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Indentation-Induced Failure of Hard Coatings

                                                            Adnan Abdul-Baqi & Erik van der Giessen
                                                                                           Koiter Institute Delft

                                                                                                                              F
Introduction




                                                                                                                                                                                                                )
                                                                                                                                                                                                                 max
                                                                                                                          O       R             r




                                                                                                                                                                                                                (τ
Indentation-induced failure of hard coatings is modelled by means of                                                 h        a                          Film (elastic)             t




                                                                                                                                                                                                                 max
                                                                                                                                                                                                                                    normal




                                                                                                                                                                                                            σ
cohesive surfaces. Interfacial delamination (normal & shear) and                                                                                                Interface
coating cracking are the failure events being under consideration.                                                    z                                                                                                         shear




                                                                                                     Symmetry axis
For the cohesive surface, the constitutive behaviour is given in terms                                                                 Substrate (elastic-plastic)                                                                            ∆ (∆ )
                                                                                                                                                                                                                                               n       t
of a traction versus separation law, where we have adopted the uni-
versal binding law used by Xu and Needleman [1]. It is characterized
mainly by the peak traction and the separation energy (Fig. 2).


Results                                                                                                                   Figure 1. Geometry.                                                    Figure 2. Cohesive zone tractions. The
                                                                                                                                                                                                 energy for normal or shear separation is
                                                                                                                                                                                                 the area under the corresponding curve.
  Interfacial delamination:

           0                                           σe/σy                  0                                                                                                             1
                                                                                                                                                     σzz/σmax
                                                                 1.40                                                                                           1.00
                                                                 1.20                                                                                                                              shear delamination
                                                                                                                                                                0.75                       0.8     normal delamination
                                                                 1.00                                                                                           0.50
    50                                                           0.80      20
                                                                                                                                                                0.25
                                                                 0.60                                                                                                                      0.6




                                                                                                                                                                                  F/Fmax
                                                                                                                                                                 0.00
                                                                         z (µm)
  z (µm)




                                                                 0.40                                                                                           -0.25
                                                                 0.20                                                                                           -0.50                      0.4
  100                                                                      40

                                                                                                                                                                                           0.2


                                                                                                                                                         (b)                                0
  150                                                      (a)             60                                                                                                                0            0.5              1            1.5                 2
               0           50             100        150                          0             20                                40            60                                                                        h/t
                                r (µm)                                                                               r (µm)
  Figure 3. (a) Shear delamination . t = 5 µm, τ max = 1.2 GPa . Arrows show the shear direction, line                                                                            Figure 4. Load versus displacement (F-h) curves for
  shows the location of the delaminated area. (b) Normal delamination. t = 2.5 µm, σ max = 1.5 GPa .                                                                              Fig. 3.




   Coating cracking:

               0                                                                   0
                                                          σrr/σmax                                                                                       σrr/σmax                    1
                                                                                                                                                                                                                                                   e
                                                                 2.00                                                                                            2.00
                                                                 1.56                                                                                            1.56                                                                   d
               5
                                                                                                                                                                                  0.8
                                                                 1.11              5                                                                             1.11
                                                                  0.67                                                                                           0.67
                                                                  0.22                                                                                           0.22             0.6
                                                                                                                                                                         F/Fmax
   z (µm)




                                                                         z (µm)




            10                                                   -0.22            10                                                                            -0.22                                                  b c
                                                                 -0.67                                                                                          -0.67             0.4
                                                                 -1.11                                                                                          -1.11
                                                                                                                                                                                                      a
            15                                                   -1.56            15                                                                            -1.56
                                                                 -2.00                                                                                          -2.00             0.2


            20                                             (a)                    20                                                                      (b)                        0
                   0   5           10           15   20                                0    5                              10          15           20                                0                    0.5                  1                          1.5
                                 r (µm)                                                                                  r (µm)                                                                                         h/t
  Figure 5. Coating cracking. t = 2 µm, σ max = 11 GPa . (a) First crack at r 1 = 7.0 µm . (b) Second                                                                    Figure 6. Load versus displacement curve for Fig. 5.
  crack at r 2 = 9.4 µm .                                                                                                                                                Labelled points correspond to specific failure types. a
                                                                                                                                                                         and b on the curve correspond to mode I cracks at loca-
                                                                                                                                                                         tions r 1 and r 2 , respectively. At c the first crack grows
Conclusions                                                                                                                                                              until the interface and at d it shears of f. Point e corre-
                                                                                                                                                                         sponds to some limited interfacial delamination in the
1. Shear delamination may occur in the loading stage. It is imprinted on the load vs displacement curve by a kink.                                                       vicinity of the coating cracks.

2. Normal delamination may occur during the unloading stage, where a circular part of the coating is lifted off
from the substrate. It is imprinted on the load vs displacement curve by a hump.

3. Coating cracking may occur during the loading stage. The first circumferential crack occurs outside the con-
tact area. The crack is imprinted on the F-h curve as a kink.

4. On further loading, subsequent cracking occurs with crack spacing of about 1.25 times the coating thickness.                                                         [1] X.-P. Xu, A. Needleman, Model. Simul. Mater. Sci. Eng. 1 (1993) 111.

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Indentation induced failure - poster

  • 1. Indentation-Induced Failure of Hard Coatings Adnan Abdul-Baqi & Erik van der Giessen Koiter Institute Delft F Introduction ) max O R r (τ Indentation-induced failure of hard coatings is modelled by means of h a Film (elastic) t max normal σ cohesive surfaces. Interfacial delamination (normal & shear) and Interface coating cracking are the failure events being under consideration. z shear Symmetry axis For the cohesive surface, the constitutive behaviour is given in terms Substrate (elastic-plastic) ∆ (∆ ) n t of a traction versus separation law, where we have adopted the uni- versal binding law used by Xu and Needleman [1]. It is characterized mainly by the peak traction and the separation energy (Fig. 2). Results Figure 1. Geometry. Figure 2. Cohesive zone tractions. The energy for normal or shear separation is the area under the corresponding curve. Interfacial delamination: 0 σe/σy 0 1 σzz/σmax 1.40 1.00 1.20 shear delamination 0.75 0.8 normal delamination 1.00 0.50 50 0.80 20 0.25 0.60 0.6 F/Fmax 0.00 z (µm) z (µm) 0.40 -0.25 0.20 -0.50 0.4 100 40 0.2 (b) 0 150 (a) 60 0 0.5 1 1.5 2 0 50 100 150 0 20 40 60 h/t r (µm) r (µm) Figure 3. (a) Shear delamination . t = 5 µm, τ max = 1.2 GPa . Arrows show the shear direction, line Figure 4. Load versus displacement (F-h) curves for shows the location of the delaminated area. (b) Normal delamination. t = 2.5 µm, σ max = 1.5 GPa . Fig. 3. Coating cracking: 0 0 σrr/σmax σrr/σmax 1 e 2.00 2.00 1.56 1.56 d 5 0.8 1.11 5 1.11 0.67 0.67 0.22 0.22 0.6 F/Fmax z (µm) z (µm) 10 -0.22 10 -0.22 b c -0.67 -0.67 0.4 -1.11 -1.11 a 15 -1.56 15 -1.56 -2.00 -2.00 0.2 20 (a) 20 (b) 0 0 5 10 15 20 0 5 10 15 20 0 0.5 1 1.5 r (µm) r (µm) h/t Figure 5. Coating cracking. t = 2 µm, σ max = 11 GPa . (a) First crack at r 1 = 7.0 µm . (b) Second Figure 6. Load versus displacement curve for Fig. 5. crack at r 2 = 9.4 µm . Labelled points correspond to specific failure types. a and b on the curve correspond to mode I cracks at loca- tions r 1 and r 2 , respectively. At c the first crack grows Conclusions until the interface and at d it shears of f. Point e corre- sponds to some limited interfacial delamination in the 1. Shear delamination may occur in the loading stage. It is imprinted on the load vs displacement curve by a kink. vicinity of the coating cracks. 2. Normal delamination may occur during the unloading stage, where a circular part of the coating is lifted off from the substrate. It is imprinted on the load vs displacement curve by a hump. 3. Coating cracking may occur during the loading stage. The first circumferential crack occurs outside the con- tact area. The crack is imprinted on the F-h curve as a kink. 4. On further loading, subsequent cracking occurs with crack spacing of about 1.25 times the coating thickness. [1] X.-P. Xu, A. Needleman, Model. Simul. Mater. Sci. Eng. 1 (1993) 111.