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DR. MAHESH JAIN (M.D.S.)
Assistant Professor
Department of Orthodontics & Dentofacial Orthopedics
Manipal College of Dental sciences
Manipal University, Mangalore (India)
Email id: doctormaheshjain@gmail.com
 I finished my Bachelors in Dental Surgery in 2007 and Masters in Orthodontics & Dentofacial
Orthopedics in 2011 from Manipal University, India.
Academic Credentials
 Received Student Plaque Award 2006 for outstanding achievement during the years of dental
study from International College of Dentists (India & Srilanka section).
 Presented paper on “Role of Dentistry in Bioterrorism” at Indian Dental Association student
conference held at Bangalore, 2006.
 Presented Poster on “Clinical manipulation of Herbst fixed functional appliance” at 13th
Indian
Orthodontic Society Post- Graduate Student’s Convention 2009 held at Davengere, India.
 Presented Paper on “Treatment of Retrusive Midface by Rapid Palatal Expansion and
Facemask Therapy: Case Report Series” at 14th
Indian Orthodontic Society Post-Graduate
Student’s Convention 2010 held at Chennai, India
 Presented Paper on “Determination of optimum adhesive thickness using varying degree of
force application and its effect on shear bond strength: an in-vitro study” at 46th
Indian
Orthodontic Conference 2011 held at Khajuraho, India.
Determination of Optimum adhesive thickness using
differential force application with light cure adhesive &
its effects on shear bond strength: an in-vitro study
Introduction
 The main concern with the orthodontists is to achieve stable bond strength
which depends on many factors which includes:
 Bracket base design
 Adhesive thickness
 Adhesive composition
 Type of enamel conditioner
 Length of etching time and so on
Many studies have evaluated the effect of these mentioned variables on
shear bond strength, however the effect of adhesive thickness on bond
strength largely remain unstudied.
Uniform adhesive thickness present between bracket base and tooth
surface may prevent the need for compensatory bends that to be
placed in finishing arch wires thereby, help in full utilization of PEA
and to obtain perfect finish.
Aims & Objectives
 Effect of varying thickness of adhesive on shear bond strength of
orthodontic bracket.
 To determine the optimum adhesive thickness achieved between
tooth surface and bracket with light cured adhesive.
Materials and Methods
Based on amount of force applied while bonding
Materials &Methods
Bucco-lingual width of each premolar along
with bracket was measured
Bucco-lingual width of each premolar was
measured again after bonding
Bracket was subjected to force applied
at centre of bracket using a fork end of
Dontrix guage
Determining adhesive thickness
Hence, difference in bucco lingual width of each premolar
with bracket prior to bonding and after bonding is
measured ;thereby adhesive thickness is determined for
specified force application.
 The mean, standard deviation and confidence interval for mean were calculated for
each group
 Analysis of variance (ANOVA) was used to determine whether significant differences
existed between the various group compared.
 Significance of level was predetermined at p value <0.001.
 The Bonferroni multiple comparison test was applied to find the group with
significant difference.
 Pearson Correlation test was performed to correlate the relationship between adhesive
thicknesses and shear bond strength
 Weibull analysis was used to calculate the probability of failure at given values of
applied force.
STATISTICAL ANALYSIS
Results
20 .9950 .04968 .01111 .9717 1.0183 127.591 p<0.001
20 .8365 .03951 .00883 .8180 .8550 HS
20 .7245 .06825 .01526 .6926 .7564
.
Group A
Group B
Group C
adhesive thickness
(mm)
N Mean
Std.
Deviation
Std.
Error Lower Bound Upper Bound
95% Confidence Interval for
Mean ANOVA F
value p value
Table I: Descriptive statistics of the three groups and comparison of adhesive thickness by ANOVA tests.
Results
Multiple Comparisons
Bonferroni
.15850 .01702 p<0.001 HS
.27050 .01702 p<0.001 HS
.11200 .01702 p<0.001 HS
(J) Group
Group B
Group C
Group C
(I) Group
Group A
Group B
Dependent Variable
adhesive thickness (mm)
Mean
Difference
(I-J) Std. Error p
Table II: Multiple comparisons of adhesive thickness
between three groups using Bonferroni test.
20 6.364 1.2727 .2846 5.768 6.960 23.956 p<0.001
20 9.559 1.4383 .3216 8.885 10.232 HS
20 8.577 1.7372 .3884 7.764 9.390
Group A
Group B
Group
c
Shear bond
strength(MPa)
N Mean
Std.
Deviation
Std.
Error Lower Bound Upper Bound
95% Confidence Interval
for Mean ANOVA F
value p value
Table III: Descriptive statistics of the three groups and comparison of shear bond strength by ANOVA tests.
 
Multiple Comparisons
Bonferroni
-3.1945 .4728 p<0.001 HS
-2.2130 .4728 p<0.001 HS
.9815 .4728 .127 NS
(J) Group
Group B
Group C
Group C
(I) Group
Group A
Group B
Dependent Variable
Shear bond
strength(MPa)
Mean
Difference
(I-J) Std. Error p
Table IV: Multiple comparisons of shear bond strength between three
groups using Bonferroni test
Correlations
-.528 .017 sig
.408 .074 NS
.122 .607 NS
Shear bond
strength(MPa)
Shear bond
strength(MPa)
Shear bond
strength(MPa)
adhesive thickness (mm)
adhesive thickness (mm)
adhesive thickness (mm)
Group
Group A
Group B
Group C
Pearson Correlation p value
Table V: Pearson's correlation test
% failure Reliability Group A Group B Group C
99.9% 0.001 1.109 0.925 0.885
99% 0.01 1.089 0.909 0.856
95% 0.05 1.069 0.893 0.826
5% 0.95 0.892 0.756 0.590
1% 0.99 0.829 0.707 0.515
Beta ( shape parameter/weibull modulus) 22.49 24.31 12.08
Alpha (characteristic life) 1.018 0.8545 0.7547
Mean adhesive thickness(mm) 0.995 0.836 0.724
Table VI: Weibull analysis for adhesive thickness
% failure Reliability Group A Group B Group C
99.9% 0.001 9.62 13.18 13.16
99% 0.01 8.96 12.48 12.24
95% 0.05 8.31 11.78 11.32
5% 0.95 4.08 6.83 5.43
1% 0.99 3.07 5.49 4.04
Beta ( shape parameter/weibull modulus) 5.725 7.467 5.539
Alpha (characteristic life) 6.867 10.175 9.291
Mean shear bond strength (MPa) 6.36 9.55 8.57
Table VII: Weibull analysis for shear bond strength
Thus, the increase in the applied force while bonding results in the decreased thickness of
the adhesive between bracket base and tooth surface. However, the amount of thickness
may vary not only due to the pressure, but also to the viscosity of the adhesive used.
Discussion
Most of the studies done till now use firm pressure while placing bracket on the enamel
surface with assumption that uniform thickness of adhesive is achieved, but as shown in
the present study even a change of 1ounce force brings about significant change in
adhesive thickness.
Mackay also noted that the stiffness of each material depends on size, type and amount of
the filler content and monomer used. Therefore, adhesive thickness obtained in this study
by varying the force of application is meant only for adhesive Transbond XT. Hence,
different types of adhesive resins will produce different thickness while applying same
amount of force.
However, Mackay (1992) reported that increasing the thickness of adhesives had no
statistically significant effect on their mean shear bond strength, although the trend was
to decreased. Evans, Powers (1985) noted that the tensile bond strength was decreased
with increased adhesive thickness. These results are similar to that reported by Jost-
Brinkmann, Schechter & others.
As adhesive thickness reduces, shear bond strength first increases from group A (6.36
MPa) to group B (9.55 MPa), but then it decreases in group C (8.57MPa); and it is
highly statistically significant.
As suggested by Buonocore (1963) & Alster(1995), increasing the thickness of the
adhesive layer results in a weaker joint due to the increased polymerization shrinkage
seen in thicker layers, along with the imperfections which lead to increase in stress
concentrations and hence decreasing the strength.
Interesting finding to be noted here is that shear bond strength reduces in group C (8.57
MPa), although its thickness is minimum (0.72mm). Although, these findings are quite
similar to our findings, but this cannot be compared directly as material and methodology
in these studies were different from the present study.
An explanation of this finding could be that strength of any material depends on its
volume to a larger extent, and since the thickness of group C is minimum we can expect
bond failure to occur early.
Li et al too reported that volume of filler had a greater effect on physical and mechanical
properties than filler size. Arici et al noticed that mean shear bond strength increased as
adhesive thickness increased; but they have tested shear bond strength at interval of
0.25mm thickness starting from 0mm to 0.5mm.
Hence, Weibull analysis is performed here to analyze the characteristic bond strength
and to know the probability of failure for each of the material.
Higher weibull modulus (ÎČ) indicates a more predictable system and possibly, a more
clinically reliable system. Group B produced higher modulus (ÎČ) values than other
groups, hence the group B could be consider as more predictable and clinically reliable
system.
Hence, we can infer that optimum adhesive thickness is required; because shear bond
strength has a tendency to decrease with decreasing thickness.
As indicated by Fox et al, mean and standard deviation values of bond strengths are not
the best indicators of the performance of any bonding material.
Weibull analysis also showed that force needed for 99.9% chance of failure is maximum
for group B (13.18 MPa) and minimum for group A(9.62 MPa). It means that group B can
withstand higher forces when compared to all other groups.
Therefore, group B with mean shear bond strength of 9.55MPa having a mean adhesive
thickness of 0.83mm could be considered as the group having optimum adhesive thickness
required to achieve sufficient bond strength to prevent chances of bond failure.
Thus, application of controlled bonding pressure (2 oz as we obtained in this study)
through a bracket holder that has a pressure gauge could be the correct way to gain a
uniform optimum adhesive thickness (0.83mm) between the bracket and enamel.
Adhesive thickness between bracket base and tooth surface decreases with
increasing the amount of force application from 1ounce to 3 ounces.
Mean shear bond strength increases when adhesive thickness decreases from
group A to Group B and then it has a tendency to decrease as shown in group
C.
0.83mm could be considered as optimum adhesive thickness which is required to
achieve sufficient bond strength to prevent chances of bond failure.
Conclusion
1. Andrews LF. Interviews on the straight wire appliance. J Clin Orthod.
1990; 24: 493-508.
2. Buonocore MG. A simple method of increasing the adhesion of acrylic
filling material to enamel surfaces. J Dent Res 34:849-853, 1955.
3. Mackay F. The effect of adhesive type and thickness on bond strength of
orthodontic brackets. Br J Orthod 1992;19:35-39.
4. SchechterG., Caputo A.A. Chaconas S.J. The effect of adhesive thickness
on retention of direct bonded brackets, Journal of Dental Research.
1980;59:285
5. Jost-Brinkmann PG, Schiffer A, Miethke RR.. The effect of adhesive
thickness layer on shear bond strength. J.Clin. Orthod. 1992;26(11):718-
720.
6. Arici S, Benan O, Arici N. Adhesive thickness effects on the bond strength
of a lightcured resin- modified glass ionomer cement. Angle Orthod 2005;
75(2); 254-259.. Farmararz M, Akhoundi M,
References
7. Farmararz M, Akhoundi M. Comparison of wire loop and shear blade
as the 2 most common methods for testing orthodontic shear bond
strength. Am J Orthod Dentofacial Orthop 2006;130:385-7.
8. Klocke A, Neike B. Effect of debonding force direction on orthodontic
shear bond strength. . Am J Orthod Dentofacial Orthop 2006; 129:261-
5.
9. Eliades T, Brantley WA. The inappropriateness of conventional
orthodontic bond strength assessment protocols. Eur J Orthod 2000;
22:13-23.
10. Evans L, Powers JM. In vitro bond strength of no-mix orthodontic
cements. Am J Orthod. 1985; 37: 508 – 12.
11. Alster D, Feilzer AJ, De Gee AJ, Davidson CL.. Tensile strength of thin
resin composite layers as a function of layer thickness. J Dent Res 1995;
74(11): 1745-8.
12. Li Y, Swartz ML, Phillips RW, Moore BK, Roberts TA.. Effect of filler
content and size on properties of composites J Dent Res 1985; 63: 1396-
1401.
13. Reynolds JR. A review of direct orthodontic bonding. Br J Orthod
1975;2:171-178.
14. Fox N A, McCabe J F, Buckley J G. A critique of bond strength testing in
orthodontics.Br J Orthod 1994; 21: 33-43.

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919 mahesh jain

  • 1. DR. MAHESH JAIN (M.D.S.) Assistant Professor Department of Orthodontics & Dentofacial Orthopedics Manipal College of Dental sciences Manipal University, Mangalore (India) Email id: doctormaheshjain@gmail.com
  • 2.  I finished my Bachelors in Dental Surgery in 2007 and Masters in Orthodontics & Dentofacial Orthopedics in 2011 from Manipal University, India. Academic Credentials  Received Student Plaque Award 2006 for outstanding achievement during the years of dental study from International College of Dentists (India & Srilanka section).  Presented paper on “Role of Dentistry in Bioterrorism” at Indian Dental Association student conference held at Bangalore, 2006.  Presented Poster on “Clinical manipulation of Herbst fixed functional appliance” at 13th Indian Orthodontic Society Post- Graduate Student’s Convention 2009 held at Davengere, India.  Presented Paper on “Treatment of Retrusive Midface by Rapid Palatal Expansion and Facemask Therapy: Case Report Series” at 14th Indian Orthodontic Society Post-Graduate Student’s Convention 2010 held at Chennai, India  Presented Paper on “Determination of optimum adhesive thickness using varying degree of force application and its effect on shear bond strength: an in-vitro study” at 46th Indian Orthodontic Conference 2011 held at Khajuraho, India.
  • 3. Determination of Optimum adhesive thickness using differential force application with light cure adhesive & its effects on shear bond strength: an in-vitro study
  • 4. Introduction  The main concern with the orthodontists is to achieve stable bond strength which depends on many factors which includes:  Bracket base design  Adhesive thickness  Adhesive composition  Type of enamel conditioner  Length of etching time and so on Many studies have evaluated the effect of these mentioned variables on shear bond strength, however the effect of adhesive thickness on bond strength largely remain unstudied.
  • 5. Uniform adhesive thickness present between bracket base and tooth surface may prevent the need for compensatory bends that to be placed in finishing arch wires thereby, help in full utilization of PEA and to obtain perfect finish.
  • 6. Aims & Objectives  Effect of varying thickness of adhesive on shear bond strength of orthodontic bracket.  To determine the optimum adhesive thickness achieved between tooth surface and bracket with light cured adhesive.
  • 7. Materials and Methods Based on amount of force applied while bonding Materials &Methods
  • 8. Bucco-lingual width of each premolar along with bracket was measured Bucco-lingual width of each premolar was measured again after bonding Bracket was subjected to force applied at centre of bracket using a fork end of Dontrix guage Determining adhesive thickness
  • 9. Hence, difference in bucco lingual width of each premolar with bracket prior to bonding and after bonding is measured ;thereby adhesive thickness is determined for specified force application.
  • 10.  The mean, standard deviation and confidence interval for mean were calculated for each group  Analysis of variance (ANOVA) was used to determine whether significant differences existed between the various group compared.  Significance of level was predetermined at p value <0.001.  The Bonferroni multiple comparison test was applied to find the group with significant difference.  Pearson Correlation test was performed to correlate the relationship between adhesive thicknesses and shear bond strength  Weibull analysis was used to calculate the probability of failure at given values of applied force. STATISTICAL ANALYSIS
  • 11. Results 20 .9950 .04968 .01111 .9717 1.0183 127.591 p<0.001 20 .8365 .03951 .00883 .8180 .8550 HS 20 .7245 .06825 .01526 .6926 .7564 . Group A Group B Group C adhesive thickness (mm) N Mean Std. Deviation Std. Error Lower Bound Upper Bound 95% Confidence Interval for Mean ANOVA F value p value Table I: Descriptive statistics of the three groups and comparison of adhesive thickness by ANOVA tests. Results
  • 12. Multiple Comparisons Bonferroni .15850 .01702 p<0.001 HS .27050 .01702 p<0.001 HS .11200 .01702 p<0.001 HS (J) Group Group B Group C Group C (I) Group Group A Group B Dependent Variable adhesive thickness (mm) Mean Difference (I-J) Std. Error p Table II: Multiple comparisons of adhesive thickness between three groups using Bonferroni test.
  • 13. 20 6.364 1.2727 .2846 5.768 6.960 23.956 p<0.001 20 9.559 1.4383 .3216 8.885 10.232 HS 20 8.577 1.7372 .3884 7.764 9.390 Group A Group B Group c Shear bond strength(MPa) N Mean Std. Deviation Std. Error Lower Bound Upper Bound 95% Confidence Interval for Mean ANOVA F value p value Table III: Descriptive statistics of the three groups and comparison of shear bond strength by ANOVA tests.
  • 14.   Multiple Comparisons Bonferroni -3.1945 .4728 p<0.001 HS -2.2130 .4728 p<0.001 HS .9815 .4728 .127 NS (J) Group Group B Group C Group C (I) Group Group A Group B Dependent Variable Shear bond strength(MPa) Mean Difference (I-J) Std. Error p Table IV: Multiple comparisons of shear bond strength between three groups using Bonferroni test
  • 15. Correlations -.528 .017 sig .408 .074 NS .122 .607 NS Shear bond strength(MPa) Shear bond strength(MPa) Shear bond strength(MPa) adhesive thickness (mm) adhesive thickness (mm) adhesive thickness (mm) Group Group A Group B Group C Pearson Correlation p value Table V: Pearson's correlation test
  • 16. % failure Reliability Group A Group B Group C 99.9% 0.001 1.109 0.925 0.885 99% 0.01 1.089 0.909 0.856 95% 0.05 1.069 0.893 0.826 5% 0.95 0.892 0.756 0.590 1% 0.99 0.829 0.707 0.515 Beta ( shape parameter/weibull modulus) 22.49 24.31 12.08 Alpha (characteristic life) 1.018 0.8545 0.7547 Mean adhesive thickness(mm) 0.995 0.836 0.724 Table VI: Weibull analysis for adhesive thickness
  • 17. % failure Reliability Group A Group B Group C 99.9% 0.001 9.62 13.18 13.16 99% 0.01 8.96 12.48 12.24 95% 0.05 8.31 11.78 11.32 5% 0.95 4.08 6.83 5.43 1% 0.99 3.07 5.49 4.04 Beta ( shape parameter/weibull modulus) 5.725 7.467 5.539 Alpha (characteristic life) 6.867 10.175 9.291 Mean shear bond strength (MPa) 6.36 9.55 8.57 Table VII: Weibull analysis for shear bond strength
  • 18. Thus, the increase in the applied force while bonding results in the decreased thickness of the adhesive between bracket base and tooth surface. However, the amount of thickness may vary not only due to the pressure, but also to the viscosity of the adhesive used. Discussion Most of the studies done till now use firm pressure while placing bracket on the enamel surface with assumption that uniform thickness of adhesive is achieved, but as shown in the present study even a change of 1ounce force brings about significant change in adhesive thickness. Mackay also noted that the stiffness of each material depends on size, type and amount of the filler content and monomer used. Therefore, adhesive thickness obtained in this study by varying the force of application is meant only for adhesive Transbond XT. Hence, different types of adhesive resins will produce different thickness while applying same amount of force.
  • 19. However, Mackay (1992) reported that increasing the thickness of adhesives had no statistically significant effect on their mean shear bond strength, although the trend was to decreased. Evans, Powers (1985) noted that the tensile bond strength was decreased with increased adhesive thickness. These results are similar to that reported by Jost- Brinkmann, Schechter & others. As adhesive thickness reduces, shear bond strength first increases from group A (6.36 MPa) to group B (9.55 MPa), but then it decreases in group C (8.57MPa); and it is highly statistically significant. As suggested by Buonocore (1963) & Alster(1995), increasing the thickness of the adhesive layer results in a weaker joint due to the increased polymerization shrinkage seen in thicker layers, along with the imperfections which lead to increase in stress concentrations and hence decreasing the strength.
  • 20. Interesting finding to be noted here is that shear bond strength reduces in group C (8.57 MPa), although its thickness is minimum (0.72mm). Although, these findings are quite similar to our findings, but this cannot be compared directly as material and methodology in these studies were different from the present study. An explanation of this finding could be that strength of any material depends on its volume to a larger extent, and since the thickness of group C is minimum we can expect bond failure to occur early. Li et al too reported that volume of filler had a greater effect on physical and mechanical properties than filler size. Arici et al noticed that mean shear bond strength increased as adhesive thickness increased; but they have tested shear bond strength at interval of 0.25mm thickness starting from 0mm to 0.5mm.
  • 21. Hence, Weibull analysis is performed here to analyze the characteristic bond strength and to know the probability of failure for each of the material. Higher weibull modulus (ÎČ) indicates a more predictable system and possibly, a more clinically reliable system. Group B produced higher modulus (ÎČ) values than other groups, hence the group B could be consider as more predictable and clinically reliable system. Hence, we can infer that optimum adhesive thickness is required; because shear bond strength has a tendency to decrease with decreasing thickness. As indicated by Fox et al, mean and standard deviation values of bond strengths are not the best indicators of the performance of any bonding material.
  • 22. Weibull analysis also showed that force needed for 99.9% chance of failure is maximum for group B (13.18 MPa) and minimum for group A(9.62 MPa). It means that group B can withstand higher forces when compared to all other groups. Therefore, group B with mean shear bond strength of 9.55MPa having a mean adhesive thickness of 0.83mm could be considered as the group having optimum adhesive thickness required to achieve sufficient bond strength to prevent chances of bond failure. Thus, application of controlled bonding pressure (2 oz as we obtained in this study) through a bracket holder that has a pressure gauge could be the correct way to gain a uniform optimum adhesive thickness (0.83mm) between the bracket and enamel.
  • 23. Adhesive thickness between bracket base and tooth surface decreases with increasing the amount of force application from 1ounce to 3 ounces. Mean shear bond strength increases when adhesive thickness decreases from group A to Group B and then it has a tendency to decrease as shown in group C. 0.83mm could be considered as optimum adhesive thickness which is required to achieve sufficient bond strength to prevent chances of bond failure. Conclusion
  • 24. 1. Andrews LF. Interviews on the straight wire appliance. J Clin Orthod. 1990; 24: 493-508. 2. Buonocore MG. A simple method of increasing the adhesion of acrylic filling material to enamel surfaces. J Dent Res 34:849-853, 1955. 3. Mackay F. The effect of adhesive type and thickness on bond strength of orthodontic brackets. Br J Orthod 1992;19:35-39. 4. SchechterG., Caputo A.A. Chaconas S.J. The effect of adhesive thickness on retention of direct bonded brackets, Journal of Dental Research. 1980;59:285 5. Jost-Brinkmann PG, Schiffer A, Miethke RR.. The effect of adhesive thickness layer on shear bond strength. J.Clin. Orthod. 1992;26(11):718- 720. 6. Arici S, Benan O, Arici N. Adhesive thickness effects on the bond strength of a lightcured resin- modified glass ionomer cement. Angle Orthod 2005; 75(2); 254-259.. Farmararz M, Akhoundi M, References
  • 25. 7. Farmararz M, Akhoundi M. Comparison of wire loop and shear blade as the 2 most common methods for testing orthodontic shear bond strength. Am J Orthod Dentofacial Orthop 2006;130:385-7. 8. Klocke A, Neike B. Effect of debonding force direction on orthodontic shear bond strength. . Am J Orthod Dentofacial Orthop 2006; 129:261- 5. 9. Eliades T, Brantley WA. The inappropriateness of conventional orthodontic bond strength assessment protocols. Eur J Orthod 2000; 22:13-23. 10. Evans L, Powers JM. In vitro bond strength of no-mix orthodontic cements. Am J Orthod. 1985; 37: 508 – 12.
  • 26. 11. Alster D, Feilzer AJ, De Gee AJ, Davidson CL.. Tensile strength of thin resin composite layers as a function of layer thickness. J Dent Res 1995; 74(11): 1745-8. 12. Li Y, Swartz ML, Phillips RW, Moore BK, Roberts TA.. Effect of filler content and size on properties of composites J Dent Res 1985; 63: 1396- 1401. 13. Reynolds JR. A review of direct orthodontic bonding. Br J Orthod 1975;2:171-178. 14. Fox N A, McCabe J F, Buckley J G. A critique of bond strength testing in orthodontics.Br J Orthod 1994; 21: 33-43.

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