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Fabric Coloring
Effect of Maysin
extracted from
Cornsilk (Maydis
stigma)

   Angeles, Julie Ann V.
 Dioneda, Ma. Christina M.
  IV – 28 BSE Chemistry
Statement of the Problem

• The main goal of this study is to determine the
  effectiveness of maysin extracted from cornsilk
  (Maydis stigma) as fabric colorant.

Specifically, it aims to obtain the following objectives:

1. Determine the presence of maysin from mature
   cornsilk (Maydis stigma) using phytochemical
   testing;
2. Compare the color of the fabric colorant
   produced from extracts of mature cornsilk
   (Maydis stigma) using various mordant (CuSO4,
   alum, and combination of CuSO4 and alum) and
   choose the best color using survey method.
3. Using the best mordant compare the pure cornsilk
   solution with the solutions of cornsilk extract and
   other ingredients in a (ingredient: cornsilk), 50:50 ratio
   and the equivalent color of commercial fabric dye in
   terms of the following:

a. color intensity of the fabric dye
b. lasting effect of the colorant
Materials and Methods

Collection    Verification of the
of Cornsilk   sample species in
 Sample               BPI




Preparation
   of the
  sample




              Preparation of the
Extraction                          Test for flavonoids
              ethanolic extracts
 Process
               of the cornsilk
Preparation     Mixing of fabric dye ingredients
of the fabric   and the addition of cornsilk
  colorant      extracts




                Soaking of the cloth into the
Mordanting      prepared mordants (CuSO4,
                   alum, CuSO4 + alum)
Observation of the
Test for the                                 effectiveness of the prepared
effectiveness   Application of the fabric     fabric colorant from cornsilk
of the fabric     dye onto the cloth         sample and determination of
colorant                                        the best mordant used.



                                                 Observation of the
                                                effectiveness of the
                                            combination of cornsilk extract
                                               with other natural dye
                                                    ingredients.



                                             Comparison of the prepared
                                               fabric colorant from pure
                                            cornsilk to the formulations and
                                             to the commercial fabric dye
Results and Discussions
Comparative Analysis of the color produced using different mordants applied
                                      in the fabrics
     Table 1.
     Color produced using pure cornsilk extract after the first dyeing process

                                          Mordants
Time (min.)        None          CuSO4               Alum        CuSO4 + Alum


    20




    25




    30
Survey Results
         Which has the best color intensity?


               CHOICES                                     NUMBER OF VOTES

a. Without mordant                                                          0

b. With CuSO4                                                               9

c. With alum                                                                1

d. With CuSO4 + alum                                                        2

                         TOTAL                                             12

                            *The fabrics used in the dyeing process were submerged in the following mordants.
Color Intensity of the Natural Fabric Colorants
          Table 2.
          Combination of natural extracts using the cloth submerged in the best mordant.
                                                                    Extracts
Time (min.)
                              Pure Cornsilk                   CE + OE                  CE + TE   Synthetic Dye



          20




          25




          30


Legend:        CE – cornsilk extracts         OE – Onion extract        TE – Tea extract
Table 3.
           Standard color of the natural extract versus the combination of the natural extract
           and corn silk extract
                                                                  Extracts
Time (min.)
                                  CE + OE                    OE                  CE + TE   TE



          20




          25




          30


Legend:        CE – cornsilk extracts   OE – Onion extract        TE – Tea extract
Lasting Effect of the Natural Fabric Colorants
          Table 4.
          Comparison of the dyed fabrics before and after 5 days of washing
                                                                          Extracts
 Time (min.)                                       CE                                         CE + OE
                                        Before                    After              Before             After



          20




          25




          30

Legend:        CE – cornsilk extracts        OE – Onion extract
Table 4.
               Comparison of the dyed fabrics before and after 5 days of washing
                                                                             Extracts
Time (min.)                                        CE + TE                                  Synthetic dye
                                         Before                      After              Before          After



          20




          25




          30


Legend:         CE – cornsilk extracts            TE – Tea extract
Conclusions

•The extracts from cornsilk have flavonoid contents and
thus could be made into a fabric dye.

•The intensity of the colorant was helped by CuSO4
which is chosen as the best mordant.

•The colorant made from the cornsilk extracts
has characteristics of a good fabric dye that is
comparable to that of the synthetic ones.
Recommendations
• Search for other extraction methods in extracting the
  compounds from the corn.
• Use other phytochemical tests to prove the presence
  of the flavonoid in the extract.
• Obtain crude extract using rotary evaporator.
• Use other fixing agents and increase the time of
  boiling the fabrics in the dye bath.
• Utilize other parts of the corn that is to be put on
  waste to make a fabric colorant.

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Fabric Coloring Effect of Maysin extracted from Cornsilk [Maydis stigma]

  • 1. Fabric Coloring Effect of Maysin extracted from Cornsilk (Maydis stigma) Angeles, Julie Ann V. Dioneda, Ma. Christina M. IV – 28 BSE Chemistry
  • 2. Statement of the Problem • The main goal of this study is to determine the effectiveness of maysin extracted from cornsilk (Maydis stigma) as fabric colorant. Specifically, it aims to obtain the following objectives: 1. Determine the presence of maysin from mature cornsilk (Maydis stigma) using phytochemical testing;
  • 3. 2. Compare the color of the fabric colorant produced from extracts of mature cornsilk (Maydis stigma) using various mordant (CuSO4, alum, and combination of CuSO4 and alum) and choose the best color using survey method.
  • 4. 3. Using the best mordant compare the pure cornsilk solution with the solutions of cornsilk extract and other ingredients in a (ingredient: cornsilk), 50:50 ratio and the equivalent color of commercial fabric dye in terms of the following: a. color intensity of the fabric dye b. lasting effect of the colorant
  • 5. Materials and Methods Collection Verification of the of Cornsilk sample species in Sample BPI Preparation of the sample Preparation of the Extraction Test for flavonoids ethanolic extracts Process of the cornsilk
  • 6. Preparation Mixing of fabric dye ingredients of the fabric and the addition of cornsilk colorant extracts Soaking of the cloth into the Mordanting prepared mordants (CuSO4, alum, CuSO4 + alum)
  • 7. Observation of the Test for the effectiveness of the prepared effectiveness Application of the fabric fabric colorant from cornsilk of the fabric dye onto the cloth sample and determination of colorant the best mordant used. Observation of the effectiveness of the combination of cornsilk extract with other natural dye ingredients. Comparison of the prepared fabric colorant from pure cornsilk to the formulations and to the commercial fabric dye
  • 9. Comparative Analysis of the color produced using different mordants applied in the fabrics Table 1. Color produced using pure cornsilk extract after the first dyeing process Mordants Time (min.) None CuSO4 Alum CuSO4 + Alum 20 25 30
  • 10. Survey Results Which has the best color intensity? CHOICES NUMBER OF VOTES a. Without mordant 0 b. With CuSO4 9 c. With alum 1 d. With CuSO4 + alum 2 TOTAL 12 *The fabrics used in the dyeing process were submerged in the following mordants.
  • 11. Color Intensity of the Natural Fabric Colorants Table 2. Combination of natural extracts using the cloth submerged in the best mordant. Extracts Time (min.) Pure Cornsilk CE + OE CE + TE Synthetic Dye 20 25 30 Legend: CE – cornsilk extracts OE – Onion extract TE – Tea extract
  • 12. Table 3. Standard color of the natural extract versus the combination of the natural extract and corn silk extract Extracts Time (min.) CE + OE OE CE + TE TE 20 25 30 Legend: CE – cornsilk extracts OE – Onion extract TE – Tea extract
  • 13. Lasting Effect of the Natural Fabric Colorants Table 4. Comparison of the dyed fabrics before and after 5 days of washing Extracts Time (min.) CE CE + OE Before After Before After 20 25 30 Legend: CE – cornsilk extracts OE – Onion extract
  • 14. Table 4. Comparison of the dyed fabrics before and after 5 days of washing Extracts Time (min.) CE + TE Synthetic dye Before After Before After 20 25 30 Legend: CE – cornsilk extracts TE – Tea extract
  • 15. Conclusions •The extracts from cornsilk have flavonoid contents and thus could be made into a fabric dye. •The intensity of the colorant was helped by CuSO4 which is chosen as the best mordant. •The colorant made from the cornsilk extracts has characteristics of a good fabric dye that is comparable to that of the synthetic ones.
  • 16. Recommendations • Search for other extraction methods in extracting the compounds from the corn. • Use other phytochemical tests to prove the presence of the flavonoid in the extract. • Obtain crude extract using rotary evaporator. • Use other fixing agents and increase the time of boiling the fabrics in the dye bath. • Utilize other parts of the corn that is to be put on waste to make a fabric colorant.