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In-situ X Ray Characterization of Semicrystalline 
Polymer Microstructure during Deformation 
1 
~1nm 
~100nm 
Time Resolved Measurements at Synchrotron Sources
Small Angle X Ray Scattering (SAXS) 
훆
SAXS Analysis 
Convert to 
Real Space 
dac 
dc 
da 
0.046 A-1 
Qy 
Qx 
Image Analysis 
SAXS Pattern Structural Model 
Image Analysis 
WAXS Pattern Structural Model
β° 
4 
Model Validation for SAXS via 2D FFT
Project Outline 
• Spatial Correlations For Single Time Step 
• Phase Recovery Algorithm To Generate Eigen 
Microstructure 
• Establish And Visualize Low Dimensional 
Representation Of Process-Structure Linkage 
• Attempt To Utilize Work Flow To Capture Orientation 
Information 
5
Thanks! 
! 
! 
David Brough 
Abhiram Kannan 
6

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Project Report for Materials Informatics

  • 1. In-situ X Ray Characterization of Semicrystalline Polymer Microstructure during Deformation 1 ~1nm ~100nm Time Resolved Measurements at Synchrotron Sources
  • 2. Small Angle X Ray Scattering (SAXS) 훆
  • 3. SAXS Analysis Convert to Real Space dac dc da 0.046 A-1 Qy Qx Image Analysis SAXS Pattern Structural Model Image Analysis WAXS Pattern Structural Model
  • 4. β° 4 Model Validation for SAXS via 2D FFT
  • 5. Project Outline • Spatial Correlations For Single Time Step • Phase Recovery Algorithm To Generate Eigen Microstructure • Establish And Visualize Low Dimensional Representation Of Process-Structure Linkage • Attempt To Utilize Work Flow To Capture Orientation Information 5
  • 6. Thanks! ! ! David Brough Abhiram Kannan 6