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Advanced Technologies to 
Reclaim roadways

      APWA Annual Meeting
      Tampa, FL
      April 5th, 2012
. Contents:
     .Eurovia Cold recycling technologies;
              .Recyflex’s ®, in‐plant processing:
                        .Formulation specifications
                        .Production, laying and compaction operations
                        .Rheological performances
                        .VLE roadway concept

              .Recyvia ®, in‐place (FDR)
              .Recyclovia ®, in‐place (CIR)
     .Recycled cold treated materials behavior;

     .Environmentals analysis;
. Recyflex’s specifications:
      .Strengthening base layer: AEC 25, AEC 20
                .Composite binder 
                          .Asphalt emulsion
                          .Cement or lime
                          .Dense gradation
      .Drainage / Frost  protection layer: HD 25
                .Composite binder
                .High air voids produce by special gradation
      ..Intermediate layer: AEC 12.5 
                ..Composite binder and dense gradation
Recyflex AEC
Strengthening course materials




                                 RECYFLEX AEC : Cold‐in‐plant treated 
                                 recycled materials by using  
                                 composite binder
Recyflex AEC Base Material
 In‐plant cold retreated material
      Mineral aggregate using 50 to 100% of recycling material (from existing pavement structure)
      Asphalt emulsion and cement/ lime treatment
      Highly improve bearing capacity instead of regular granular material
      Indirect tensile Resilient Modulus at 10°C > 4 000 MPa
      Density of 2 100 kg/m³ (air voids of 12‐15%) 
Recyflex HD
 High drainability material
      Mineral aggregate using 30 to 50% of recycling material (from existing pavement structure)
      Low density = Air void insulation, 1 800 kg/m³
      Porous material = air voids ± 30% 
      Asphalt emulsion and cement/lime treatment
      Frost penetration reduction
RECYFLEX AEC 0/20 mm


Production by using 
portable plant
RECYFLEX AEC 0/20 mm, Thickness application of 100 @ 300 mm
RECYFLEX AEC 0/20 mm, Grading/ Compaction operations




            Final aspect during the cure period
Recyflex AEC                    Protection and Paving




Application of tack coat emulsion


            Chipping application
RECYFLEX AEC, A‐20 Mix Rheological performances
   Formulation:                                             Proportions established from the 
            40% of Crushed concrete;                         rehabilitation existing roadway 
            40% of Rap                                        (optimization of the recycled 
            20% of new aggregates screenings                            quantities)
            Composite binders: Asphalt emulsion + cement 


   Physical and Rheologicals Characterization of:
            Voids and densities;
            Cohesion built‐up behavior;
            Rutting resistance;
            Modulus evolution vs curing time;
            Effects of Freeze and thaw cycles on the mechanical performances;
            Tensile stress vs low temperture.     
Laboratory samples preparation by Vibrocompression method 
            Piston : axial force




Vibration                          Molds




                                                           Diameter = 16 cm , High
                                                           = 32 cm
                                                           Voids average 16.5%


                                           Gammadensitometer
100


Visual Voids analysis                90
                                     80
                                     70




                           psa t -
  with ultraviolets




                          % a s nd
                                     60
                                     50
                                     40
                                     30
                                     20
                                     10
                                      0
                                       0.01   0.10     1.00    10.00   100.00
                                                     Tamis (mm)




      Air voids




                                                               RAP
       Crushed Concrete
Physical Characteristics                              Emulsion treated base 
                                                      material (Grave‐Émulsion)
   Rheologicals Characteristics study 2001 
      French Gyratory compactor
           Voids at 10 gyrations = 21.2%            22%
           Voids at 200 gyrations = 13.0%           15%

        Duriez
           Resistance before immersion = 6.4 Mpa    4Mpa
           r/R ratio = 0.68                         0.55
           Duriez voids = 11.7%                     13%
Rheological Characteristics                                    Rutting resistance spec. on 
                                                                     HMA < 10% after 30 000 
    Rutting test analysis                                           cycles at 60°C
       Rutting
             Only 0.7% after100 000 cycles at 60°C, Exceptional performance



             Material without rutting
             due to the internal
             aggregates friction and 
             the presence of 
             hydraulic binder   




    Rutting test machine
        Cohesion Built‐up behavior

                                   Time




               600
                                          Emulsion mix
               500
Force (N)
   Force, kN




               400
                                                          Workability of ± 3 hours
               300

               200                                        Recyflex AEC

               100

                0
                     0   30   60    90    120    150     180    210     240
                                      Time, min.
                         Temps de conservation (minutes)
Rheologicals behavior study

   Stiffness Modulus analysis

        Diametral Sinusoïdal Compression ‐DSC
            Bresilian test :
                Rupture limit establishement = 8800 N
                DSC strenght at 20% of the rupture limit


             DSC testing at 1.00 kN  0.75 kN corresponding of maximale compression of 1750 N
Modulus evolution with CDS
                         9000

                                    curve at 10°C
                                                                                        900 Mpa
                         8000                                                          or +11,5%
Modulus at 10 Hz (MPa)




                                                              curve at 15°C
                         7000



                         6000


                                                          Effect of the hydraulic binder
                         5000



                         4000
                                0    7   14   21    28   35   42    49    56    63     70   77   84   91
                                               Time from production (days)
Rheologicals behavior study

   Freeze and thaw cycles effects

       Diametral Sinusoïdal Compression –DSC

            Two types of simulation
                Short term freeze‐thaw : 2 cycles of 24 hours produced between the 4th and 
                  52th hours of curing, each cycle corresponding to a: 
                   temperature drop of +5°C to ‐10°C in 12 hours
                   temperature gain of ‐10°C to +5°C in 12 hours

                  Long term freeze‐thaw : 50 freeze‐thaw cycles after optimun cohesion, each 
                   cycle corresponding to a:
                  Temperature drop of +10°C to ‐20°C in less 3 hours
                  Temperature gain of ‐20°C to +10°C in less 3 hours
Effect freeze‐thaw cycles, short term

                          Modulus measurements
                                 Diametral Sinusoïdal Compression ‐DSC
                                     Freeze‐thaw  at beginning  Modulus evolution at 10 Hz




                       9000                                                                     9000        Air curing
Modulus at 15°c, MPa




                                                                         Modulus at 10°c, MPa
                       8000          Air curing                                                 8000                             - 11.5%
                                                            - 9.4%                              7000
                       7000
                                                                                                                          Freeze-thaw
                       6000                          Freeze-thaw                                6000
                                                                                                             - 22.8%
                                      - 23.5%                                                   5000
                       5000
                       4000                                                                     4000
                              0 10 20 30 40 50 60 70 80 90                                             0 10 20 30 40 50 60 70 80 90
                               Temps depuis fabrication (jours)                                         Temps depuis fabrication (jours)
                                           Time, hours                                                             Time, hours
Effect freeze‐thaw cycles, short term

   Modulus measurements

        Diametral Sinusoïdal Compression –DSC

             Short term freeze‐thaw during beginning of curing
                 Freeze‐thaw between the 4th and 52th hours of curing

                 Slowing down cement hydratation phenomenon at the beginning with small 
                   effect on long term
                 Delayed internal cohesion

                 Modulus loss of about 23% at  10 days

                 Long term modulus loss of about 10% (> 90 days)

                 Validated value after 365days
Effect freeze‐thaw cycles, long term

    Modulus measurements

         Diametral Sinusoïdal Compression –DSC

              Long term freeze‐thaw cycles 
                  Freeze‐thaw (50 cycles) between 24d et 36d

                  Modulus loss of 20% immediatly after the thermal sollicitations

                  Modulus recovery « normal » at long term
Effect of 50 freeze‐thaw cycles, long term
                         9000
                                                     curve at 15°C
                                                     without freeze-
                         8000                             thaw
Modulus at 10 Hz (MPa)




                                     24 days

                         7000                      - 20%


                         6000             37days


                                          50 freeze-thaw
                         5000                  cycles



                         4000
                                10                               100         1000
                                               Time from production (days)
Rheologicals behavior study
                     Thermal stress, Contraints development




                      5.0
Tensile strain, MPa




                      4.0                     HM A wit h 70
 Contrainte
   (Mpa)df




                                              /100 bit umen
                      3.0
                      2.0
                                   RECYFLEX 
                      1.0
                                     EBC
                      0.0
                            -35      -30 -25           -20     -15 -10   -5   0   5
                                                   Température (°C)
                                                    Temperature, °C
Recyflex AEC Observations


    Process for optimun use of recyclable materials;
    Cold treatment using composite binder
    Strenghtened materials
    Low emissions production
    Accelarated curing time
    No rutting 
    Avoid maniability over 3 hours
Recyflex AEC Observations


  Behavior between flexible and rigid pavements
  DSC Modulus
     E (15°C,10Hz) = 7600 Mpa 

     Optimum around 30d‐60d

     Definitive loss of 10% in case of freeze‐thaw in the firsts hours of 
      cure
     Temporary loss of 20% after freeze‐thaw if Recyflex AEC have 
      obtained the optimal cure
  Low contrains development with thermal reduction

  Fatigue analysis to complete
Flexibles pavement structures comparaison, A20 Highway

      80 M esal : 2X 2 lanes (3450 Truks/day/direction/TL over 20 years)
      Supposed Recyflex AEC Resilient Modulus = 3 000 MPa

                                                                                 Recyflex AEC
                 Chaussée                          Ecoroute                       Alternative
  0                                                                               25 RUGOVIA TM
 50             60 ESG-10                         60 ESG-10
                                                                                   60 ESG-14
100             70 ESG-14                         70 ESG-14                         100 HMA
150                                                                                  Binder
200            160 HMA-20                        180 HMA-20
250
                                                                              200 RECYFLEX AEC
300
350
           Residual pavement structure     Residual pavement structure
400
450                                                                        Residual pavement structure

500
Highway , Alternate pavement design

                        Hwy 485 Asphalt Pavement Design
                                         Alternate 1
                                                AASHTO Structual
      Thickness (in.)      Material              Coefficient Value       Structual total
            3              S9.5D                        0.44                  1.32
            4              I19.0D                       0.44                  1.76
           11.5            B25.0C                       0.3                   3.45
                                                                                0
                          Subgrade
            7            Stabilization                 0.14                   0.98
                                                 Total Structual Value        7.51


                                         Alternate 4
                                               AASHTO Structual
      Thickness (in.)      Material              Coefficient Value       Structual total
            3              S9.5D                        0.44                  1.32
            6              I19.0D                       0.44                  2.64
            0              B25.0C                       0.3                     0
            8            Recyflex                     0.34                   2.72
                          Subgrade
            7            Stabilization                 0.14                   0.98
                                                 Total Structual Value        7.66
Highway , Alternate pavement design
Recyflex AEC,
                                     Arrival from Paris


Main Runway Montreal airport‐ 1998




 Arrival from Orlando
Development of a new Roadway pavement structure concept by 
using recycled materials




                                          Recyflex
                                          AEC




                                                              31
Recyvia, in‐Place (FDR)
   In‐Place full depth reclamation




                             Cold In place  Recycling using composite binder or bitumen 
                                             emulsion /foamed bitumen
Example of using composite binder in‐Place




Réalisation du projet
   stabilisation




     Stabilisation 175mm (16/08 au 28/08)
                    ±56800m²
RECYCLOVIA® 
Field of application




   CIR In‐Place Cold recycling 
           Existing Asphalt 
                  6 à >15 cm.
              pavement
                                                         Chip Seal        1 à 5 cm.                Chip Seal           1 à 5 cm.


                                                                                                 Granular base
         Granular Base or                             Granular base
          Treated base 



                                                                                             Supply of aggregate for
                                                                                              gradation correction


RECYCLOVIA ®                                RECYCLOVIA ®                              RECYCLOVIA ®

In‐Place treatment : 6 à 15 cm              In‐Place treatment :8 à 15 cm             In‐Place treatment: 8 à 15 cm  
 Asphalt Emulsion with                      Asphalt Emulsion / Foam asphalt           Asphalt Emulsion / Foam asphalt
 Cement                                      with Cement or hydrated lime             With cement or hydrated lime




                                             + HMA / WMA wearing course
                               Microsurfacing / Chip seal / Dense Cold mix (low trafic road)
Recyclovia, in‐Place (CIR)
      Weight empty: 47 t
      Power : 800 hp 600 kW
      Lenght : 15 m
                                                                              Cement bin (4 t)




Paver screed, extendable      Rotor for milling/recycling/mixing, with    Cement spreader unit
equiped with tamper bar       possible injection of:
compactor                     ‐ Foam asphalt
                              ‐ Asphalt emulsion
                              ‐ Water
Recyclovia
Recyclovia, in‐Place (CIR)
‐Recycled cold treated materials behavior


     ‐Same mix design methodology for In‐plant, FDR and CIR;

           ‐Mechanical performances, Stability and Modulus;
           ‐Air Voids;
           ‐Retained Stability; 

     ‐Observations behavior:

           ‐Effect of RAP content

                                                   Mix 1            Mix 2            Mix 3
                                Requirements       38% CC           40% CC           100% RAP
                                    Min.           16% RAP          40% RAP
                                                   45% Aggregates   20% Aggregates
 % Recovering Asphalt                                     0,63%          2,10%          5,38%
 % Added Bitumen                                          1,53%          1,85%           1,0%
 Marchall Stability at         7 000 @ 10 000            26 200          18 583         8 575
 22.2°C (N)
 Retained Stability (%)               70                       84           90           93

 % Coating                            50                       82           88           95
‐Recycled cold treated materials behavior
Complete environmental impact analysis
Thanks for your attention




                     Janvier 2011 - page 43

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Advanced Technologies To Reclaim Roadways

  • 1. Advanced Technologies to  Reclaim roadways APWA Annual Meeting Tampa, FL April 5th, 2012
  • 2. . Contents: .Eurovia Cold recycling technologies; .Recyflex’s ®, in‐plant processing: .Formulation specifications .Production, laying and compaction operations .Rheological performances .VLE roadway concept .Recyvia ®, in‐place (FDR) .Recyclovia ®, in‐place (CIR) .Recycled cold treated materials behavior; .Environmentals analysis;
  • 3. . Recyflex’s specifications: .Strengthening base layer: AEC 25, AEC 20 .Composite binder  .Asphalt emulsion .Cement or lime .Dense gradation .Drainage / Frost  protection layer: HD 25 .Composite binder .High air voids produce by special gradation ..Intermediate layer: AEC 12.5  ..Composite binder and dense gradation
  • 4. Recyflex AEC Strengthening course materials RECYFLEX AEC : Cold‐in‐plant treated  recycled materials by using   composite binder
  • 5. Recyflex AEC Base Material  In‐plant cold retreated material  Mineral aggregate using 50 to 100% of recycling material (from existing pavement structure)  Asphalt emulsion and cement/ lime treatment  Highly improve bearing capacity instead of regular granular material  Indirect tensile Resilient Modulus at 10°C > 4 000 MPa  Density of 2 100 kg/m³ (air voids of 12‐15%) 
  • 6. Recyflex HD  High drainability material  Mineral aggregate using 30 to 50% of recycling material (from existing pavement structure)  Low density = Air void insulation, 1 800 kg/m³  Porous material = air voids ± 30%   Asphalt emulsion and cement/lime treatment  Frost penetration reduction
  • 10. Recyflex AEC Protection and Paving Application of tack coat emulsion Chipping application
  • 11. RECYFLEX AEC, A‐20 Mix Rheological performances  Formulation:  Proportions established from the   40% of Crushed concrete; rehabilitation existing roadway   40% of Rap (optimization of the recycled   20% of new aggregates screenings quantities)  Composite binders: Asphalt emulsion + cement   Physical and Rheologicals Characterization of:  Voids and densities;  Cohesion built‐up behavior;  Rutting resistance;  Modulus evolution vs curing time;  Effects of Freeze and thaw cycles on the mechanical performances;  Tensile stress vs low temperture.     
  • 12. Laboratory samples preparation by Vibrocompression method  Piston : axial force Vibration Molds Diameter = 16 cm , High = 32 cm Voids average 16.5% Gammadensitometer
  • 13. 100 Visual Voids analysis  90 80 70 psa t - with ultraviolets % a s nd 60 50 40 30 20 10 0 0.01 0.10 1.00 10.00 100.00 Tamis (mm) Air voids RAP Crushed Concrete
  • 14. Physical Characteristics Emulsion treated base  material (Grave‐Émulsion)  Rheologicals Characteristics study 2001   French Gyratory compactor  Voids at 10 gyrations = 21.2%  22%  Voids at 200 gyrations = 13.0%  15%  Duriez  Resistance before immersion = 6.4 Mpa  4Mpa  r/R ratio = 0.68          0.55  Duriez voids = 11.7%  13%
  • 15. Rheological Characteristics Rutting resistance spec. on  HMA < 10% after 30 000   Rutting test analysis cycles at 60°C  Rutting  Only 0.7% after100 000 cycles at 60°C, Exceptional performance Material without rutting due to the internal aggregates friction and  the presence of  hydraulic binder    Rutting test machine
  • 16. Cohesion Built‐up behavior Time 600 Emulsion mix 500 Force (N) Force, kN 400 Workability of ± 3 hours 300 200 Recyflex AEC 100 0 0 30 60 90 120 150 180 210 240 Time, min. Temps de conservation (minutes)
  • 17. Rheologicals behavior study  Stiffness Modulus analysis  Diametral Sinusoïdal Compression ‐DSC  Bresilian test :  Rupture limit establishement = 8800 N  DSC strenght at 20% of the rupture limit  DSC testing at 1.00 kN  0.75 kN corresponding of maximale compression of 1750 N
  • 18. Modulus evolution with CDS 9000 curve at 10°C 900 Mpa 8000 or +11,5% Modulus at 10 Hz (MPa) curve at 15°C 7000 6000 Effect of the hydraulic binder 5000 4000 0 7 14 21 28 35 42 49 56 63 70 77 84 91 Time from production (days)
  • 19. Rheologicals behavior study  Freeze and thaw cycles effects  Diametral Sinusoïdal Compression –DSC  Two types of simulation  Short term freeze‐thaw : 2 cycles of 24 hours produced between the 4th and  52th hours of curing, each cycle corresponding to a:   temperature drop of +5°C to ‐10°C in 12 hours  temperature gain of ‐10°C to +5°C in 12 hours  Long term freeze‐thaw : 50 freeze‐thaw cycles after optimun cohesion, each  cycle corresponding to a:  Temperature drop of +10°C to ‐20°C in less 3 hours  Temperature gain of ‐20°C to +10°C in less 3 hours
  • 20. Effect freeze‐thaw cycles, short term  Modulus measurements  Diametral Sinusoïdal Compression ‐DSC  Freeze‐thaw  at beginning  Modulus evolution at 10 Hz 9000 9000 Air curing Modulus at 15°c, MPa Modulus at 10°c, MPa 8000 Air curing 8000 - 11.5% - 9.4% 7000 7000 Freeze-thaw 6000 Freeze-thaw 6000 - 22.8% - 23.5% 5000 5000 4000 4000 0 10 20 30 40 50 60 70 80 90 0 10 20 30 40 50 60 70 80 90 Temps depuis fabrication (jours) Temps depuis fabrication (jours) Time, hours Time, hours
  • 21. Effect freeze‐thaw cycles, short term  Modulus measurements  Diametral Sinusoïdal Compression –DSC  Short term freeze‐thaw during beginning of curing  Freeze‐thaw between the 4th and 52th hours of curing  Slowing down cement hydratation phenomenon at the beginning with small  effect on long term  Delayed internal cohesion  Modulus loss of about 23% at  10 days  Long term modulus loss of about 10% (> 90 days)  Validated value after 365days
  • 22. Effect freeze‐thaw cycles, long term  Modulus measurements  Diametral Sinusoïdal Compression –DSC  Long term freeze‐thaw cycles   Freeze‐thaw (50 cycles) between 24d et 36d  Modulus loss of 20% immediatly after the thermal sollicitations  Modulus recovery « normal » at long term
  • 23. Effect of 50 freeze‐thaw cycles, long term 9000 curve at 15°C without freeze- 8000 thaw Modulus at 10 Hz (MPa) 24 days 7000 - 20% 6000 37days 50 freeze-thaw 5000 cycles 4000 10 100 1000 Time from production (days)
  • 24. Rheologicals behavior study  Thermal stress, Contraints development 5.0 Tensile strain, MPa 4.0 HM A wit h 70 Contrainte (Mpa)df /100 bit umen 3.0 2.0 RECYFLEX  1.0 EBC 0.0 -35 -30 -25 -20 -15 -10 -5 0 5 Température (°C) Temperature, °C
  • 25. Recyflex AEC Observations  Process for optimun use of recyclable materials;  Cold treatment using composite binder  Strenghtened materials  Low emissions production  Accelarated curing time  No rutting   Avoid maniability over 3 hours
  • 26. Recyflex AEC Observations  Behavior between flexible and rigid pavements  DSC Modulus  E (15°C,10Hz) = 7600 Mpa   Optimum around 30d‐60d  Definitive loss of 10% in case of freeze‐thaw in the firsts hours of  cure  Temporary loss of 20% after freeze‐thaw if Recyflex AEC have  obtained the optimal cure  Low contrains development with thermal reduction  Fatigue analysis to complete
  • 27. Flexibles pavement structures comparaison, A20 Highway 80 M esal : 2X 2 lanes (3450 Truks/day/direction/TL over 20 years) Supposed Recyflex AEC Resilient Modulus = 3 000 MPa Recyflex AEC Chaussée Ecoroute Alternative 0 25 RUGOVIA TM 50 60 ESG-10 60 ESG-10 60 ESG-14 100 70 ESG-14 70 ESG-14 100 HMA 150 Binder 200 160 HMA-20 180 HMA-20 250 200 RECYFLEX AEC 300 350 Residual pavement structure Residual pavement structure 400 450 Residual pavement structure 500
  • 28. Highway , Alternate pavement design Hwy 485 Asphalt Pavement Design Alternate 1 AASHTO Structual Thickness (in.) Material Coefficient Value Structual total 3 S9.5D 0.44 1.32 4 I19.0D 0.44 1.76 11.5 B25.0C 0.3 3.45 0 Subgrade 7 Stabilization 0.14 0.98 Total Structual Value 7.51 Alternate 4 AASHTO Structual Thickness (in.) Material Coefficient Value Structual total 3 S9.5D 0.44 1.32 6 I19.0D 0.44 2.64 0 B25.0C 0.3 0 8 Recyflex 0.34 2.72 Subgrade 7 Stabilization 0.14 0.98 Total Structual Value 7.66
  • 30. Recyflex AEC, Arrival from Paris Main Runway Montreal airport‐ 1998 Arrival from Orlando
  • 33. In‐Place full depth reclamation Cold In place  Recycling using composite binder or bitumen  emulsion /foamed bitumen
  • 34. Example of using composite binder in‐Place Réalisation du projet  stabilisation Stabilisation 175mm (16/08 au 28/08) ±56800m²
  • 35.
  • 36. RECYCLOVIA®  Field of application  CIR In‐Place Cold recycling  Existing Asphalt  6 à >15 cm. pavement Chip Seal 1 à 5 cm. Chip Seal 1 à 5 cm. Granular base Granular Base or  Granular base Treated base  Supply of aggregate for gradation correction RECYCLOVIA ® RECYCLOVIA ® RECYCLOVIA ® In‐Place treatment : 6 à 15 cm   In‐Place treatment :8 à 15 cm   In‐Place treatment: 8 à 15 cm   Asphalt Emulsion with  Asphalt Emulsion / Foam asphalt Asphalt Emulsion / Foam asphalt Cement with Cement or hydrated lime With cement or hydrated lime + HMA / WMA wearing course Microsurfacing / Chip seal / Dense Cold mix (low trafic road)
  • 37. Recyclovia, in‐Place (CIR) Weight empty: 47 t Power : 800 hp 600 kW Lenght : 15 m Cement bin (4 t) Paver screed, extendable  Rotor for milling/recycling/mixing, with  Cement spreader unit equiped with tamper bar  possible injection of: compactor ‐ Foam asphalt ‐ Asphalt emulsion ‐ Water
  • 40. ‐Recycled cold treated materials behavior ‐Same mix design methodology for In‐plant, FDR and CIR; ‐Mechanical performances, Stability and Modulus; ‐Air Voids; ‐Retained Stability;  ‐Observations behavior: ‐Effect of RAP content Mix 1 Mix 2 Mix 3 Requirements 38% CC 40% CC 100% RAP Min. 16% RAP 40% RAP 45% Aggregates 20% Aggregates % Recovering Asphalt 0,63% 2,10% 5,38% % Added Bitumen 1,53% 1,85% 1,0% Marchall Stability at 7 000 @ 10 000 26 200 18 583 8 575 22.2°C (N) Retained Stability (%) 70 84 90 93 % Coating 50 82 88 95
  • 43. Thanks for your attention Janvier 2011 - page 43