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Single- and Double-Layer Graphene  for in-situ High-Pressure Raman scattering Synthesis and Characterization  of Carbon-based Nanomaterials Nicolas MORAL Supervisor: Pr. Alexander SOLDATOV High-Pressure Spectroscopy Laboratory Division of Physics, Luleå Tekniska Universitet, 971 87 Luleå, SWEDEN Department of Applied Physics and Mechanical Engineering
Table of contents ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Introduction Carbon-based Nanomaterials Raman scattering High-Pressure
Carbon-based Nanomaterials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Graphene ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Graphene ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Graphene ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Introduction Carbon-based Nanomaterials Raman scattering High-Pressure
Raman scattering ,[object Object],[object Object],[object Object],[object Object]
Raman Scattering
High-Pressure ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Motivation of the thesis Preparation of in-situ HP  Resonance Raman Spectroscopy
Motivation of the thesis ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and materials Source Materials, Equipment, Protocols
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials Route 1: Supported Graphene Route 2: Free-Standing Graphene
Methods and Materials
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials
Methods and Materials
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials Route 1: Supported Graphene Route 2: Free-Standing Graphene
Methods and Materials ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Methods and Materials 100 µm
Results and discussions ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Supported Graphene ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Conclusion ,[object Object],[object Object],[object Object],[object Object],[object Object]
Results and discussions ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Optical observation ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Optical observation Graphite Glue DLG ? FLG MLG SLG ?
Results and discussions ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Reference spectra ,[object Object],[object Object],[object Object],[object Object],[object Object]
Reference spectra
Reference spectra
Reference spectra
Conclusion ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Results and discussions ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Spectral confirmation ,[object Object],[object Object],[object Object]
Spectral confirmation ,[object Object],[object Object],[object Object]
Spectral confirmation ,[object Object],[object Object],[object Object]
Spectral confirmation ,[object Object],[object Object],[object Object]
Spectral confirmation
Spectral confirmation ,[object Object],[object Object],[object Object]
Spectral confirmation
Spectral confirmation
Spectral confirmation ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Spectral confirmation
Spectral confirmation ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Conclusion ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Results and discussions ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Transfer ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Conclusion ,[object Object],[object Object],[object Object],[object Object]
Results and discussions ,[object Object],[object Object],[object Object],[object Object]
Free-Standing Graphene
Free-Standing Graphene
Free-Standing Graphene
Conclusion ,[object Object],[object Object],[object Object],[object Object],[object Object]
Results and discussions ,[object Object],[object Object],[object Object],[object Object]
Transfer ,[object Object],[object Object],[object Object],[object Object]
Transfer
Conclusion ,[object Object],[object Object],[object Object],[object Object],[object Object]
Summary of Conclusions Route 1: Supported Graphene Route 2: Free-Standing Graphene
Summary of Conclusions ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Future Work ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Future Work Gband 1580cm -1 (intensity a.u.) G’band 2670cm -1 (intensity a.u.) Gband G’band
Acknowledgements ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Thank you for your attention Please address your questions NOW !
 

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Graphene Syntheis and Characterization for Raman Spetroscopy At High Pressure

Hinweis der Redaktion

  1. Young’s Modulus ~1TPa / High toughness-to-weight ratio / High e - and heat conductance (ballistic) All these come from GRAPHENE !!
  2. 2D does not exist : Start with the bonds, get from graphite to graphene, why it is excellent
  3. Young 1GPA; Thermal 50times diamond;
  4. Add legend