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Day 1


Table of pH vs. NaOH volume used in Potentiometric Titration of Mixed Ac

pH                BURETTE READING (ml)        Volume used (ml)     ∑ Volume used (ml)
             Initial Volume Final Volume
      1.38              0.69           0.00                     0.00                    0.00
      1.36              0.69           1.71                     1.02                    1.02
      1.34              1.71           2.69                     0.98                    2.00
      1.36              2.69           3.71                     1.02                    3.02
      1.38              3.71           4.72                     1.01                    4.03
      1.42              4.72           5.70                     0.98                    5.01
      1.46              5.70           6.73                     1.03                    6.04
      1.50              6.73           7.75                     1.02                    7.06
      1.56              7.75           8.68                     0.93                    7.99
      1.61              8.68           9.69                     1.01      pH   of solution vs. Volume of N
                                                                                        9.00
      1.67              9.69          10.70          14.00      1.01                   10.01
      1.76             10.70          11.71                     1.01                   11.02
      1.86             11.71          12.79                     1.08                   12.10
      1.99             12.79          13.81          12.00      1.02                   13.12
      2.16             13.81          14.71                     0.90                   14.02
      2.48             14.71          15.72                     1.01                   15.03
      2.94             15.72          16.68          10.00      0.96                   15.99
      3.37             16.68          17.74                     1.06                   17.05
      3.62             17.74          18.69                     0.95                   18.00
      3.81             18.69          19.70           8.00      1.01                   19.01
      3.96             19.70          20.72                     1.02                   20.03
                                                pH




      4.09             20.72          21.79                     1.07                   21.10
      4.20             21.79          22.80           6.00      1.01                   22.11
      4.29             22.80          23.73                     0.93                   23.04
      4.39             23.73          24.75                     1.02                   24.06
      4.48             24.75          25.73           4.00      0.98                   25.04
      4.57             25.73          26.79                     1.06                   26.10
      4.65             26.79          27.80                     1.01                   27.11
      4.74             27.80          28.75           2.00      0.95                   28.06
      4.84             28.75          29.72                     0.97                   29.03
      4.94             29.72          30.71                     0.99                   30.02
      5.05             30.71          31.79           0.00      1.08                   31.10
      5.18             31.79          32.80              0.00   5.00
                                                                1.01   10.00   15.00 32.11 25.00 30.00
                                                                                       20.00
      5.33             32.80          33.82                     1.02                   33.13
                                                                                Volume of NaOH used
      5.49             33.82          34.70                     0.88                   34.01
      5.76             34.70          35.79                     1.09                   35.10
      6.39             35.79          36.88                     1.09                   36.19
     11.25             36.88          38.21                     1.33                   37.52
     11.55             38.21          39.15                     0.94                   38.46
     11.73             39.15          40.13                     0.98                   39.44
     11.84             40.13          41.11                     0.98                   40.42
     11.91             41.11          42.12                     1.01                   41.43
     11.97             42.12          43.10                     0.98                   42.41
ration of Mixed Acid

         pH

                     1.38
                     1.36
                     1.34
                     1.36
                     1.38
                     1.42
                     1.46
                     1.50
                     1.56
 solution vs. Volume 1.61
                     of NaOH used
                     1.67
                     1.76
                     1.86
                     1.99
                     2.16
                     2.48
                     2.94
                     3.37
                     3.62
                     3.81
                     3.96
                     4.09                    Column F
                     4.20
                     4.29
                     4.39
                     4.48
                     4.57
                     4.65
                     4.74
                     4.84
                     4.94
                     5.05
 .00 20.00 25.00 30.00 35.00 40.00
                     5.18            45.00
                     5.33
Volume of NaOH used
                     5.49
                     5.76
                     6.39
                    11.25
                    11.55
                    11.73
                    11.84
                    11.91
                    11.97

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Data For Lab Day 1

  • 1. Day 1 Table of pH vs. NaOH volume used in Potentiometric Titration of Mixed Ac pH BURETTE READING (ml) Volume used (ml) ∑ Volume used (ml) Initial Volume Final Volume 1.38 0.69 0.00 0.00 0.00 1.36 0.69 1.71 1.02 1.02 1.34 1.71 2.69 0.98 2.00 1.36 2.69 3.71 1.02 3.02 1.38 3.71 4.72 1.01 4.03 1.42 4.72 5.70 0.98 5.01 1.46 5.70 6.73 1.03 6.04 1.50 6.73 7.75 1.02 7.06 1.56 7.75 8.68 0.93 7.99 1.61 8.68 9.69 1.01 pH of solution vs. Volume of N 9.00 1.67 9.69 10.70 14.00 1.01 10.01 1.76 10.70 11.71 1.01 11.02 1.86 11.71 12.79 1.08 12.10 1.99 12.79 13.81 12.00 1.02 13.12 2.16 13.81 14.71 0.90 14.02 2.48 14.71 15.72 1.01 15.03 2.94 15.72 16.68 10.00 0.96 15.99 3.37 16.68 17.74 1.06 17.05 3.62 17.74 18.69 0.95 18.00 3.81 18.69 19.70 8.00 1.01 19.01 3.96 19.70 20.72 1.02 20.03 pH 4.09 20.72 21.79 1.07 21.10 4.20 21.79 22.80 6.00 1.01 22.11 4.29 22.80 23.73 0.93 23.04 4.39 23.73 24.75 1.02 24.06 4.48 24.75 25.73 4.00 0.98 25.04 4.57 25.73 26.79 1.06 26.10 4.65 26.79 27.80 1.01 27.11 4.74 27.80 28.75 2.00 0.95 28.06 4.84 28.75 29.72 0.97 29.03 4.94 29.72 30.71 0.99 30.02 5.05 30.71 31.79 0.00 1.08 31.10 5.18 31.79 32.80 0.00 5.00 1.01 10.00 15.00 32.11 25.00 30.00 20.00 5.33 32.80 33.82 1.02 33.13 Volume of NaOH used 5.49 33.82 34.70 0.88 34.01 5.76 34.70 35.79 1.09 35.10 6.39 35.79 36.88 1.09 36.19 11.25 36.88 38.21 1.33 37.52 11.55 38.21 39.15 0.94 38.46 11.73 39.15 40.13 0.98 39.44 11.84 40.13 41.11 0.98 40.42 11.91 41.11 42.12 1.01 41.43 11.97 42.12 43.10 0.98 42.41
  • 2. ration of Mixed Acid pH 1.38 1.36 1.34 1.36 1.38 1.42 1.46 1.50 1.56 solution vs. Volume 1.61 of NaOH used 1.67 1.76 1.86 1.99 2.16 2.48 2.94 3.37 3.62 3.81 3.96 4.09 Column F 4.20 4.29 4.39 4.48 4.57 4.65 4.74 4.84 4.94 5.05 .00 20.00 25.00 30.00 35.00 40.00 5.18 45.00 5.33 Volume of NaOH used 5.49 5.76 6.39 11.25 11.55 11.73 11.84 11.91 11.97