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Abrasion wear
performance of quenched
wear resistant steels
Niko Ojala1)*, Kati Valtonen1), Marke Kallio2), Joonas Aaltonen2),
Pekka Siitonen2) and Veli-Tapani Kuokkala1)
1) Tampere University of Technology,
Department of Materials Science, Tampere Wear Center, Finland
2) Metso Minerals, Inc., Finland
*email: niko.ojala@tut.fi
WTC 2013
Torino, Italy
8th – 13th September 2013
Motivation
• Quenched wear resistant steels are widely
used in industrial applications.
• The Brinell hardness grades are considered
as standards.
• But the wear performance is not extensively
studied.
Overview to topics
1) Materials and methods
2) Results
3) Discussion
0.142
0.158
0.163
0.165
0.172
0.173
0.176
0.180
0.186
0.189
0.192
0.199
0.202
0.208
0.216
0
100
200
300
400
500
600
700
800
900
1000
0.000
0.050
0.100
0.150
0.200
0.250
0 2 15 4 14 3 10 11 5 24 18 17 6 16 1
Surfacehardness[HV5]
Massloss[g]15 commercially available
400 HB steels were tested
• Sheet thicknesses were 10 or 12 mm.
• Decarburization layers were removed before testing
• Five steels were selected to closer study.
A B C D E
Crushing pin-on-disk
• The equipment is based on the pin-on-disk
principle
• In the tests, the pin is repeatedly pressed against
the gravel bed and the disk with a pneumatic
cylinder
– The pin does not come into direct contact with the
disk at any time
• The loss of material of both the pin and the disk
are measured by weighting, and the size change of
the abrasive during the test can measure by sieving
Test parameters
• Disk speed: 20 rpm
• Disk material: S355 (200 HV)
• Pin pressure: 1.1 bar
– 235 N nominal crushing force
• Pretest: 15 minutes, 10 minutes contact time
– 500 grams of 2/4 mm granite
• Test: 30 minutes, 20 minutes contact time
– With granite gravel
according to the table
100%
116%
131%
135%
153%
430
390
450
350
400
0
100
200
300
400
500
600
700
800
0%
20%
40%
60%
80%
100%
120%
140%
160%
A B C D E
Surfacehardness[HV5]
MasslosscomparedtosteelA
Up to 50 % difference in abrasion
wear performance
Average mass
losses [mg]
142 165 186 192 216
Tempered martensite with
untempered white martensite
A
B
C
D
20 µm
E
High-stress abrasive wear
EA
In general, the
more scratches
on the wear
surface, the
larger the mass
loss.
Wear mechanism
for scracthes:
two-body
abrasion
Surface characterization with
optical profilometer
• Estimated
average thickness
of the removed
material was
between 20 and
30 µm
• Deepest
scratches were
about 50-60 µm
deep
Optical profilometer image of steel C
Differences in wear surface
deformations
C
BA
E
Chemical compositions
• Hardenability
– Carbon
– Molybdenum (+Nickel)
– Boron
• Martensite formation
– Total amount of alloying
elements
– Amount of aluminum
and nickel
Steel A B C E
C 0.16 0.15 0.15 0.14
Si 0.4 0.28 0.22 0.38
Cr 0.14 0.37 0.41 0.46
Ni 0.04 0.07 0.09 0.04
Mo 0.15 0.1 0.01 0
Al 0.034 0.031 0.1 0.025
N 0.005 0.006 0.005 0.007
B 0.003 0.001 0.002 0.002
∑ 2.349 2.013 2.4 2.519
Chemical composition (wt%)
Steel D is removed due to possible manufacturing
faults
Concluding remarks
• Marked differences between the 400 HB grade
quenched steels in the wear performance
• Chemical composition: hardenability,
martensite formation and self temperability
• Microstructure: grain size and amount of
tempered martensite and white martensite
• Wear process: abrasive cutting
• Surface deformation: hardenability and self
temperability (a localized ‘requench’ process)
Thank you for your attention!
Niko Ojala
Research Scientist, PhD student
Tampere University of Technology
Department of Materials Science, Tampere Wear Center
P.O.Box 589, FI-33101 Tampere, Finland
phone: +358 50 317 4516
email: niko.ojala@tut.fi
www.tut.fi/twc/en
Acknowledgements

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Abrasion wear performance of quenched wear resistant steels

  • 1. Abrasion wear performance of quenched wear resistant steels Niko Ojala1)*, Kati Valtonen1), Marke Kallio2), Joonas Aaltonen2), Pekka Siitonen2) and Veli-Tapani Kuokkala1) 1) Tampere University of Technology, Department of Materials Science, Tampere Wear Center, Finland 2) Metso Minerals, Inc., Finland *email: niko.ojala@tut.fi WTC 2013 Torino, Italy 8th – 13th September 2013
  • 2. Motivation • Quenched wear resistant steels are widely used in industrial applications. • The Brinell hardness grades are considered as standards. • But the wear performance is not extensively studied.
  • 3. Overview to topics 1) Materials and methods 2) Results 3) Discussion
  • 4. 0.142 0.158 0.163 0.165 0.172 0.173 0.176 0.180 0.186 0.189 0.192 0.199 0.202 0.208 0.216 0 100 200 300 400 500 600 700 800 900 1000 0.000 0.050 0.100 0.150 0.200 0.250 0 2 15 4 14 3 10 11 5 24 18 17 6 16 1 Surfacehardness[HV5] Massloss[g]15 commercially available 400 HB steels were tested • Sheet thicknesses were 10 or 12 mm. • Decarburization layers were removed before testing • Five steels were selected to closer study. A B C D E
  • 5. Crushing pin-on-disk • The equipment is based on the pin-on-disk principle • In the tests, the pin is repeatedly pressed against the gravel bed and the disk with a pneumatic cylinder – The pin does not come into direct contact with the disk at any time • The loss of material of both the pin and the disk are measured by weighting, and the size change of the abrasive during the test can measure by sieving
  • 6.
  • 7. Test parameters • Disk speed: 20 rpm • Disk material: S355 (200 HV) • Pin pressure: 1.1 bar – 235 N nominal crushing force • Pretest: 15 minutes, 10 minutes contact time – 500 grams of 2/4 mm granite • Test: 30 minutes, 20 minutes contact time – With granite gravel according to the table
  • 8. 100% 116% 131% 135% 153% 430 390 450 350 400 0 100 200 300 400 500 600 700 800 0% 20% 40% 60% 80% 100% 120% 140% 160% A B C D E Surfacehardness[HV5] MasslosscomparedtosteelA Up to 50 % difference in abrasion wear performance Average mass losses [mg] 142 165 186 192 216
  • 9. Tempered martensite with untempered white martensite A B C D 20 µm E
  • 10. High-stress abrasive wear EA In general, the more scratches on the wear surface, the larger the mass loss. Wear mechanism for scracthes: two-body abrasion
  • 11. Surface characterization with optical profilometer • Estimated average thickness of the removed material was between 20 and 30 µm • Deepest scratches were about 50-60 µm deep Optical profilometer image of steel C
  • 12. Differences in wear surface deformations C BA E
  • 13. Chemical compositions • Hardenability – Carbon – Molybdenum (+Nickel) – Boron • Martensite formation – Total amount of alloying elements – Amount of aluminum and nickel Steel A B C E C 0.16 0.15 0.15 0.14 Si 0.4 0.28 0.22 0.38 Cr 0.14 0.37 0.41 0.46 Ni 0.04 0.07 0.09 0.04 Mo 0.15 0.1 0.01 0 Al 0.034 0.031 0.1 0.025 N 0.005 0.006 0.005 0.007 B 0.003 0.001 0.002 0.002 ∑ 2.349 2.013 2.4 2.519 Chemical composition (wt%) Steel D is removed due to possible manufacturing faults
  • 14. Concluding remarks • Marked differences between the 400 HB grade quenched steels in the wear performance • Chemical composition: hardenability, martensite formation and self temperability • Microstructure: grain size and amount of tempered martensite and white martensite • Wear process: abrasive cutting • Surface deformation: hardenability and self temperability (a localized ‘requench’ process)
  • 15. Thank you for your attention! Niko Ojala Research Scientist, PhD student Tampere University of Technology Department of Materials Science, Tampere Wear Center P.O.Box 589, FI-33101 Tampere, Finland phone: +358 50 317 4516 email: niko.ojala@tut.fi www.tut.fi/twc/en Acknowledgements