatures. Sheet Extrusion Process Troubleshooting Guidelines 6
  • 18. Problem Cause Solution Uneven Layer Thickness in Non-Uniform Melt Reduce screw RPM. Transverse Direction, Cont’d. Temperatures Increase head pressure to improve mixing. Rheology or Optimize core-layer rheology by changing the melt temperature Equipment in extruder, die and feedblock. Interactions Optimize skin-layer rheology by changing the melt temperature in extruder, die and feedblock. Modify feedblock’s slot shape or flow configuration. Modify die design. Multi-manifold die can help. Improper Retract the die restrictor bar to minimize flow disruption. Equipment Setup or Op- Check for proper operation of the temperature control system. eration Remove remaining flow restrictions such as sharp corners, melt thermocouples. Clean buildup from equipment. Uneven Layer Thick- Improper Extrusion Reduce rolling bank at the chill roll. ness in the Machine Operation Direction (Zigzag and Check for extruder surging. Wave Instability will both give machine Check to see that roll stack’s pull rolls are functioning properly. direction thickness (See roll drive problems in Lines in Transverse Direction.) variation.) Sheet Extrusion Process Troubleshooting Guidelines 7
  • 19. Problem Cause Solution Vent Flow (Considered the Output of Screw (First Stage Reduce output of the first stage by raising temperature of the opposite of surging. The Higher than Second Stage first and/or second extruder barrel zone. screw is melting and pump- Can Handle) ing more material than can Increase output of second stage by opening gate valve or be handled further down- raising the front barrel zone and die temperature or raise the stream so the excess mate- restrictor bar. rial comes out of the vent.) Redesign screw. Wave Instability (Zigzag and Mismatch in the Rheological Increase skin layer viscosity by switching to a lower MFR resin Wave Instability will both give Properties of the Different or lowering the skin layer’s melt temp. machine direction thickness Layers at a Given Set of variation.) Process Conditions Decrease core layer viscosity by changing to a higher MFR resin or by raising the core layer’s melt temp. Make the structure more symmetrical. Use a different die design. (A multi-manifold die helps.) Correct velocity mismatches in the feedblock. Zigzag Instability (Zigzag and Excessive Interfacial Shear Increase die lip opening. Wave Instability will both give Stress in Die Land machine direction thickness Increase relative thickness of skin layer. variation.) Reduce throughput. Decrease viscosity of skin layer by raising its temperature or by using a resin with a higher MFR. Raise die lip temperature. Sheet Extrusion Process Troubleshooting Guidelines 8
  • 20. Corporate Headquarters 2655 White Oak Circle Aurora, IL 60502 T. 630-585-5800 F. 630-585-5855 PTi Europe Fibichova 4, Jihlava 586 01 Czech Republic T. +420 567 214 464 F. +420 567 214 474 www.ptiextruders.com USA - CANADA - EUROPE - ASIA - LATIN AMERICA