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Flammability Testing of Plastics By  Jinish Doshi Matrikulation Nr. : 26869 M. Sc. In Polymer Technology Aalen University of Applied Sciences
Overview ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Why add flame retardants? ,[object Object],[object Object],[object Object],[object Object]
Types of Flame Retardants ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Standards for Flammability Testing of Plastic Materials ,[object Object],[object Object],[object Object],[object Object]
Flammability Tests ISO 4589-1, -2  Limiting Oxygen Index IEC 60695-2, -13 Glow Wire Ignition Temperature (GWIT) IEC 60695-2, -12  Glow Wire Flammability Index (GWFI) UL 94 - Flame Rating Other   ISO   Flammability
Types of pre-selection test programs ,[object Object],[object Object],[object Object],[object Object]
UL 94 Flame Classifications ,[object Object],[object Object],[object Object],[object Object],[object Object]
UL 94 Flame Classifications ,[object Object],[object Object]
UL 94 Test: Sample Preparation ,[object Object],Note : All dimensions are in mm
Horizontal Testing (HB) Flame applied only once
Horizontal Testing (HB) Specimens must stop burning before the flame reaches the 100 mm mark Specimens must not have a burning rate greater than 40 mm/minute for thicknesses between 3 and 13 mm and 75 mm/minute for thicknesses less than 3 mm HB Requirements   Horizontal Rating
Vertical Testing (V0, V1, V2) Flame is applied twice
Vertical Testing (V0, V1, V2) No specimen can have glowing combustion remain for longer than 30 seconds after removal of the test flame  Specimens must not drip flaming particles that ignite the cotton Specimens must not burn with flaming or glowing combustion up to the specimen holding clamp Total flaming combustion time must not exceed 50 seconds for each set of 5 specimens Specimens must not burn with flaming combustion for more than 10 seconds after either test flame application  V-0 Requirement Vertical Rating
Vertical Testing (V-0, V-1, V-2) No specimen can have glowing combustion remain for longer than 60 seconds after removal of the test flame Total flaming combustion time must not exceed 250 seconds for each set of 5 specimens Specimens can drip flaming particles that ignite the cotton V-2 Specimens must not burn with flaming combustion for more than 30 seconds after either test flame application V-1 Requirement Vertical Rating
Vertical Testing (5V-A, 5V-B) Flame is applied 5 times at an interval of 5 seconds
Vertical Testing (5V-A, 5V-B) Specimens must not have any flaming or glowing combustion for more than 60 seconds after the five flame applications  5V-A Plaque specimens may exhibit burn through (a hole)   5V-B Plaque specimens must not exhibit burn through (a hole)  Specimens must not drip flaming particles that ignite the cotton  Requirements Vertical Rating
Horizontal v/s Vertical Positioning ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Vertical Testing of Thin Materials (VTM-0, VTM-1, VTM-2) Flame applied at an interval of 3 seconds twice for a set of 5 specimens
Vertical Testing of Thin Materials  (VTM-0, VTM-1, VTM-2) No specimen shall have flaming or glowing combustion up to a mark 125 mm from the bottom of the specimen No specimen can have glowing combustion remain for longer than 30 seconds after removal of the test flame  Specimens must not drip flaming particles that ignite the cotton  Specimens must not burn with flaming or glowing combustion up to the specimen holding clamp  Total flaming combustion time must not exceed 50 seconds for each set of 5 specimens  Specimens must not burn with flaming combustion for more than 10 seconds after either test flame application  VTM-0 Requirements Vertical Rating
Vertical Testing of Thin Materials  (VTM-0, VTM-1, VTM-2) Specimens can drip flaming particles that ignite the cotton   VTM-2 No specimen can have glowing combustion remain for longer than 60 seconds after removal of the test flame   Total flaming combustion time must not exceed 250 seconds for each set of 5 specimens   Specimens must not burn with flaming combustion for more than 30 seconds after either test flame application   VTM-1 Requirements Vertical Rating
Glow Wire Flammability  Index (GWFI) ,[object Object],[object Object],[object Object],[object Object],[object Object],(˚C) Contact Time Test Temperatures 30 seconds 960 900 850 800 750 700 650 600 550
Glow Wire Flammability  Index (GWFI) With Flame Without Flame
Glow Wire Ignition  Temperature (GWIT) ,[object Object],[object Object],[object Object],[object Object],30 seconds Contact Time 960 900 850 800 750 700 650 600 550 Test  (˚C) Temperatures
Limited Oxygen Index (LOI) ,[object Object],[object Object],[object Object],[object Object]
Limited Oxygen Index: Sample Preparation Thin Film  0.02-0.1 20 140-200 6 Flexible Film or Sheet  10.5 52 140 5 Alternative size for molding or sheet materials. For electrical purposes.  3 6.5 70-150 4 Sheet Materials  <10.5 10 80-150 3 Cellular Materials  10 10 80-150 2 Molding Materials  4 10 80-150 1 Usage Thickness (mm) Width (mm) Length (mm) Specimen Test Specimens
RoHS Compliant Materials ,[object Object],1000 Polybrominated diphenyl ether (PBDE) 1000 Polybrominated biphenyl (PBB) 1000 Mercury (Hg) 1000 Lead (Pb) 1000 Hexavalent Chromium (Cr+6) 100 Cadmium (Cd) ppm Restricted Substance
References ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Thank You

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Flammability Testing Of Plastics Jinish Doshi

  • 1. Flammability Testing of Plastics By Jinish Doshi Matrikulation Nr. : 26869 M. Sc. In Polymer Technology Aalen University of Applied Sciences
  • 2.
  • 3.
  • 4.
  • 5.
  • 6. Flammability Tests ISO 4589-1, -2 Limiting Oxygen Index IEC 60695-2, -13 Glow Wire Ignition Temperature (GWIT) IEC 60695-2, -12 Glow Wire Flammability Index (GWFI) UL 94 - Flame Rating Other ISO Flammability
  • 7.
  • 8.
  • 9.
  • 10.
  • 11. Horizontal Testing (HB) Flame applied only once
  • 12. Horizontal Testing (HB) Specimens must stop burning before the flame reaches the 100 mm mark Specimens must not have a burning rate greater than 40 mm/minute for thicknesses between 3 and 13 mm and 75 mm/minute for thicknesses less than 3 mm HB Requirements Horizontal Rating
  • 13. Vertical Testing (V0, V1, V2) Flame is applied twice
  • 14. Vertical Testing (V0, V1, V2) No specimen can have glowing combustion remain for longer than 30 seconds after removal of the test flame Specimens must not drip flaming particles that ignite the cotton Specimens must not burn with flaming or glowing combustion up to the specimen holding clamp Total flaming combustion time must not exceed 50 seconds for each set of 5 specimens Specimens must not burn with flaming combustion for more than 10 seconds after either test flame application V-0 Requirement Vertical Rating
  • 15. Vertical Testing (V-0, V-1, V-2) No specimen can have glowing combustion remain for longer than 60 seconds after removal of the test flame Total flaming combustion time must not exceed 250 seconds for each set of 5 specimens Specimens can drip flaming particles that ignite the cotton V-2 Specimens must not burn with flaming combustion for more than 30 seconds after either test flame application V-1 Requirement Vertical Rating
  • 16. Vertical Testing (5V-A, 5V-B) Flame is applied 5 times at an interval of 5 seconds
  • 17. Vertical Testing (5V-A, 5V-B) Specimens must not have any flaming or glowing combustion for more than 60 seconds after the five flame applications 5V-A Plaque specimens may exhibit burn through (a hole) 5V-B Plaque specimens must not exhibit burn through (a hole) Specimens must not drip flaming particles that ignite the cotton Requirements Vertical Rating
  • 18.
  • 19. Vertical Testing of Thin Materials (VTM-0, VTM-1, VTM-2) Flame applied at an interval of 3 seconds twice for a set of 5 specimens
  • 20. Vertical Testing of Thin Materials (VTM-0, VTM-1, VTM-2) No specimen shall have flaming or glowing combustion up to a mark 125 mm from the bottom of the specimen No specimen can have glowing combustion remain for longer than 30 seconds after removal of the test flame Specimens must not drip flaming particles that ignite the cotton Specimens must not burn with flaming or glowing combustion up to the specimen holding clamp Total flaming combustion time must not exceed 50 seconds for each set of 5 specimens Specimens must not burn with flaming combustion for more than 10 seconds after either test flame application VTM-0 Requirements Vertical Rating
  • 21. Vertical Testing of Thin Materials (VTM-0, VTM-1, VTM-2) Specimens can drip flaming particles that ignite the cotton VTM-2 No specimen can have glowing combustion remain for longer than 60 seconds after removal of the test flame Total flaming combustion time must not exceed 250 seconds for each set of 5 specimens Specimens must not burn with flaming combustion for more than 30 seconds after either test flame application VTM-1 Requirements Vertical Rating
  • 22.
  • 23. Glow Wire Flammability Index (GWFI) With Flame Without Flame
  • 24.
  • 25.
  • 26. Limited Oxygen Index: Sample Preparation Thin Film 0.02-0.1 20 140-200 6 Flexible Film or Sheet 10.5 52 140 5 Alternative size for molding or sheet materials. For electrical purposes. 3 6.5 70-150 4 Sheet Materials <10.5 10 80-150 3 Cellular Materials 10 10 80-150 2 Molding Materials 4 10 80-150 1 Usage Thickness (mm) Width (mm) Length (mm) Specimen Test Specimens
  • 27.
  • 28.